NANO-MULTILAYERS WITH HIGH PERPENDICULAR ANISOTROPY FOR MAGNETIC RECORDING

(FePt/Ag)n nano-multilayers were deposited on MgO (100) single crystal with laser ablation and then subjected to annealing. FePt L1o grains with (001) texture and thus a large perpendicular magnetic anisotropy constant Ku of the order of 106 J/m3 were formed. A thick Ag layer is found to be favorable for decreasing the dispersion of the easy axis for magnetization. The measurement of time decay of magnetization gave rise to a small activation volume of the order of 10-25m3, showing the promising of being the recording medium for future high density perpendicular recording.     

铝合金复合铸造技术装备及其柔性化生产

1 概述铝合金复合铸造生产线主要由高压釜浇注罐系统、低压铸造系统(含保温炉)、真空系统、增压系统、铝镁合金熔化和保温系统(含铝锭预热及加料装置)、及其附属装置(铝镁合金液测氢仪和旋转除气装置及多点测温仪)等六大部分所组成。该生产线不仅可以     

压痕法测定热压MoSi2基复合材料K1C值的研究

用不同的压痕方程计算了纳米ＺｒＯ２粒子韧化ＭｏＳｉ２基复合材料的室温断裂韧性Ｋ１ｃ值，同时研究了压痕载荷对Ｋ１ｃ值的影响。结果表明，试验材料在试验条件下的断裂韧性不遵从半月状裂纹系统方程，而遵从巴氏裂纹系统方程，其室温压痕断裂韧性保持与压痕载荷的独立性。     

SiCp/Cu包覆粉体及其热沉材料的制备

采用化学镀铜工艺制备了Cu包覆SiCp复合粉体,并对复合粉体的组成和形貌进行了分析.同时,利用制得的复合粉体,结合适当的热压烧结工艺制备了Cu-35SiCp热沉材料,并对热沉材料的微观组织和热物理性能进行了研究.结果表明,SiCp颗粒在热沉材料的基体中均匀分布,界面结合良好.在试验条件下,Cu-35SiCp热沉材料的导热系数为165.7 W/(m·K),30～200 ℃温度区间内的热膨胀系数为15.1×10-6/K.     

NUMERICAL SIMULATION OF ALTERNATIVE HORIZONTAL LEVITATION ELECTROMAGNETIC CONTINUOUS CASTING（Ⅱ）

ＮＵＭＥＲＩＣＡＬＳＩＭＵＬＡＴＩＯＮＯＦＡＬＴＥＲＮＡＴＩＶＥＨＯＲＩＺＯＮＴＡＬＬＥＶＩＴＡＴＩＯＮＥＬＥＣＴＲＯＭＡＧＮＥＴＩＣＣＯＮＴＩＮＵＯＵＳＣＡＳＴＩＮＧ（Ⅱ）￥ＺｈｕＳｈｏｕｊｕｎ；ＲｅｎＺｈｏｎｇｍｉｎｇ；ＤｅｎｇＫａｎｇ；Ｊｉａｎ...     

Al-18%Si合金在梯度强磁场中凝固时初生硅的行为

研究了Al-18%Si合金在10 T梯度强磁场下加热至半固态和全熔态后的凝固过程,观察了初生硅的分布和形态,测定了其冷却曲线.结果表明:在磁场的磁感应强度和磁场梯度的乘积Bz·dBz/dz为正时,初生硅向上部聚集;而在Bz·dBz/dz为负时,初生硅向下部聚集;在强磁场下,加热至全熔态冷却下来的凝固组织中初晶硅的形态发生了明显的改变,由板片状转变为块状,初晶硅显著细化.对强磁场细化初晶硅的机制进行了探讨.     

喷雾干燥器粘壁产生的原因

引言众所周知,喷雾干燥工艺及设备是陶瓷、保护渣、化工、高岭土等行业常用的泥浆干燥设备。不管是哪个行业都或多或少存在喷雾塔体粘壁问题。此问题看似小问题,其实对使用厂会造成诸多不便,同时也造成了能源的浪费,尤其是粘性较大的泥浆原料,此问题尤为突出。     

SERCOS Ⅱ在注塑机全电动设计中的应用

针对传统注塑机在加工精度、加工效率上的不足，提出一种全电子注塑机的控制方案，介绍了基于SERCOSⅡ实时系统的运动控制方法，分析了实现注塑过程的高速高精度的硬件体系。在试验样机3个月的连续工作中，当周期循环时间为4ms，注射量最大达到80cm^3时，产品的成型周期能够控制在15s以内，注出产品的质量、精度均满足要求，表明该设计切实可行。     

Studies on crystallization behaviors and crystal morphology of polyamide 66/clay nanocomposites

X‐ray diffraction methods, DSC thermal analysis, and polarized light microscopy (PLM) were used to investigate the structural changes of nylon 66/clay nanocomposites. PA 66/clay nanocomposites were prepared by the method of melt intercalation. The results indicate that the addition of the intercalated organo‐montmorillonite (OMMT) can induce generation of the β‐form crystal of PA 66 and substantially affect the arrangement of molecules in the α‐form crystal, although the crystallinity scarcely changes. Also, the DSC results indicate that the addition of OMMT in the PA 66 matrix leads to increases of crystallization temperatures and the full width at half maximum (FWHM) of the exothermic peaks. Moreover, the viscosity factor is the main influence on FWHM of the exothermic peaks of PA 66/clay nanocomposites. The results of nonisothermal crystallization kinetics show that OMMT has the effect of heterogeneous nucleation and leads to the decrease of the size of the spherocrystal. The heterogeneous nucleation effects of OMMTs influence the mechanism of crystallization and the growth mode of PA 66 crystals. PLM photographs verify that the size of spherocrystal is decreased and visually confirm the theory of crystallization kinetics. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 95: 756–763, 2005     

Curing behavior and structure of an epoxy/clay nanocomposite system

The curing behavior of an epoxy/clay nanocomposite system composed of a bifunctional epoxy resin with an aromatic amine curing agent and an organically modified clay was investigated. Differential scanning calorimetry (DSC) was used to investigate the curing behavior of the epoxy/clay nanocomposite system. The curing rate of the nanocomposite system increased with increasing clay content. A kinetic equation, considering an autocatalytic reaction mechanism, could describe fairly well the curing behavior of the epoxy/clay nanocomposite system. The reaction kinetic parameters of the kinetic equation were determined by fitting DSC conversion data to the kinetic equation, using a nonlinear numerical method. Dynamic mechanical analysis was used to investigate the thermomechanical properties of the epoxy/clay nanocomposite system. The glass transition temperature of the epoxy/clay nanocomposite system increased slightly with increasing clay content. The structure of the nanocomposite system was characterized by X‐ray diffraction analysis and transmission electron microscope imaging. The formation of intercalated structures was observed dominantly in the epoxy/clay nanocomposites, together with some exfoliated structures. POLYM. ENG. SCI., 46:1318–1325, 2006. © 2006 Society of Plastics Engineers