A fully on-chip LDO voltage regulator with 37 dB PSRR at 1 MHz for remotely powered biomedical implants

This article presents a fully on-chip low-power LDO voltage regulator dedicated to remotely powered wireless cortical implants. This regulator is stable over the full range of alternating load current and provides fast load regulation achieved by applying a time-domain design methodology. Moreover, a new compensation technique is proposed and implemented to improve PSRR beyond the performance levels which can be obtained using the standard cascode compensation technique. Measurement results show that the regulator has a load regulation of 0.175 V/A, a line regulation of 0.024%, and a PSRR of 37 dB at 1 MHz power carrier frequency. The output of the regulator settles within 10-bit accuracy of the nominal voltage (1.8 V) within 1.6 μs, at full load transition. The total ground current including the bandgap reference circuit is 28 μA and the active chip area measures 290 μm × 360 μm in a 0.18 μm CMOS technology.     

Effects of core excess reactivity and coolant average temperature on maximum operable time of NIRR-1 miniature neutron source reactor

We appraised in this study the effects of core excess reactivity and average coolant temperature on the operable time of the Nigeria Research Reactor-1 (NIRR-1), which is a miniature neutron source reactor (MNSR). The duration of the reactor operating time and fluence depletion under different operation mode as well as change in core excess reactivity with temperature coefficient was investigated over a period of five years. Our result shows that there is a strong dependence of reactor operating time on core excess reactivity and temperature coefficient. It was observed in 2004 that with a cold core excess reactivity of 3.77 mk, at full-power flux of 1.0 × 10¹² n cm⁻² s⁻¹ the reactor operated for 5 continues hours. At half-power flux of 0.5 × 10¹² n cm⁻² s⁻¹ and under the same excess reactivity condition, the reactor reaches 8 h of operation. However, re-measurements done in 2009 shows that excess reactivity of the reactor has reduced to 2.80 mk, the operable time at full flux dropped to 3.5 h while that of half-power became 7 h. We also investigated the reactor's energy consumption within the period under study and found to be much more in 2008 compared to the previous years. We infer that the amount of fluence consumed and the excessive reactor usage in 2008 has contributed significantly to the reduction of the reactor's excess reactivity in that year. The results obtained here revels that for an MNSR with a clean core excess reactivity between 3.5 mk and 4.0 mk, 5 and 8 h are the maximum operable times under full and half-power flux conditions, respectively. Negative deviation from these optimum times is therefore an indication of a drop in excess reactivity and the need for beryllium shims addition.     

Preparation and textile application of poly(methyl methacrylate-co-methacrylic acid)/n-octadecane and n-eicosane microcapsules

In this study, a series of microencapsulated phase change materials with poly(methyl methacrylate-co-methacrylic acid) P(MMA-co-MAA) shell and n-octadecane or n-eicosane core were synthesized by emulsion polymerization method. The aim was to produce microencapsulated n-alkanes having functional groups on their outer surface, so that functional groups would help increasing physical interactions between microcapsules and fiber surface. Therefore, methyl methacrylate (MMA), ethylene glycoldimethacrylate (EGDM), and methacrylic acid (MAA) were copolymerized in oil phase of n-alkane. FT-IR results proved the successful synthesis of P(MMA-co-MAA) shell of microencapsulated n-alkanes. The DSC results indicated that the microencapsulated n-alkanes have considerable latent heat storage capacity in a range of 58–145 J/g. The average melting and freezing temperatures of the microencapsulated n-alkanes were measured as 27 and 26 °C for n-octadecane and 36 and 35 °C for n-eicosane, respectively. The microcapsules were of spherical and compact shape with particle sizes between 15 and 32 μm. The microcapsules on the cotton fabric applied by pad-dry-cure method were found highly durable and they showed sufficient stability upon several washings and rub fastness. Thermo-regulating properties of the fabrics were declared as a result of thermal history measurements.     

Feasibility study of utilization of commercially available polyurethane resins to develop non-biocidal wood preservation treatments

Evaluation of commercially available polyurethane resins used up to now for coating applications to develop non-biocidal wood preservation treatments has been conducted. A simple method of vacuum impregnation of these resins into beech wood (Fagus sylvatica L.) and pine wood (Pinus sylvestris L.) samples followed by varied curing processes at ambient temperature, 103, and 200 °C has been performed. Based on the analysis of weight percent gain before and after leaching, treatment resistance to leaching, anti-swelling efficiency, wettability and decay durability measured for treated and untreated blocks after leaching with the white-rot fungus Coriolus versicolor for both wood species and the brown-rot fungi Poria placenta and Gloeophyllum trabeum for pine wood, it can be concluded that such treatment can be considered as potential valuable non-biocidal treatments.     

Photoelectrocatalytic determination of NADH in a flow injection system with electropolymerized methylene blue

It was firstly described that a glassy carbon electrode electropolymerized with methylene blue shows an efficient photoelectrocatalytic activity towards NADH oxidation in a phosphate buffer solution (pH 7.0). In order to perform the photoelectrocatalytic determination of NADH in a flow injection analysis (FIA) system, a home-made flow electrochemical cell with a suitable transparent window for the irradiation of the electrode surface was constructed. The currents obtained from the photoamperometric measurements in the FIA system at optimum conditions (flow rate of carrier solution, 1.3 mL min⁻¹; transmission tubing length, 10 cm; injection volume, 100 μL; and constant applied potential, +150 mV vs. Ag/AgCl) were linearly dependent on the NADH concentration and linear calibration curves were obtained in the range of 1.0 × 10⁻⁷–2.0 × 10⁻⁴ M. The detection limit was found to be 4.0 × 10⁻⁸ M for photoamperometric determination of NADH.     

Synthesis,characterization, and properties of flexible magnetic nanocomposites of cobalt ferrite–polybenzoxazine–linear low‐density polyethylene

A simple method for the preparation of magnetic nanocomposites consisting of cobalt ferrite (CF; CoFe₂O₄) nanoparticles, polybenzoxazine (PB), linear low‐density polyethylene (LLDPE), and linear low‐density polyethylene‐g‐maleic anhydride (LgM) is described. The composites were prepared by the formation of benzoxazine (BA)–CF nanopowders followed by melt blending with LLDPE and the thermal curing of BA. The composites were characterized by X‐ray diffraction, thermogravimetric analysis, differential scanning calorimetry, scanning electron microscopy, universal testing machine measurement, and vibrating sample magnetometry. The composites consisting of LLDPE, PB, and LgM (47.5L–47.5PB–5LgM) exhibited a higher tensile strength (23.82 MPa) than pure LLDPE and a greater elongation at break (6.11%) than pure PB. The tensile strength of the composites decreased from 19.92 to 18.55 MPa with increasing CF loading (from 14.25 to 33.25 wt %). The saturation magnetization of the composites containing 33.25 wt % CF was 18.28 emu/g, and it decreased with decreasing amount of CF in the composite. The composite films exhibited mechanical flexibility and magnetic properties. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013     

Polyurethaneurea–silica nanocomposites: Preparation and investigation of the structure–property behavior

Nanocomposites consisting of thermoplastic polyurethane–urea (TPU) and silica nanoparticles of various size and filler loadings were prepared by solution blending and extensively characterized by Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), thermal analysis, tensile tests, and nanoindentation. TPU copolymer was based on a cycloaliphatic diisocyanate and poly(tetramethylene oxide) (PTMO-2000) soft segments and had urea hard segment content of 20% by weight. TPU/silica nanocomposites using silica particles of different size (29, 74 and 215 nm) and at different loadings (1, 5, 10, 20 and 40 wt. %) were prepared and characterized. Solution blending using isopropyl alcohol resulted in even distribution of silica nanoparticles in the polyurethane–urea matrix. FTIR spectroscopy indicated strong interactions between silica particles and polyether segments. Incorporation of silica nanoparticles of smaller size led to higher modulus and tensile strength of the nanocomposites, and elastomeric properties were retained. Increased filler content of up to about 20 wt. % resulted in materials with higher elastic moduli and tensile strength while the glass transition temperature remained the same. The fracture toughness increased relative to neat TPU regardless of the silica particle size. Improvements in tensile properties of the nanocomposites, particularly at intermediate silica loading levels and smaller particle size, are attributed to the interactions between the surface of silica nanoparticles and ether linkages of the polyether segments of the copolymers.     

The PANOPTIC Camera: A Plenoptic Sensor with Real-Time Omnidirectional Capability

A new biologically-inspired vision sensor made of one hundred “eyes” is presented, which is suitable for real-time acquisition and processing of 3-D image sequences. This device, named the Panoptic camera, consists of a layered arrangement of approximately 100 classical CMOS imagers, distributed over a hemisphere of 13 cm in diameter. The Panoptic camera is a polydioptric system where all imagers have their own vision of the world, each with a distinct focal point, which is a specific feature of the Panoptic system. This enables 3-D information recording such as omnidirectional stereoscopy or depth estimation, applying specific signal processing. The algorithms dictating the image reconstruction of an omnidirectional observer located at any point inside the hemisphere are presented. A hardware architecture which has the capability of handling these algorithms, and the flexibility to support additional image processing in real time, has been developed as a two-layer system based on FPGAs. The detail of the hardware architecture, its internal blocks, the mapping of the algorithms onto the latter elements, and the device calibration procedure are presented, along with imaging results.     

Acoustical absorptive properties of spunbonded nonwovens made from islands-in-the-sea bicomponent filaments

In this paper, we report on the acoustical absorptive behavior of spunbonded nonwovens that contain bicomponent islands-in-the-sea filaments. Nylon 6 (PA6) and polyethylene were used as the islands and the sea polymers, respectively. Spunbonded webs made with islands-in-the-sea bicomponent filaments with island counts of 1, 7, 19, 37, and 108 were produced at the Nonwovens Institute’s pilot facilities at NC State University. The filaments were fibrillated by hydroentangling, where high-speed water jets were used to fibrillate the fiber and ‘free’ the islands. The influence of the number of islands on acoustical absorptive behavior of the spunbonded nonwovens was investigated. A comparison of acoustical absorptive properties of multi-layer islands-in-the-sea nonwoven and high loft nonwoven was also performed to evaluate the potential use of spunbonded nonwovens made from islands-in-the-sea bicomponent filaments in place of bulky fibrous sound absorbers. Results have shown that multi-layer 108 nonwoven islands were better acoustic absorbers at nearly half of the frequency range. Spunbonded nonwovens made from islands-in-the-sea bicomponent filaments can be a good alternative in applications where there is desire to replace bulky fibrous sound absorbers.     

Effect of different denture adhesives on retention of complete dentures: an in vivo study

The increase in prevalence of tooth loss with the effect of population aging produces the growing need for complete dentures. The success and acceptance of complete dentures by the patient depends on sufficient retention and stability. Therefore, denture adhesives are regularly used by denture wearers to improve the function of complete denture. We evaluated the effect of three different denture adhesives (Corega, Protefix, Fittydent) on the retention of maxillary complete denture (MCD) using with digital dynamometer (DD). For this purpose, denture adhesives were applied on MCDs of 30 participants. After chewing procedure, the force was applied at 45° to the palatal surface of denture by DD. Dislodgement force was recorded by means of Newton. There were four measurements on each patient including; group of control: Group C; Group CR: Corega; Group F: Fittydent; Group P: Protefix. The result of the study was statistically evaluated by using analysis of variance (ANOVA) and Tukey HSD test. Statistics of ANOVA showed a significant difference among all the four groups (p = 0.00, <0.05). Tukey HSD test indicated that there was a statistical difference between Group F and the other groups, but there was not a significant difference between the other groups. The highest adhesive strength value was observed in group F, the lowest in group C. Use of denture adhesives improved the retentive strength of complete denture.