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161.
The influence of liquid penetration at grain boundary regions on the rate of advance of the solid-liquid interface during
isothermal solidification of transient liquid phase (TLP) brazed nickel joints has been examined. The test samples used in
this study were Ohno-cast nickel with a grain size of >4 mm and a fine-grained nickel with a grain size of around 40 μm. Both
Ni-base materials had the same chemical composition. The rate of isothermal solidification was greater when fine-grained nickel
was employed during TLP brazing using Ni-11 wt pct P filler metal at 1200 °C. Liquid penetration at grain boundaries accelerates
the isothermal solidification process by increasing the effective solid-liquid interfacial area and increasing the rate of
solute diffusion into the base material. An analysis of electron channeling patterns has confirmed that random high-angle
boundaries have a greater influence on the rate of isothermal solidification than ordered boundaries including small-angle
or twin boundaries.
Formerly Visiting Scientist, Department of Metallurgy and Materials Science, University of Toronto.
Formerly Postdoctoral Fellow, Department of Metallurgy and Materials Science, University of Toronto 相似文献
162.
163.
The atomistic structure and energies of high-index interphase boundaries are explored using a combination of molecular statics
and dynamics simulations with embedded atom potentials. We investigate planar boundaries between the α2 and γ phases in the Ti−Al system. The class of boundaries considered has a high-index boundary orientation; the orientation
relationship between the α2 and γ phases also is high index, and a set of planes from each phase meet edge to edge at the boundary plane. For the particular
case of a boundary that is commensurate in one direction and coincides with a moiré plane given by the so-called “Δg” diffraction condition, the boundary is not structurally singular, but it is energetically stable and does not appear to
dissociate into other low-energy configurations. Misfit compensating defects are not observed; misfit in directions other
than the commensurate one appears to be distributed uniformly. The boundary energy is evaluated as a function of the orientation
of the boundary plane, and the edge-to-edge (moiré) boundary is found to lie in an energy cusp.
This article is based on a presentation made in the “Hume-Rothery Symposium on Structure and Diffusional Growth Mechanisms
of Irrational Interphase Boundaries,” which occurred during the TMS Winter meeting, March 15–17, 2004, in Charlotte, NC, under
the auspices of the TMS Alloy Phases Committee and the co-sponsorship of the TMS-ASM Phase Transformations Committee. 相似文献
164.
165.
The synthesis of thermal-shock-resistant materials from the system Ta2O5WO3 was investigated. Ta2WO8 had a very low unit-cell thermal expansion coefficient (+0.5 X 10–6° C–1). Ta30W2O81 also had a relatively low coefficient (+4.0 X 10–6 ° C–1) and a thermal durability over 1600° C. The thermal expansion curves of these polycrystalline ceramics were lowered because of microcracks caused by the large thermal expansion anisotropy of the crystal axes and were accompanied by hysteresis loops. The densification of Ta2WO8 ceramic was promoted by the addition of some metal oxides, and the strong ceramic of Ta30W2O81 was obtained by controlling grain growth. 相似文献
166.
Microbial sensor for preliminary screening of mutagens utilizing a phage induction test 总被引:1,自引:0,他引:1
For the preliminary screening of mutagens, a novel microbial sensor system was developed utilizing a phage induction test. Escherichia coli lysogenic strain GY5027 and nonlysogenic strain GY5026 were used in this study. The number of living cells was determined by measuring the respiration of cells immobilized onto an oxygen electrode. The injection of a mutagen, such as AF-2 and MNNG, caused the phage induction in the lysogenic strain, resulting in the decreased respiration of only the lysogenic strain immobilized onto the oxygen electrode but not of nonlysogenic strain. The rate of current increase correlated well with the concentration of mutagens. The sensor responses to the antibiotics and bactericides were definitely different from those of mutagens. Therefore, utilization of this microbial sensor system makes possible the estimation of a substrate's mutagenicity. 相似文献
167.
X. S. Ning K. Suganuma T. Okamoto A. Koreeda Y. Miyamoto 《Journal of Materials Science》1989,24(8):2879-2883
Two kinds of additive-free silicon nitride ceramics were brazed with aluminium; one was with as-ground faying surfaces and
the other was with faying surfaces heat-treated at 1073K for 1.8 ksec in air. The heat-treatment of the silicon nitride ceramics
formed a silicon oxynitride layer on the faying surfaces and increased the brazing strength of the joints. A silica-alumina
non-crystalline layer and a β′-sialon layer were formed successively from the aluminium side at the interface of the joints.
The heat-treatment which made the former layer thicker is a necessary process in making reliable, strong brazed joints. 相似文献
168.
169.
170.
A. Sadananda Chary S. Narender Reddy T. Chiranjivi 《Journal of Materials Science》1989,24(6):2199-2202
Dielectric properties, dielectric constant (k), dielectric loss (tan δ) and a.c. conductivity (σ) in the solution-grown single crystals of RbNO3 are presented from room temperature to about 200°C covering the frequency range 102 to 105 Hz. A broad peak observed in tan δ-frequency data between 103 and 105Hz is thought to be due to impurity-vacancy dipoles. The sudden rise of three parameters near 160°C is attributed to the known
phase transition from trigonal to CsCl structure. 相似文献