Effect of anionic surfactant on vaterite CaCO3

Calcium carbonate (CaCO₃) crystals with various shapes have been synthesized by aging calcium chloride and urea hybrid solution containing sodium dodecylsulfonate (SDSN) or sodium dodecylbenzenesulfonate (SDBS) in a 90 °C bath. The effects of SDSN and SDBS on the morphology and polymorph of precipitated CaCO₃ are investigated with the help of scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) spectrometer and X-ray diffraction (XRD). Flower-like vaterite changes from monolayer to multilayer structure with the increase of SDSN concentration. While the crystal shape changes from plate-like, through rose-shaped, hat-like, to bicone-like as the concentration of SDBS is increased.     

PMD补偿器和PMD补偿接收机的特性

以介绍ITU—TG．666建议主要内容的方式，讨论了有关PMD补偿器和PMD补偿接收机的特性。     

Synthesis and characterization of Ti-SBA-16 ordered mesoporous silica composite

Ti-SBA-16 mesoporous silica with a cubic Im3m structure has been successfully synthesized through prehydrolysis of a silica precursor in the presence of a tri-block copolymer F127 under acidic condition. X-ray diffraction (XRD) shows that the highly ordered mesostructure was maintained even at the high loading of titanium up to 5.5 (bulk molar ratio SiO₂/TiO₂). UV–vis and Raman spectroscopy reveal that the titanium species was highly dispersed in the silica framework with tetrahedral coordinate and octahedral coordinate, respectively. N₂-adsorption data exhibit that the BET surface, pore size and pore volume were maintained with an increase of titanium species loading for this cubic Im3m mesoporous composite. SEM image shows its amorphous morphology. The synthesis of mesoporous TiO₂-containing SBA-16 composite with a cubic Im3m structure will open new applications for catalysts.     

Coning motion stability of wrap around fin rockets

Both the asymptotical stability criterion and the bounded stability criterion of the coning motion for wrap around fin(WAF) rockets are proposed through the analy-sis of coning motion equations,which can be easily used to determine the exis-tence of the coning motion during the rocket design. The correctness of the crite-rions is verified by mathematical simulation examples of a WAF rocket with differ-ent setting angles. It is also found that the setting angle of WAF has great effects on the rolling moment and side moment of the rocket.     

Comparative study of β-Si3N4 powders prepared by SHS sintered by spark plasma sintering and hot pressing

β-Si3N4 powders prepared by self-propagating high-temperature synthesis (SHS) with additions of Y2O3 and Al2O3 were sintered by spark plasma sintering (SPS). The densification, microstructure, and mechanical properties of Si3N4 ceramics prepared using this method were compared with those obtained by hot pressing process. Well densified Si3N4 ceramics with finer and homo- geneous microstructure and better mechanical properties were obtained in the case of the SPS technique at 200°C lower than that of hot pressing. The microhardness is 15.72 GPa, the bending strength is 716.46 MPa, and the fracture toughness is 7.03 MPa?m1/2.     

换流站直流刀闸发热改造

就两起换流站直流刀闸发热的问题进行技术分析,从技术、经济及工程施工难易程度方面进行方案比较,在回路电阻计算的基础上提出了增加旁路导电带的改造方案.实施改造后在实际运行中测量结果表明改造结果良好.     

大功率立式电机转子有限元结构分析与优化

基于Pro/Engineer建立了某型号的大功率电机转子的实体模型和虚拟样机模型,在MSC.PATTERN/NASTRAN环境下,利用有限元方法进行了电机转子的动力学仿真、应力位移仿真,得到了转子两端轴承的力学状态、转子的应力、位移等参数值.根据仿真结果,进行了转子的强度和刚度校核,分析了转子的主要破坏形式和危险位置.结果表明现有电机转子的结构基本满足设计要求,并在此基础上优化转子外径和支承结构,减小电机振动,优化工艺,为同类产品的开发和改进提供了参考.     

基于Shear-warp的交互式海量数据场体绘制算法

提出了基于min-max Octree快速分类Shear-warp的交互式海量数据场体绘制算法.主要包括根据海量数据的特征,快速读入数据以及设计适当的不透明度传递函数;建立Summed-Area表与min-max Octree数据结构,并对体数据进行快速分类,然后,利用分类的结果进行快速体绘制.实验证明该方法不仅效率高,而且显示效果好.     

提高电梯运行舒适感的有效途径

本文全面论述了影响电梯运行舒适感的原因，并提出了从电气和机械两个方面解决这些问题的办法。     

关于网络课堂的构建

优化教学手段、改善教学技术是保持高校设计艺术教育先进性的体现。利用网络实现课堂教学的互补也是新时期对教师提出的一项要求。本文介绍了构筑在“你我家”网络真实社区（http：／／www．niwojia．com）平台上的专业合作，交流组织“艺术设计联盟”（http：／／design．niwojia．com）的形成背景、发展历程和主要特点。