Hydrothermal Reaction Mechanism and Pathway for the Formation of K2Ti6O13 Nanowires

Calculations and detailed first principle and thermodynamic analyses have been performed to understand the formation mechanism of K₂Ti₆O₁₃ nanowires (NWs) by a hydrothermal reaction between bulk Na₂Ti₃O₇ crystals and a KOH solution. It is found that direct ion exchange between K⁺ and Na⁺ plus H⁺ interactions with [TiO₆] octahedra in Na₂Ti₃O₇ promote the formation of an intermediate H₂K₂Ti₆O₁₄ phase. The large lattice mismatch between this intermediate phase and the bulk Na₂Ti₃O₇ structure, and the large energy reduction associated with the formation of this intermediate phase, drive the splitting of the bulk crystal into H₂K₂Ti₆O₁₄ NWs. However, these NWs are not stable because of large [TiO₆] octahedra distortion and are subject to a dehydration process, which results in uniform K₂Ti₆O₁₃ NWs with narrowly distributed diameters of around 10 nm.     

A Study on NMR and GC/MS Spectra of the Isomers of Linear Hexyl Naphthalene

The GC/MS and NMR analysis of the reaction products of naphthalene with 1-bromohexane were reported. The products obtained were suggested to have six isomers of linear hexylnaphthalene and the structure of each isomer was determined by GC/MS and NMR spectra. For the first time, the unique chemical shift data were obtained. The content of each isomer calculated by ¹H NMR and ¹³C NMR spectra was consistent with that by GC/MS spectra, which confirmed the accuracy of NMR data.     

工程造价管理经验在房地产中的应用

随着近几年我国房地产事业蓬勃发展，因此研究和探讨工程概预算的技术数据是项目管理工作中的重要信息，也是房地产加强工程造价有效控制的重要途径，本文结合工作实际，就如何积累工程造价经验数据，谈一点个人的体会。     

Fault-aware Communication Mapping for NoCs with Guaranteed Latency

As feature sizes shrink, transient failures of on-chip network links become a critical problem. At the same time, many applications require guarantees on both message arrival probability and response time. We address the problem of transient link failures by means of temporally and spatially redundant transmission of messages, such that designer-imposed message arrival probabilities are guaranteed. Response time minimisation is achieved by a heuristic that statically assigns multiple copies of each message to network links, intelligently combining temporal and spatial redundancy. Concerns regarding energy consumption are addressed in two ways. First, we reduce the total amount of transmitted messages, and, second, we minimise the application response time such that the resulted time slack can be exploited for energy savings through voltage reduction. The advantages of the proposed approach are guaranteed message arrival probability and guaranteed worst case application response time.     

EPP在便携式数据采集系统中的应用

分析了并口处于EPP(增强型并行端口)模式时和单片机进行数据交换的原理.介绍了有关EPP的基本特性、信号定义、操作模式及其程序设计方法,设计了基于EPP协议的便携式数据采集系统,给出了技术解决方案,讨论了系统的硬件接口电路和软件编程.方案具有可靠性高、速度快、软硬件设计简捷等优点.     

（E）-2-壬烯酸合成方法的改进

(E)-2-壬烯酸是有机合成的一种重要中间体,我们利用Knoevenagel反应机理,改进了(E)-2-壬烯酸的合成工艺,在不使用脱水剂条件下,使用少量吡啶作催化剂,获得了83%的反应收率。     

近年新疆能源工业回顾与展望

新疆是我国的能源资源富集区，“九大煤田”、“十八条大河”、“三大油田”、“九大风区”资源储量丰富，品质优良，是新疆的优势资源之一，不但为新疆的开发建设提供了雄厚的物质基础，同时也将是我国重要的能源开发接替地。     

基于SPA的模式识别

发展和深化了集对分析（SPA）基础理论，并在此基础上探讨了基于集对分析的模式识别方法，给出了集对模式识别的三个判定原则，这对SPA的发展及其在模式识别中的应用提供了理论支持。     

四川马海毛钢花呢的试制

根据四川马海毛原料资源的品质特性，运用精纺粗做的方法，成功地试制出手感滑糯而富有弹性、光泽明亮悦目，各项物理指标符合FZ/T24002-93标准的四川马海毛纯毛钢花呢，达到了马海毛产品的特殊风格。同时指出四川马海毛制成率偏低。     

矿石中金的快速测定

研究了活性炭纤维滤布富集分离的条件和解脱方法,并利用微波溶样、液珠萃取比色法测定矿石中的金。该方法的测定范围为(0.5~xx)×10-6,相对标准偏差RSD为3.2%,可用于矿石中金的野外快速测定。