高含硫钻井液缓蚀剂的合成及性能研究

本文合成了抑制H₂S腐蚀的咪唑啉类缓蚀剂,并研究了它们的性能。正交试验表明,最佳合成条件是:反应温度:190～200℃;酸:胺(mol比)=1:1.05;反应时间以3～5小时为宜。根据以上条件合成的缓蚀剂,在含有3200mg/lH₂S的泥浆中,用量为0.2%时,抑制效果能达到80～90%,与碱式碳酸锌复配使用时,能提高缓蚀效率和降低碱式碳酸锌的用量,并发现缓蚀剂与CaO之间具有明显的协同效应。泥浆流变性能试验表明,缓蚀剂能提高泥浆的动切力和动塑比,对失水量影响不大。此外,利用X-射线衍射试验证明:(1)低碳钢在含H₂S的泥浆中,腐蚀产物的主要组成为Fe₉S₆;(2)H₂S会破坏FCLS的稳定性,分解出Fe²⁺,与H₂S反应生成面心立方的Fe₂S₄。     

稀土树脂相分光光度法研究

在HCl—KCl(pH0.5)介质中,稀土—三溴偶氮胂二元络合物能较好地被阴离子交换树脂吸附。RE_2O_8在0～8μg/25ml范围内符合比尔定律,以双波长等吸收点法(测量波长λ_1=650nm,参比波长λ_2=740nm)扣除树脂背景影响,应用于稀土矿中稀土总量测定,结果令人满意。     

Exploratory analysis of brain connectivity with ICA.

Covariance-based methods of exploration of functional connectivity of the brain from functional magnetic resonance imaging (fMRI) experiments, such as principal component analysis (PCA) and structural equation modeling (SEM), require a priori knowledge such as an anatomical model to infer functional connectivity. In this research, a hybrid method, combining independent component analysis (ICA) and SEM, which is capable of deriving functional connectivity in an exploratory manner without the need of a prior model is introduced. The spatial ICA (SICA) derives independent neural systems or sources involved in task-related brain activation, while an automated method based on the SEM finds the structure of the connectivity among the elements in independent neural systems. Unlike second-order approaches used in earlier studies, the task-related neural systems derived from the ICA provide brain connectivity in the complete statistical sense. The use and efficacy of this approach is illustrated on two fMRI datasets obtained from a visual task and a language reading task.     

论GPS星座组成及若干抗AS方案

本文首先讨论GPS星座组成及美国的用政策，阐述了AS措施及其对GPS测量的影响。然后，对抗AS的若干方案进行介绍，分别对平方法、互相关法、码相关干法及P－W技术（Ashtech法）进行叙述和评论，指出它们的优缺点，评述它们在GPS技术发展过程所起的作用。最后，对GPS星座建成后的形势作了小结，并对当前我国GPS事业的有关问题提出四点建议。     

叶绿素衍生物─CPD_4在人血清中的激发和发射荧光谱

叶绿素衍生物４号（ＣＰＤ４）是一种新型中药光敏剂，本文研究了不同浓度的ＣＰＤ４分别在含１０％不同血型人血清的生理盐水中以及纯生理盐水中的激发和发射荧光光谱，并对结果进行了分析，结论对ＣＰＤ４在光动力诊断恶性肿瘤的临床应用具有一定的指导意义．     

石家庄市CATV系统网络技术指标分配初探

在ＣＡＴＶ系统网络工程设计中，技术指标的分配产关键问题。本文介绍了石家庄市在系统设计时采用的符合实际的设计程序，并对系统前端，传输及用户网各部分技术指标的确定，计算与分配方法，指标的核算等作了较详细地阐述，以供同行参考。     

双波长Nd：YAG脉冲激光器的实验研究

根据多波长同时振荡条件，我们建立了大能量１０６４ｎｍ和１３１８ｎｍ同时运转的双波长脉冲Ｎｄ：ＹＡＧ激光器。得到了１０６４ｎｍ和１３１８ｎｍ的激光输出能量分别为０．５９４Ｊ和０．８６１Ｊ，效率分别为０．３１％和０．４５％。实验结果说明了该双波长激光器有较好的时间和空间重选性。     

稀土在搪瓷面釉上应用的研究

采用稀土氧化物和无机化合物的复合物（不简称ＲＩ－复合物）作为搪瓷釉浆悬浮剂，使之全部或大部分代替粘土，进行了一系列试验，已获得成功，突破了长期来搪瓷工业离不开粘土的传统工艺，并实现了工业化生产。     

镀镍云母导电复合材料的研究

对云母粒子化学镀镍及以LDPE为基材,镀镍云母粒子为填料制备的导电复合材料进行研究。认为此种导电复合材料只有质量轻、强度大及良好的导电等性能。     

Condom use: A self-efficacy model.

A survey of heterosexually active college students gathered information about condom use, self-efficacy (SE), outcome expectancies, sexual attitudes, peer group influences, AIDS knowledge, and a perceived vulnerability to AIDS. On the basis of A. Bandura's (1986) social-cognitive theory, a structural model with SE as the central mediator was formulated and evaluated with LISREL. This model explained 46% of the variance in condom use from judgments of SE and effects attributable to peers and 53% of the variance in SE from outcome expectancies and peer group influences. Sexual attitudes, AIDS knowledge, and perceived vulnerability did not predict condom use. Most students were well-informed about HIV transmission but reported not feeling at risk, even though many engaged in risky sexual behavior. (PsycINFO Database Record (c) 2010 APA, all rights reserved)