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101.
102.
Water-soluble amino acid derivatives of gadolinium (Gd) endohedral metallofullerenes (AAD-EMFs), Gd@C82Om(OH)n(NHCH2CH2COOH)l (m ≈ 6, n ≈ 16 and l ≈ 8) are synthesized by a direct reaction of the pure endohedral metallofullerene Gd@C82 with an excess of alkaline solution of β-alanine. The structure of the AAD-EMFs is characterized by FTIR, XPS and laser-desorption time-of-flight (LD-TOF) mass spectrometries. Water proton relaxivity analysis indicates that the longitudinal relaxivity R1 (the effect on 1/T1, 9.1 mM−1 s−1) of AAD-EMFs is higher than that of the commercial MRI contrast agent, Magnevist (gadolinium-diethylenetriaminepentaacetic acid, Gd-DTPA, 5.6 mM−1 s−1). The MRI phantom studies are performed to confirm the high efficiency of this sample as MRI contrast agents. 相似文献
103.
Various electrochemical methods with different conditions were used to prepare lead dioxide (PbO2). The observation revealed that the morphology of deposited PbO2 could be controlled by simply changing deposition parameters. Under the condition of oxygen evolution, which dominates the electrode process, uniformly distributed high porous structured PbO2 was formed. The results indicated that large current density or high potential polarization should be one of the most important and necessary factors for forming high surface area PbO2 deposit. Only β-PbO2 was identified by X-ray diffraction measurement for the deposit prepared by present methods and solution. One potential application of this method is to prepare nanoscaled PbO2 parallel lines. 相似文献
104.
油田废水电解杀菌研究 总被引:1,自引:0,他引:1
采用电解杀菌技术处理油田废水,研究了电解时间、电流强度、极板间距以及电极联结方式等因素对废水中硫酸盐还原菌杀灭效果的影响。结果表明,油田废水经3min电解杀菌,硫酸盐还原菌杀灭率高达99.90%。随着电解时间的增加,硫酸盐还原菌的杀菌率进一步提高;电流强度增加,硫酸盐还原菌的杀灭率升高。在电流强度保持不变的情况下,随着极板间距增加,极板之间电压升高,更有利于杀灭硫酸盐还原菌。在极板间电流强度相同的条件下,两种电极联结方式的杀菌率差别不大,杀菌率均在99.9%以上。 相似文献
105.
106.
Handling occlusion is a very challenging problem in object detection. This paper presents a method of learning a hierarchical model for X-to-X occlusion-free object detection (e.g., car-to-car and person-to-person occlusions in our experiments). The proposed method is motivated by an intuitive coupling-and-decoupling strategy. In the learning stage, the pair of occluding X?s (e.g., car pairs or person pairs) is represented directly and jointly by a hierarchical And–Or directed acyclic graph (AOG) which accounts for the statistically significant co-occurrence (i.e., coupling). The structure and the parameters of the AOG are learned using the latent structural SVM (LSSVM) framework. In detection, a dynamic programming (DP) algorithm is utilized to find the best parse trees for all sliding windows with detection scores being greater than the learned threshold. Then, the two single X?s are decoupled from the declared detections of X-to-X occluding pairs together with some non-maximum suppression (NMS) post-processing. In experiments, our method is tested on both a roadside-car dataset collected by ourselves (which will be released with this paper) and two public person datasets, the MPII-2Person dataset and the TUD-Crossing dataset. Our method is compared with state-of-the-art deformable part-based methods, and obtains comparable or better detection performance. 相似文献
107.
Huapeng Yu Yongxin Chang Pei Lu Zhiyong Xu Chengyu Fu Yafei Wang 《Computers & Electrical Engineering》2014
In this paper, we make use of biologically inspired selective attention to improve the efficiency and performance of object detection under clutter. At first, we propose a novel bottom-up attention model. We argue that heuristic feature selection based on bottom-up attention can stably select out invariant and discriminative features. With these selected features, performance of object detection can be improved apparently and stably. Then we propose a novel concept of saccade map based on bottom-up attention to simulate the saccade (eye movements) in vision. Sliding within saccade map to detect object can significantly reduce computational complexity and apparently improve performance because of the effective filtering for distracting information. With these ideas, we present a general framework for object detection through integrating bottom-up attention. Through evaluating on UIUC cars and Weizmann–Shotton horses we show state-of-the-art performance of our object detection model. 相似文献
108.
109.
110.
合成丁酸异戊酯的新方法 总被引:3,自引:0,他引:3
采用超强酸代替浓硫酸作催化剂,对丁酸异戊酯合成反应进行了研究,讨论了影响收率的多种因素,在最佳条件下,酯化反应时间短,催化剂可以重复使用,丁酸异戊酯收率达到98%。 相似文献