3D reconstruction based on hard tissue microtome cross-section pictures in dentistry

The aim of this study was to examine the accuracy of the computerized 3D surface analyzing and volume measuring method in dentistry. Two different types of test objects were used in the first part of the measurements. Each sample of the two groups was cross-sectioned using a hard tissue microtome. The sections were photographed on both sides and were projected on a graphical tablet and analyzed using a computer program. The measured and calculated parameters were compared. In the second part, 200 microm thick horizontal sections were prepared from 11 human incisor roots using the hard tissue microtome. This way, five sections were prepared from the apical 2 mm of each root. The effects of section thickness and number were modeled by decreasing the inclusion rate of the obtained number of sections from 10 to 2 and its influence on the calculated results was determined. This method was suitable for the approximation and analysis of 3D parameters. The results indicated that using 200-300 microm section thickness, the measured values were approximately 8-21% lower than the real parameters.     

Richard Bright in Hungary: a reevaluation

Richard Bright, the highly respected physician and nephrologist at Guy's Hospital, had a strong liking for travel. In 1815 he traveled in Hungary and made very important observations about the country. His 762-page book, entitled Travels from Vienna through Lower Hungary has detailed, sometimes appreciative, sometimes very critical remarks and comments on Hungarian history, art, archeology, religion, the situation of nationalities, education, social conditions, law, farming, and mining. The Hungarians cherished the memory of Bright's travel in their country as reflected in several papers and on two commemorative tablets recognizing him as a true and sincere friend of Hungary.     

Buckling analysis with the aska program system

The theoretical and practical considerations involved in extending the very large, general purpose finite element program system ASKA to include linear buckling mode analysis are presented. The main analysis features and their software implementation are discussed in the context of modular processors and data operands. A broader interpretation of buckling load factors and modes in relation to mode superposition is given, and typical applications are presented to illustrate both classical bifurcation buckling analyses and buckling mode superposition response.     

The mechanism of the adsorption of alkyl xanthate species on galena

Oxidation of galena produced thiosulphate and sulphate ions at the mineral surface but flotation activity, using isopropyl xanthate as collector, was found to depend on the concentration of thiosulphate ions at the surface. It is proposed that the thiosulphate ion reacts with di-isopropyl dixanthogen formed by oxidation of xanthate ion in solution. It was demonstrated that these species react in homogeneous solution to give xanthate and xanthogen-thiosulphate ions. The proposed surface reaction may account for the formation of a layer of adsorbed xanthate ions and for the surface redox potential being raised to a value where more xanthate ions can be chemisorbed and where dixanthogen is stable.     

On the growth mechanism of single-walled carbon nanotubes by catalytic carbon vapor deposition on supported metal catalysts

A comprehensive kinetic study was performed to throw light on the formation mechanism of single walled carbon nanotubes (SWNTs) in chemical vapor deposition processes. SWNTs were synthesized by catalytic decomposition of methane or ethylene on supported transition metal catalysts. Kinetic curves (the amount of SWNT as a function of time) were obtained as a function of the nature and the preparation of the supported catalysts, temperature, the fluxes of the gases (the reagent hydrocarbon and the carrying gas), and the partial pressure of the hydrocarbon. The final products were characterized by transmission electron microscopy, Raman spectroscopy, chemical analysis, and thermogravimetric measurements. The fundamental factors determining the SWNT formation are discussed in detail, taking into consideration several observations from the literature as well.     

Hydrocarbon decomposition in alumina membrane: an effective way to produce carbon nanotubes bundles

Carbon nanotubes were synthesised within the pores of an alumina membrane. The membrane had 200 nm diameter pores and 60 microm thickness, and ethylene was used as carbon source. Membrane dissolution by HF results in a bundle of parallel open tubes, aligned without macroscopic defects. The external diameter of the tubes is uniform and there is no evidence of any amorphous carbon. Wall thickness control was obtained by varying the reaction time, length by the thickness of alumina membrane, and external tube diameter by the membrane pore size. Scanning (SEM) and transmission (TEM) electron microscopy, atomic force microscopy (AFM), X-ray diffraction, thermogravimetric analysis (TG) and surface area evaluation by nitrogen adsorption were used for the characterization of membrane and nanotubes.     

Device for the reversed-phase separation and on-target deposition of peptides incorporating a hydrophobic sample barrier for matrix-assisted laser desorption/ionization mass spectrometry

The separation of peptide mixtures from proteolytic cleavage is often necessary prior to mass spectrometry (MS) to enhance sensitivity and peptide mapping coverage. When buffers, salts, and other higher abundance peptides/contaminants are present, competition for charge during the electrospray ionization and matrix-assisted laser desorption/ionization (MALDI) processes can lead to ion suppression for the targeted analyte(s). In this note, a simple reversed-phase microcolumn sample separation and deposition device (Sep-Dep) is described. The use of this device improves or renders possible the analysis of complex or contaminated peptide mixtures by MALDI-MS. The method is simple and inexpensive and utilizes single-use low-cost Geloader-type columns packed with reversed-phase material. The device described utilizes an open column, allowing for a gradient or narrow-step gradient to be applied by any solvent delivery system or manually with a pipet. A key feature of the device is a deposition chamber that can be custom-built to hold any MALDI target. The Sep-Dep device is attached directly to an in-house vacuum line and draws solvent from the open-ended LC column. The elution of separated peptides is performed directly onto a target that has been treated with a hydrophobic barrier. This barrier effectively isolates fractions and improves the quality and morphology of the matrix crystals. The method produces efficient separations of proteolytic peptides, significantly reducing signal suppression effects in MALDI.     

Mechanisms of heat transfer between a surface and a gas-fluidized bed for combustor application

There is currently considerable interest in the development of fluidized-bed boilers for efficient and environmentally clean combustion of coal. Fluidized beds have the advantages of high heat transfer rates and intimate mixing of additives such as limestone or dolomite for sulfur dioxide absorption produced as a result of combustion of coal containing sulfur. However, design for optimum heat transfer remains uncertain and essentially empirical. The mechanisms of heat transfer are complicated because of the many variables in a commercial combustion operation such as particle size distribution, particle shape, particle and gas thermal properties, reactor geometry and boiler tube design.An understanding of the mechanisms of bed to tube heat transfer is essential to sound design and interpretation of empirically derived correlations. Here we will review and criticize the major mechanisms of heat transfer that have been proposed. These mechanisms are proposed and developed from two schools of thought: (a) The principal resistance to heat transfer is a fluid film, and the moving fluidized particles scour the film to reduce the resistance to heat transfer; (b) Heat is absorbed by the fluidized particles and the rate of heat transfer depends on the rate of heat absorption.Radiant heat transfer is also discussed in this review in detail. Heat transfer by radiation is an important consideration in combustors but has received limited attention. The results of theoretical calculations are given which have been recently reported on the basis of the alternate-slab model of Gabor.The review will predominantly deal with the mechanistic models of heat transfer and various correlations developed over years will not be covered as this topic is dealt with in another review article by Saxena, Grewal, Gabor, Zabrodsky and Galershtein.