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991.
La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La3+ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La3+ content, the site of dopant ion varies, the grain growth of Bi5TiNbWO15 is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process. 相似文献
992.
Wenwei He Wuping Liao Weiwei Wang Deqian Li Chunji Niu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(9):1314-1320
BACKGROUND: Thermodynamics and kinetics data are both important to explain the extraction property. In order to develop a novel separation technology superior to current extraction systems, many promising extractants have been developed including calixarene carboxylic acids. The extraction thermodynamics behavior of calix[4]arene carboxylic acids has been reported extensively. In this study, the mass transfer kinetics of neodymium(III) and the interfacial behavior of calix[4]arene carboxylic acid were investigated. RESULTS: The rate constant (Kao) becomes constant when the stirring speed was controlled between 250 rpm and 400 rpm. The activation energy (Ea) was calculated to be 21·41 kJ mol?1 or 88·17 kJ mol?1 (dependent on temperature) from the slope of log Kao against 1000/T. The linear relationship between the specific area and the extraction rate is the characteristic of an interfacial reaction control. The minimum bulk concentration of the extractant necessary to saturate the interface (Cmin) is lower than 4·19 × 10?4 mol L?1. CONCLUSION: The effect of stirring speed, temperature, and species concentration on the extraction rate demonstrates that the extraction regime depends on the extraction conditions. The chemical reaction control governs the extraction regime at temperatures below 303 K and a mixed control regime occurs when the temperature is between 303 K and 318 K. The probable locale for the chemical reaction is at the liquid–liquid interface and the rate equation is deduced to be: ? d[Nd3+](a)/dt = kf[Nd3+](a)[H4A](o)0·727[H+](a)?0·978. The rate‐controlling step was suggested by the analysis of the experimental results. Copyright © 2008 Society of Chemical Industry 相似文献
993.
994.
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996.
Collection and evaluation of existing data: an ecological risk assessment perspective. 总被引:1,自引:0,他引:1
James T Markwiese 《Quality Assurance: Good Practice, Regulation, and Law》2003,10(3-4):107-116
All scientific disciplines rely to some degree upon existing data to design new studies, test hypotheses, and make decisions. Because existing data can take many forms, a framework for addressing the quality of these data must be general and comprehensive. By nature of this inclusiveness, quality categories for existing data are necessarily broad. Effective employment of existing data requires the development of specific acceptance criteria from broad data quality categories. A framework is presented for collecting and evaluating existing data with examples of Environmental Protection Agency projects employing a tiered data review. The systematic planning inherent in a tiered review is described and attendant data quality considerations are developed in the context of an ecological risk assessment; specifically, the process is illustrated by defining an ecologically protective concentration of a chemical in soil. 相似文献
997.
A. D. Bulanov P. G. Sennikov V. A. Krylov T. G. Sorochkina L. A. Chuprov O. Yu. Chernova O. Yu. Troshin 《Inorganic Materials》2007,43(4):364-368
Using gas chromatography and high-resolution Fourier-transform IR spectroscopy, we have determined the concentrations of C1–C4 hydrocarbon impurities in isotopically unmodified silicon tetrafluoride before and after fine purification and in 28Si-enriched SiF4. The concentrations of C1–C4 hydrocarbon impurities in silicon tetrafluoride for SiH4 synthesis have been shown to correlate with those in the synthesized silane. 相似文献
998.
The authors present a theory for understanding risk for problem drinking among reservation-dwelling American Indians. The theory offers an overall framework for understanding the risk process for this group. It considers the distinction between factors that influence mean levels of American Indian problem drinking and factors that influence individual differences in American Indian drinking. It proposes important contextual differences between reservation-dwelling American Indians and Caucasians that may help explain the higher mean levels of American Indian problem drinking. The theory further holds that, within the high mean level of problem drinking characteristic of many American Indian reservations, individual differences in problem drinking can be explained by very similar personality and learning factors as those that influence problem-drinking levels for other ethnic groups. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
999.
M.-F. Foulon T. Crepin X. Melique D. Lippens 《Microwaves, Antennas & Propagation, IET》2007,1(1):23-28
Co-planar strip (CPS) transmission lines, aimed at operating up to sub-millimetre wavelengths, were periodically loaded by lumped capacitances and inductances in series and shunt configuration, respectively. Under this condition, propagation on the line is backward with group and phase velocities of opposite signs. The transmission lines were fabricated onto a quartz substrate by e-beam patterning and thin film deposition, silicon nitride and gold layers, on a deep sub-micron scale (~200 nm). A direct evidence of left-handedness between 160 and 380 GHz was achieved via the tracking of phase advance in a differential phase experiment using electro-optic sampling. The comparison between modelling results by electromagnetic full wave circuit analysis and experiment was performed in the time and frequency domains. It shows a good agreement in the dispersion characteristics and ultra-fast variations in the transmitted signals. At last, we took benefit of a lumped element fitting approach in order to discuss of the frequency capability of this non-resonant approach 相似文献
1000.
In wintertime, the use of studded tyres is common in the Nordic countries, steeply in creasing road wear. Apart from reducing surface quality and durability, the airborne dust presents a potential health hazard. To reduce road wear and dust release, there is a tendency to use harder and more wear-resistant aggregate materials.On the roads in and around Trondheim, mid-Norway, three types of aggregate material are common: greenstone, jasper and ‘mylonite’, in fact a cataclasite. Extensive laboratory testing suggests that cataclasite aggregate has better wear resistance than greenstone, but less than jasper [Erichsen E, Schiellerup H, Gautneb, H, Ottesen RT, Broekmans M. Road dust in Trondheim — analysis of the mineral content of airborne dust. (In Norwegian.) Geological Survey of Norway, NGU-report 2004. 037; 2004. p. 73]. However , observations on fluorescence-impregnated plane and thin sections demonstrate that in practice, cataclasite wears faster than greenstone, which may be attributed to its oriented fabric, as opposed to the random fabric in greenstone and jasper. The original article by Rosiwal from 1896 [Rosiwal A. Neue Untersuchungser gebnisse über die Härte von Mineralien und Gesteine. Verhandlungen der kaiserlich-königlichen geologischen Reichsanstalt, vol. 17/18; 1896. p. 475–491] on abrasion hardness and anisotropy provides an elegant explanation for the field observations. 相似文献