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971.
The stability of the reactive interface during the solid-state displacement reaction, Cu2O+Co1−X
Fe
X
=2Cu+(Co1−X
Fe
X
)O, is studied as a function of Co-Fe alloy composition at 1223 K. For X≤0.03, the reaction zone has a layered structure, and the cation diffusion in (Co, Fe)O is the rate-limiting step. The interface
is unstable in the early stages of the reaction; the instability decreases with time as the oxide thickness increases, and
the interface becomes planar at long times. The time required for the attainment of interface planarity increases with the
value of X. The reaction kinetics are consistent with the available cation-diffusion data in (Co, Fe)O. For X≥0.045, the product zone is a composite of Cu+(Co, Fe)O, and the rate is limited by the oxygen transport in copper. The transition
to interface instability occurs when the oxide can support a cation flux that exceeds the maximum possible oxygen flux in
copper. During the reaction, composition gradients develop in (Co, Fe)O because of higher diffusion rates for iron than for
cobalt. 相似文献
972.
This report deals with direct observations of microcrack linkage at the crack tip prior to macroscopic crack initiation. It is shown that this process is directly linked to the inclusion distribution in the material and can be considered in terms of an R curve to describe microcrack development. 相似文献
973.
974.
Self-similarity in diffraction by a self-similar fractal screen 总被引:1,自引:0,他引:1
Lakhtakia A. Holter N. Varadan V. 《Antennas and Propagation, IEEE Transactions on》1987,35(2):236-239
Using the Sierpinski gasket as an example, it has been shown here that the paraxial Fraunhoffer-zone diffracted field of a self-similar fractal screen also exhibits self-similarity. This also establishes that fractal structures can be used with great profit in problems involving array syntheses. Recently, it has been shown that the Sierpinski gasket is itself a member of a much wider class of gaskets, and the potential for the use of fractal structures in electromagnetic (EM) problems may be vast indeed. 相似文献
975.
976.
977.
978.
The mean convergence of various versions of a genetic algorithm are considered. A number of convergence statements are formulated
and relevant estimates are obtained. A hypothesis concerning the form of these estimates under variation of the structure
of a genetic algorithm is put forward.
Roman Riviyanovich Sharapov. Born 1981. Graduated from the Faculty of Mechanics and Mathematics, Ural State University, in 2003. Presently, a postgraduate
at the Department of Mathematical Economics at the same university. Scientific interests: genetic algorithms, neural networks,
and financial mathematics.
Aleksandr Vyacheslavovich Lapshin. Born 1980. Graduated from the Faculty of Mechanics and Mathematics, Ural State University, in 2003. Presently, a postgraduate
at the Department of Mathematical Economics at the same university. Scientific interests: financial mathematics, genetic algorithms,
and neural networks. 相似文献
979.
Synthesis of 2-[18F]fluoro-2-deoxy-D-glucose ([18F]FDG) involving base hydrolysis was optimized. Fluorine-18 was isolated from irradiated water to more than 90% by sorption of [1
8F]fluoride on QMA anion-exchange resin, which was followed by elution with a 96 : 4 (by volume) acetonitrile-water mixture containing Kryptofix 2.2.2 and potassium carbonate (molar ratio 2 : 1). This composition is the best for preparing the complex [K/K2.2.2]+
18F- used in nucleophilic fluorinations. No additional azeotropic drying is required. Base hydrolysis under optimized conditions (40-45°C), followed by neutralization with HCl, removal of traces of the solvent, and purification of the final product on a combined SCX/Alumina N column, yielded [1
8F]FDG of high radiochemical (>99%) and chemical purity with minimal product loss. With an RB-86 robotic system (Anatech, Sweden), the synthesis time was 38 min. The procedure is used in the Institute of Human Brain, Russian Academy of Sciences for routine synthesis of FDG; the radiochemical yield of the product by the end of synthesis (EOS) is reproducibly high: 63±3% (n = 40). 相似文献
980.
D. C. Peets R. Liang C. Stock W. J. L. Buyers Z. Tun L. Taillefer R. J. Birgeneau D. A. Bonn W. N. Hardy 《Journal of Superconductivity and Novel Magnetism》2002,15(6):531-534
We have grown cubic centimeter-size crystals of YBa2Cu3O x suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2% Y2BaCuO5 and 0.5% Pt (by mass) were required to prevent melt loss and to obtain the highest crystallinity. A neutron diffraction study on a mosaic of six such crystals found that the final Y2BaCuO5 concentration was 5%, while other impurity phases comprised less than 1% by volume. The oxygen content was set to x = 6.5, the crystals were detwinned, and then carefully annealed to give the well-ordered ortho-II phase. The neutron study determined that 70% of the mosaic's volume was in the majority orthorhomic domain. The neutron (006) and (110) rocking curve widths were ~1° per crystal and ~2.2° for the mosaic, and the oxygen chain correlation lengths were >100 Å in the a- and b-directions and ~50 Å in the c-direction. 相似文献