Mechanical alloying in the Al-Bi alloy system

Mechanical alloying (MA) was carried out to investigate the MA behaviour of the immiscible Al-10, 30 at % Bi alloys. After the MA processing, the Al and Bi were finely and homogeneously alloyed. The Bi crystallite size decreased to 25 nm and 30 nm in the Al-10 at % Bi and Al-30 at % Bi alloys, respectively. By increasing the MA time, the hardness increased up to a value of 80 H _v, which is larger than that obtained from the rule of mixtures. The lattice parameter of Bi decreased by about 0.27%, which shows the formation of a non-equilibrium hcp Bi super-saturated solid solution. The extended solubility of Al in Bi was 1.9% in the Al-30 at % Bi alloy. Due to the extended solubility, depression of the melting temperature of hcp Bi was confirmed in the mechanically alloyed Al-Bi alloys. The maximum depression in the temperature was about 10 K. The measured values corresponded well with those estimated from the extrapolation of the solidus line.     

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本文通过对在用钻机井架的现场实际测试,建立数据库、测评模型,对实测的数据用计算机技术进行分析,提出了初始弯曲应力;数据正态分布检验——x～2检验;建立回归方程;在给定置信度下测评当前承载能力的技术概念。解决了在用钻机A型井架的安全性评估问题,是一种较为合理、可靠、科学的测评技术和方法。     

Preparation of core–shell type nanoparticles of diblock copolymers of poly(L‐lactide)/poly(ethylene glycol) and their characterization in vitro

Core–shell type nanoparticles of poly(L ‐lactide)/poly(ethylene glycol) (LE) diblock copolymer were prepared by a dialysis technique. Their size was confirmed as 40–70 nm using photon correlation spectroscopy. The ¹H‐NMR analysis confirmed the formation of core–shell type nanoparticles and drug loading. The particle size, drug loading, and drug release rate of the LE nanoparticles were slightly changed by the initial solvents that were used. The drug release behavior of LE core–shell type nanoparticles showed an initial burst during the first 12 h and then a sustained release until 100 h. The degradation behavior of LE block copolymer nanoparticles was divided into three phases: the initial rapid degradation phase, the stationary phase, and the rapid degradation phase until complete degradation. It was suggested that lidocaine release kinetics were predominantly governed by the diffusion mechanism in the initial burst phase and after that by both of the diffusion and degradation mechanisms. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 2625–2634, 2002     

一种新型同位素示踪剂载体及应用

同位素沾污、低注井同位素示踪剂因沉降造成的上返速度慢或无法上返、大孔道地层同位素示踪剂失踪等是影响注水开发油田后期吸水剖面测井资料质量的主要问题。同位素示踪剂载体的物理参数，尤其是其密度，是产生上述问题的重要因素。通过对同位素示踪剂载体技术指标优选而生产的一种新型同位素示踪剂，可以解决低注井同位素上返速度慢的问题，并能有效识别大孔道地层，减少同位素沾污。这种同位素示踪剂载体已在河南油田吸水剖面测井中应用，并见到了很好的效果。     

三相四线统一电能质量调节器的控制策略

针对电网输入电压的不平衡、非正弦及负载的不平衡、非线性特性，提出了一种基于三相静止坐标系下的三相四线统一电能质量调节器（UPQC）的协调控制策略。该策略将UPQC的串联变流器控制为基波正弦电流源，而并联变流器控制为基波正弦电压源，从而实现了三相四线UPQC对电能质量的综合控制能力，既改善了电网侧的电能质量问题，实现了电网输入电流的正弦及单位输入功率因数，也改善了负载侧的电能质量问题，实现了负载电压的平衡、额定及正弦。10 kVA系统实验装置的实验结果表明了该控制策略的有效性。     

河流二维水质模型与地理信息系统的集成研究

根据水质预测、管理的不同需求,提出基于二维对流扩散方程的三种水质计算模式:连续点源排放水质模型,瞬时点源排放水质模型,有限体积法求解的数值解水质模型。基于MO进行GIS系统的组件式开发,实现了GIS平台下河势贴体河道二维正交网格的自动生成,解决了二维水体的空间网格离散问题。在此基础上,将三种类型的二维水质模型模块与GIS平台集成,以更好满足水质预测与管理在水质模型计算方式选取、计算精度与实现效率等方面的需求。     

某跨线桥施工支架方案设计

结合某大桥的概况,根据梁体施工工艺要求、现场实地勘察情况确定跨线施工方案,支架采用布架灵活、搭拆方便、承载力大的WDJ碗扣式多功能钢支架,部分预应力现浇连续箱梁采用支墩加纵梁预留门洞的支架现浇,取得良好效果。     

变异函数在进间砂体预测中的应用

应用变异函数探讨了砂体的定量预测问题。通过对北二东密井网试验区不同类型砂体，不同井网密和岩厚度的预测，检验了此方法的精度（为70％左右），在原方法的基础上，通过对预报精度的分析并结合精度地质研究进一步完善了该方法，提出二次建模法并应用于北二东西块聚驱井的砂岩厚度预测中，预测精度可提高5％以上，从而说明应用变异函数研究砂体的定量预测问题具有可借鉴性，可以为今后新井调整厚度的预测及砂体描述提供依据。     

用最优化方法和双水模型评价泥质砂岩储集层

本文从测井资料数字处理和解释的角度出发,在系统考察分析常用的各种最优化方法的基础上,认为采用抛物线插值法作一维搜索和变尺度法中的BFGS法作多维搜索相结合的最优化方法,用双水解释模型对泥质砂岩储集层进行评价是适宜的。为此编制了最优化测井解释程序,对胜利油田砂泥岩的测井资料进行了实际处理,并针对本地区的地质特点,对测井响应方程和解释参数的选择等重要问题进行了探讨。数字处理的结果表明,所获得的储集层参数和岩性矿物成分,与岩心分析资料和斯仑贝谢公司的GLOBAL程序处理结果相当吻合。证明它有较好的效果。     

分光光度法测定黄磷尾气中总磷

实验研究了溴化硝酸吸收－分光光度法测定黄磷尾气中总磷含量的方法，总磷回收≥97%,方法检测限可达0.2μg/mL.