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981.
The effect of side chain length of π-conjugated poly(9,9-dialkylfluorene)s has been studied in semi-dilute (10 mg/mL) toluene solutions using small-angle neutron scattering (SANS) and 1H and 2H NMR spectroscopies. Under these conditions, SANS data indicate that poly(9,9-dinonylfluorene) and poly(9,9-dioctylfluorene) are dissolved down to the molecule level and appear as elongated one-dimensional chains (length >20-30 nm). In contrast, the shorter side chain polymers exhibit a self-association so that poly(9,9-diheptylfluorene) forms thin sheet-like (∼1 nm) and poly(9,9-dihexylfluorene) thin (∼1 nm) and thick sheet-like (>6 nm) aggregates. 1H NMR data, together with the density functional theory (DFT) calculations, however, show that this occurs without changes in the conformation of the polymer backbone. 相似文献
982.
983.
A. Ya. Eremin Ya. B. Kukolev R. R. Gilyazetdinov L. A. Makhortova Yu. V. Stepanov N. V. Tsarev 《Coke and Chemistry》2008,51(11):434-439
The efficiency of selective crushing with pneumomechanical separation is investigated as a function of the quality of the coal batch and the operating conditions of the fluidized-bed separator. 相似文献
984.
W. Kulisch C. Popov H. Rauscher L. Sirghi T. Sasaki S. Bliznakov F. Rossi 《Diamond and Related Materials》2008,17(7-10):1116-1121
Nucleation and growth, but especially the development of the morphology of nanocrystalline diamond/amorphous carbon (NCD/a-C) nanocomposite films have been investigated by systematic variation of three important parameters, namely the deposition time, the growth rate, and the substrate pre-treatment used to enhance the nucleation density. The films have been characterized, among others, by scanning electron microscopy, atomic force microscopy, and Fourier transform infrared spectroscopy. It is shown that, by successive addition of ultradispersive diamond powder to the suspension of nanocrystalline diamond powder in n-pentane used for the ultrasonic pre-treatment, the nucleation density can be enhanced by two orders of magnitude from 1 · 108 cm− 2 to > 1 · 1010 cm− 2. This reduces the thickness required to achieve closed films from 1 µm to 100 nm. However, once coalescence of the individual nodules emerging from the nucleation sites has taken place the films loose “memory” of the nucleation step and start to develop the typical NCD morphology consisting of larger features with diameters of some hundreds of nm which are in turn composed of much smaller features. Irrespective of the feature size and of the parameters used, the films of this investigation possess AFM rms roughnesses of 9–13 nm, indicating that rms values are not sufficient to characterize NCD surfaces. 相似文献
985.
The energy dependence of the relative yield of delayed neutrons and of half-lives of their precursor nuclei with fissioning
239Pu by 14.2–17.9 MeV neutrons is measured. The data obtained are analyzed in terms of the average half-life 〈T〉 of the precursor
nuclei of the delayed neutrons. It is shown that the observed growth of 〈T〉 with increasing primary neutron energy in the
energy range studied is due predominately to opening of the channels for the emission fission of nuclei. Comparing the data
on the average half-life of the precursor nuclei of delayed neutrons obtained in the present work with those obtained by other
authors showed that the anomalously high values of 〈T〉 are due to methodological features of the experiment which are related
with the properties of the reaction T(d, n)4He used as a neutron source on electrostatic charged-particle accelerators. The data obtained are of great value for developing
instrumentational nondestructive means for determining the nuclide composition of nuclear fuel based on the detection of delayed
neutrons.
__________
Translated from Atomnaya énergiya, Vol. 101, No. 6, pp. 441–444, December, 2006. 相似文献
986.
Patterns in the solidification of a pure material are dealt with in this article. Results, deduced from a simple model based on heat conduction in the two phases and the effect of surface tension on the equilibrium temperature at the moving front, present a guide for experimental work. By introducing far-field conditions imitating what can be achieved in an experiment, we explain how the depths of the phases and the width of the container influence the patterns that can be seen if one advances the control variable to the critical point and then just beyond. Our new result is the existence of a third critical point. It occurs at small wave numbers and it is independent of surface tension. It appears because we take the depths of the phases into account. These depths are input values that offer the possibility of controlling crest-to-trough conduction, stabilizing in the solid, destabilizing in the liquid. The new critical point, and the patterns attending its appearance, can be found in cells of easily attainable widths. 相似文献
987.
Steady-State Control Reference and Token Conservation Laws in Continuous Petri Net Systems 总被引:1,自引:0,他引:1
Mahulea C. Ramirez-Trevino A. Recalde L. Silva M. 《Automation Science and Engineering, IEEE Transactions on》2008,5(2):307-320
This paper addresses several questions related to the control of timed continuous Petri nets under infinite server semantics. First, some results regarding equilibrium states and control actions are given. In particular, it is shown that the considered systems are piecewise linear, and for every linear subsystem the possible steady states are characterized. Second, optimal steady-state control is studied, a problem that surprisingly can be computed in polynomial time, when all transitions are controllable and the objective function is linear. Third, an interpretation of some controllability aspects in the framework of linear dynamic systems is presented. An interesting finding is that noncontrollable poles are zero valued. 相似文献
988.
An empirical investigation of bias and variance in time series forecasting: modeling considerations and error evaluation 总被引:1,自引:0,他引:1
Bias and variance play an important role in understanding the fundamental issue of learning and generalization in neural network modeling. Several studies on bias and variance effects have been published in classification and regression related research of neural networks. However, little research has been done in this area for time-series modeling and forecasting. We consider modeling issues related to understanding error components given the common practices associated with neural-network time-series forecasting. We point out the key difference between classification and time-series problems in consideration of the bias-plus-variance decomposition. A Monte Carlo study on the role of bias and variance in neural networks time-series forecasting is conducted. We find that both input lag structure and hidden nodes are important in contributing to the overall forecasting performance. The results also suggest that overspecification of input nodes in neural network modeling does not impact the model bias, but has significant effect on the model variance. Methods such as neural ensembles that focus on reducing the model variance, therefore, can be valuable and effective in time-series forecasting modeling. 相似文献
989.
Weldable primers are thin zinc-rich organic coatings that are weldable due to the electrical conductivity provided by the zinc dust. They are used in the automotive industry to provide corrosion protection in regions of difficult access. The zinc particles are highly susceptible to corrosion attack and, due to the small thickness, the protection conferred by these systems is limited. 相似文献
990.
In this paper passive and reciprocal thermal networks are introduced which model the finite velocity of heat propagation. In particular it is shown that the theory of distributed and discretized thermal networks deduced from the heat diffusion equation and the multi-point moment matching technique for deriving approximated lumped thermal networks of small state-space dimensions can be extended to thermal networks ruled by the hyperbolic heat equation. 相似文献