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231.
J. C. G. Calado J. M. N. A. Fareleira U. V. Mardolcar C. A. Nieto de Castro 《International Journal of Thermophysics》1988,9(3):351-363
The thermal conductivity of liquids has been shown in the past to be difficult to predict with a reasonable accuracy, due to the lack of accurate experimental data and reliable prediction schemes. However, data of a high accuracy, and covering wide density ranges, obtained recently in laboratories in Boulder, Lisbon, and London with the transient hot-wire technique, can be used to revise an existing correlation scheme and to develop a new universal predictive technique for the thermal conductivity of liquid normal alkanes. The proposed correlation scheme is constructed on a theoretically based treatment of the van der Waals model of a liquid, which permits the prediction of the density dependence and the thermal conductivity of liquid n-alkanes, methane to tridecane, for temperatures between 110 and 370 K and pressures up to 0.6 MPa, i.e., for 0.3T/T
c0.7 and 2.4P/P
c3.7, with an accuracy of ±1%, given a known value of the thermal conductivity of the fluid at the desired temperature. A generalization of the hard-core volumes obtained, as a function of the number of carbon atoms, showed that it was possible to predict the thermal conductivity of pentane to tetradecane±2%, without the necessity of available experimental measurements. 相似文献
232.
Jean-Marie Degroodt Brigitte Wyhowski de Bukanski Sarah Srebrnik 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1992,195(6):566-568
Summary A method combining immunoaffmity-chromatography (IAC) and high-performance liquid chromatography (HPLC) for the analysis of Salbutamol in liver with a low quantification limit of 1 g/kg has been developed. Salbutamol was extracted with 0.01 mol/L HCl and purified by IAC. The samples were analysed on a liquid Chromatograph fitted with a C18 -Bondapak column. A fluorometer was used for the detection of salbutamol. Recoveries of 67–80% could be obtained.
Immunoaffinitätschromatographische Reinigung von Salbutamol in Leber und Rückstandsbestimmung mittels HPLC und fluorimetrischer Detektion
Zusammenfassung Eine Methode, die Immunoaffinitäts-und Hochleistungsflüssigchromatographie verbindet, ist für die Analyse von Salbutamol in Leber entwickelt worden. Eine niedrige Bestimmungsgrenze von 1 g/kg Leber wurde erreicht. Salbutamol wurde mit 0,01 mol/L Salzsäure freigesetzt und durch Immunoaffinitätschromatographie gereinigt. Die Proben wurden durch Flüssigchromatographie auf einer C18 -Bondapak-Säule analysiert. Ein Fluorimeter wurde für die Detektion von Salbutamol benutzt. Ausbeuten von 67 bis 80% konnten erreicht werden.相似文献
233.
W. Montfrooij E. C. Svensson I. M. de Schepper 《Journal of Low Temperature Physics》1992,89(3-4):437-440
We correct for the effect of temperature induced frequency shifts on the observed dynamic structure factor S(q,) and find that the intrinsic behavior for non-superfluid4He is remarkably similar to that for other noble-gas fluids. 相似文献
234.
235.
236.
Pyros, which is a Ni-base alloy (82% Ni, 8% Cr, 4% W, 3% Mn, and 3% Fe), has been used extensively in France since 1926 as a temperature sensor and as a reference material for thermal expansion measurements. In this paper we present recent data on the expansion and expansivity of Pyros from 20 to 1273 K. Expansivity results, obtained by taking the derivative of a cubic-spline polynomial fitting performed to the L/L experimental data, show that Pyros is a stable material in the 20 to 1273 K temperature range. Furthermore, since the expansivity values are similar to those of steels, Pyros should be of special interest to laboratories which are concerned with expansion measurements on steels. Therefore, we suggest that Pyros be considered as a suitable reference material for thermal expansion measurements on steels, and until more accurate results are obtained, we propose our results as reference data between 20 and 1273 K.Paper presented at the Ninth Symposium on Thermophysical Properties, June 24–27, 1985, Boulder, Colorado, U.S.A. 相似文献
237.
Catalysis Letters - The NdM0.25Ni0.75O3 (M?=?Cr, Fe) named NCN and NFN catalysts precursors were synthesized and characterized. The CO2 utilization in the feed was studied in the... 相似文献
238.
239.
C. Okkerse A. de Jonge J. W. E. Coenen A. Rozendaal 《Journal of the American Oil Chemists' Society》1967,44(2):152-156
Many investigators associate the poor keeping properties of soybean oil with its linolenic acid content. On the other hand
the high linoleic acid content is a desired property from a nutritional point of view. We have therefore developed a process
for the preferential reduction of the linolenic acid content by selective hydrogenation. Conventional catalysts for the hydrogenation
of fats have a rather low selectivity in this respect. When linolenic acid in soybean oil is hardened (e.g., with a nickel
catalyst), most of the linoleic acid is converted into less unsaturated acids.
It was found that linolenic acid is hydrogenated much more preferentially in the presence of copper catalysts than in that
of nickel and other hydrogenation catalysts. At a linolenic acid content of 2%, soybean oil hardened with nickel catalyst
contained about 28% linoleic acid, whereas with copper catalyst the hardened soybean oil contained 49% linoleic acid.
By means of our process it is possible to manufacture a good keepable oil of, e.g., I.V. 115 and containing 1% linolenic acid
and 46% linoleic acid. The storage stability of this product is comparable with that of sunflower-seed oil. A liquid phase
yield of 86% is obtained after winterization at 5C for 18 hr.
The high selectivity for linolenate reduction of copper catalysts must be ascribed to the copper part of the catalyst. Investigations
into the structure of the catalyst indicate that the active center consists of copper metal crystallites; whether these centers
are promoted by the carrier or traces of other substances is under investigation. 相似文献
240.
M A Rossi S Zucoloto J E Dutra de Oliveira P F Becker J S Oliveira 《Archivos latinoamericanos de nutrición》1978,28(1):29-40
A study of the effect of long-term alcohol consumption on the liver of well-nourished rats is described. Rats fed for 16 weeks on a semipurified diet supplemented with high levels of vitamins and lipotropic factors and alcohol corresponding to 35% of the total caloric intake developed marked fatty changes of the liver. Mild fatty changes were observed in pair-fed controls receiving as isoenergetic equivalent of sucrose instead of alcohol. Intracellular hyaline bodies, corresponding ultrastructurally to giant mitochondria were abundantly found in the hepatocytes of alcoholic rats, while in the controls they were not seen. Te findings in this investigation are postulated to provide further evidence that the long-term intake of alcohol exerts a direct causative role in the pathogenesis of liver damage. 相似文献