Physico-chemical properties of glycyrrhizic acid in aqueous media. I. Surface-active properties and formation of molecular aggregates (author''s transl)

As shown in 138 embryos and fetuses in the 40-285 mm crown-rump length range, carpal and carpal-metacarpal "fusions" arise from incomplete separation of the cartilaginous precursors rather than from failure of initiation, thus accounting for the "fusions" seen in postnatal radiographs and the grooves that are evident enough in adult fusions. Radiographs selected from over 20,000 apparently normal individuals provide postnatal counterparts for the prenatal examples shown in histological sections.     

High temperature superconductor micro-superconducting-quantum-interference-device magnetometer for magnetization measurement of a microscale magnet

We have developed a high temperature superconductor (HTS) micrometer-sized dc superconducting quantum interference device (SQUID) magnetometer for high field and high temperature operation. It was fabricated from YBa2Cu3O7-delta of 92 nm in thickness with photolithography techniques to have a hole of 4x9 microm2 and 2 microm wide grain boundary Josephson junctions. Combined with a three dimensional magnetic field coil system, the modulation patterns of critical current Ic were observed for three different field directions. They were successfully used to measure the magnetic properties of a molecular ferrimagnetic microcrystal (23x17x13 microm3), [Mn2(H2O)2(CH3COO)][W(CN)8]2H2O. The magnetization curve was obtained in magnetic field up to 0.12 T between 30 and 70 K. This is the first to measure the anisotropy of hysteresis curve in the field above 0.1 T with an accuracy of 10(-12) J T(-1) (10(-9) emu) with a HTS micro-SQUID magnetometer.     

Metallurgical and tribological investigations of aluminium bronze bushes made by a novel centrifugal casting technique

Aluminium bronzes have been used as high strength, corrosion and wear resistance alloys for many decades. However, the alloy has a narrow solidification range and a complex nature which has confined its use to a limited field of applications. Published data on the wear characteristics and the metallurgical nature of the alloy system is limited, leaving wide possibilities for research. In the work described in this paper a study has been made of the metallurgical and tribological characteristics of aluminium bronzes conforming to BS 1400 AB2 specification. A novel centrifugal casting technique using a bonded sand lining integrated into a standard rotating die was adapted to cast a series of test bushes. Mechanical and microscopic aspects are studied and an attempt is made to correlate the physical properties with the tribological behaviour of the bushes. The results show that the test behaviour of the test bush was in some respects better than that of commercially produced bushes made by forging techniques. Detrimental embrittlement, due to ‘self annealing’ is significantly reduced by the adoption of the novel centrifugal casting technique referred to above.     

Cause–effect analysis on Fukushima accident reports – What did McMaster undergraduate students learn?

In the ENG PHYS 4ES3 Course “Special Topics in Energy Systems (2014–2015)” in McMaster University, sixteen 4th-year undergraduate students studied the Fukushima accident, discussed the causes of accident and its impacts on the energy systems from the sustainability point of view, made the oral presentation and submitted the reports. In this paper, a cause–effect and causal-loop analysis was applied to the discussion in the reports, the diagram of cause–effect relationship was drawn, and the important problems were extracted from the diagram. It was found that the important problems and the diagram of cause–effect relationship McMaster undergraduate students considered were similar to the essential problems and the diagram Horii pointed out, although Interim Report of the Investigation Committee on the Accident at Fukushima Nuclear Stations of Tokyo Electric Power Company which Horii used was not adopted in the reports submitted by students.     

Characteristics of the Arc Voltage of a High‐Current Air Arc in a Sealed Chamber

The effect of the arc voltage on various factors of design and control was investigated for high currents in order to develop design guidelines for circuit breakers. In this study, the dependence on such factors, namely, the current, arc length, electrode surface area, and internal pressure of the arc voltage, was evaluated quantitatively. As a result of the evaluations, it was estimated that the arc voltage near the electrode surface rises linearly with the arc current and the power ?0.8 of the surface area, and that the voltage in the arc column rises as the 0.3 power of the pressure increase. We confirmed the validity of the estimated voltage characteristics by comparison with the generated voltage in an actual arc‐extinction chamber. The characteristics of the estimated voltage can provide effective guidelines for the design of arc extinguishing chambers. © 2013 Wiley Periodicals, Inc. Electr Eng Jpn, 186(1): 34–42, 2014; Published online in Wiley Online Library ( wileyonlinelibrary.com ). DOI 10.1002/eej.22487     

Production of thin graphite sheets for a high electrical conductivity film by the mechanical delamination of ternary graphite intercalation compounds

Herein we propose a production scheme for conductive films composed of thin graphite sheets with high crystallinity and polymeric resin. The crystalline graphite sheets were successfully produced from natural graphite powder by solution-phase synthesis of graphite intercalation compounds (GICs), following a wet planetary-ball milling under mild conditions. The shear forces in the milling pot lead to a peeling of graphite flakes. Taking into consideration the interlayer bonding force, the delamination should be preferentially done from the expanded GICs interlayer rather than intrinsic graphite one. Some composite films derived from the phenolic resin and flaky graphite sheets displayed much higher electrical conductivities compared to the film from the feed graphite particles. We also demonstrate the stage structure of synthetic GICs affected the film conductivity. The composite films made from exfoliated products of ground (around stage IV) GICs exhibited high electrical conductivity with a small amount of the graphite sheets.