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We examined methodological and theoretical issues related to accuracy measures used as criteria in performance-rating research. First, we argued that existing operational definitions of accuracy are not all based on a common accuracy definition; we report data that show generally weak relations among different accuracy operational definitions. Second, different methods of true score development are also examined, and both methodological and theoretical limitations are explored. Given the difficulty of obtaining true scores, criteria are discussed for examining the suitability of expert ratings as surrogate true score measures. Last, the usefulness of using accuracy measures in performance-rating research is examined to highlight situations in which accuracy measures might be desirable criterion measures in rating research. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
424.
Lorne S. Reid 《Journal of research of the National Institute of Standards and Technology》1989,94(1):65-78
The procedures used to model a protein structure are well established when the novel protein has high sequence similarity to a protein of known structure. Many proteins of interest have low (i.e. <50%) sequence similarity to any known structure. In these cases new approaches to prediction of structure are required.The use of sequence profiles which relate sequence to known structure has been proposed as one method to assign local regions of structure. As a first stage, templates or “icons” of the many relevant substructural motifs found in proteins must be defined. The sequences which gave rise to these structures are then aligned and a weighted profile obtained.Average structures of the 8 and 12 residue helix-turn and turn-helix motifs have been prepared. These coordinate templates were then used to scan through the Brookhaven protein structural database for similar, superimposable fragments. A composite template of 100 similar fragments for each element was found to be internally consistent to a rmsd=0.92 Å for HT8, 1.54 Å for HT12, 0.41 Å for TH8 and 1.40 Å for TH12. All of the sequences, from these structures, were then used to create an overall sequence profile.The four sequence profiles were scanned against the amino acid sequences of the proteins in the Brookhaven database: tertiary structure was correctly identified only about 10% of the time. This value is too low for predictive purposes. However, it could be increased by checking for multiple occurrences of the template in one protein. 相似文献
425.
Harini Gunda Keith G. Ray Leonard E. Klebanoff Chaochao Dun Maxwell A. T. Marple Sichi Li Peter Sharma Raymond W. Friddle Joshua D. Sugar Jonathan L. Snider Robert D. Horton Brendan C. Davis Jeffery M. Chames Yi-Sheng Liu Jinghua Guo Harris E. Mason Jeffrey J. Urban Brandon C. Wood Mark D. Allendorf Kabeer Jasuja Vitalie Stavila 《Small (Weinheim an der Bergstrasse, Germany)》2023,19(6):2205487
Metal boride nanostructures have shown significant promise for hydrogen storage applications. However, the synthesis of nanoscale metal boride particles is challenging because of their high surface energy, strong inter- and intraplanar bonding, and difficult-to-control surface termination. Here, it is demonstrated that mechanochemical exfoliation of magnesium diboride in zirconia produces 3–4 nm ultrathin MgB2 nanosheets (multilayers) in high yield. High-pressure hydrogenation of these multilayers at 70 MPa and 330 °C followed by dehydrogenation at 390 °C reveals a hydrogen capacity of 5.1 wt%, which is ≈50 times larger than the capacity of bulk MgB2 under the same conditions. This enhancement is attributed to the creation of defective sites by ball-milling and incomplete Mg surface coverage in MgB2 multilayers, which disrupts the stable boron–boron ring structure. The density functional theory calculations indicate that the balance of Mg on the MgB2 nanosheet surface changes as the material hydrogenates, as it is energetically favorable to trade a small number of Mg vacancies in Mg(BH4)2 for greater Mg coverage on the MgB2 surface. The exfoliation and creation of ultrathin layers is a promising new direction for 2D metal boride/borohydride research with the potential to achieve high-capacity reversible hydrogen storage at more moderate pressures and temperatures. 相似文献