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71.
Martin E. Valdez H. Shibata Alan W. Cramb 《Metallurgical and Materials Transactions B》2006,37(6):959-965
The objective of this study is to determine the conditions under which the inclusions present in liquid steel can act as heterogeneous
nucleants for solidification. In order to study the factors that define the undercooling of a given metal/oxide couple, the
undercooling of a pure iron sessile droplet in contact with Al2O3, ZrO2, and MgO substrates was measured under controlled oxygen partial pressures by observing droplet recalescence. The results
showed that the undercooling of iron, in contact with a particular substrate, did not have a unique value, but was significantly
affected by the oxygen content on the gas phase. For oxygen partial pressures between 10−21 and 10−19, the undercooling of iron on ZrO2 substrates was stable and around 290 °C. In the same range of oxygen partial pressure, the undercooling of iron on MgO substrates
remained below 100 °C due to the low stability of this oxide. At lower oxygen contents, substrate decomposition might be the
cause for the observed drop in the undercooling of iron on ZrO2 substrates to below 100 °C. The undercooling also decreased for increasing oxygen content as verified when the gas was changed
from gettered Ar/Ar-H2 to CO/CO2 mixtures. The variation in undercooling was related to the wetting of the substrate by the liquid metal, where the deep undercooling
observed in the ZrO2 experiments occurred when the highest contact angle between the liquid metal and the substrate was achieved. 相似文献
72.
Xiaoming Zhou Martin Jacobsson Henk Uijterwaal Piet Van Mieghem 《International Journal of Communication Systems》2008,21(6):643-663
Although packet delay and loss are two important parameters of the Internet performance, to the best of our knowledge, the evolution of large‐scale IPv6 delay and loss performance has previously not been studied. In this paper, we analyze more than 600 end‐to‐end IPv6 paths between about 26 testboxes of RIPE Network Coordination Centre over two years, and compare the delay and loss performance over time with their IPv4 counterparts. We present and discuss the measurement methodologies and show that IPv6 paths have a higher delay and loss than their IPv4 counterparts. The main reason for the worse performance stems from IPv6‐in‐IPv4 tunnels rather than from native IPv6 paths and such tunnels are still widely used today. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献
73.
Maisto Stephen A.; Chung Tammy A.; Cornelius Jack R.; Martin Christopher S. 《Canadian Metallurgical Quarterly》2003,17(2):98
This study investigated the Stages of Change Readiness and Treatment Eagerness Scale (SOCRATES: W. R. Miller & J. S. Tonigan, 1996) in adolescents presenting for treatment of alcohol use disorder (AUD). The participants were 80 males and 43 females (mean age=16.8 years) who presented for AUD treatment (95.1% outpatient, 4.9% inpatient). Participants completed assessments at baseline and 1 year and provided information on alcohol use and related variables monthly between these 2 assessments. Principal-components and confirmatory factor analyses of the baseline SOCRATES identified 2 factors, Taking Steps and Recognition, which showed good internal consistency and concurrent and predictive evidence of validity. The results were interpreted as supporting the use of the SOCRATES with clinical samples of adolescents. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
74.
Martin Meyer 《Scientometrics》2007,70(3):779-810
This contribution formulates a number of propositions about the emergence of novel nanoscience and nanotechnology (N&N). Seeking
to complement recent work that aims to define a research agenda and draws on general insights from the innovation literature,
this paper aims to synthesize knowledge from innovation-related studies of the N&N field. More specifically, it is suggested
that N&N is often misconstrued as either a field of technology or an area of (broadly) converging technologies while evidence
to date suggests rather that N&N be considered a set of inter-related and overlapping about not necessarily merging technologies.
The role of instrumentation in connecting the various N&N fields is underlined. Finally, the question is raised whether change
in N&N tends to be incremental rather than discontinuous, being the result of technological path-dependencies and lock-ins
in industry-typical search regimes that are only slowly giving way to more boundary-crossing activities. 相似文献
75.
Karin Bucher Jens Mende Michael Mehring Martin Jansen 《Fullerenes, Nanotubes and Carbon Nanostructures》2007,15(1):29-42
A new Eu-endohedral fullerene cage, namely, Eu@C72, was synthesized, separated, and a single isomer, Eu@C72-I, has been isolated by multi-step HPLC for the first time and characterized by LDI-TOF mass spectrometry, UV-Vis and EPR spectroscopy. Additionally, a second isomer, Eu@C72-II, has been separated by HPLC and identified by LDI-TOF mass spectrometry. 相似文献
76.
The deformation characteristics of artificially cemented calcareous soil subjected to undrained cyclic triaxial loading are investigated at different confining pressure and cyclic stress levels. The influence of cementation on the shear stiffness is investigated by comparing the behavior of cemented and uncemented soils with similar initial conditions. It is observed that the deviator stress and the deviatoric strain at yield reduced with increasing number of cycles for cemented sand due to progressive degradation of bond, which results in significant decrease in stiffness. On the other hand, a strain-hardening effect is observed in uncemented sand and this results in increasing yield stress and strain with progressive number of cycles. A linear relationship between degradation index and number of cycles is observed for cemented sand. This relationship has been synthesized in the form of an empirical equation by modifying a previously proposed equation for cohesive soils. This empirical equation was further used to evaluate the fatigue life of soils by adopting a failure criterion. 相似文献
77.
G. G. Martin 《Journal of Failure Analysis and Prevention》2004,4(1):37-39
Piston failures are not a common occurrence, but they do occur, and failure is usually associated with fatigue crack growth.
Most failures initiate at the gudgeon pin hole or in the skirt of the piston. Occasionally they fail elsewhere. In the example
covered in this paper, failure initiated in the crown and progressed down to the gudgeon pin before final failure occurred.
This paper outlines the cause and mode of failure and shows that small metallurgical discontinuities can contribute to these
failures under the right circumstances. 相似文献
78.
Alloying zinc coatings with elements such as magnesium and titanium increases the corrosion resistance in industrial tests. Based on the fundamental mechanism of cathodic delamination, a simple concept how alloying zinc with specific elements might improve its resistance to cathodic delamination is presented in this paper. As an example, results concerning the delamination of a simple polymer from the zinc‐magnesium intermetallic MgZn2 are presented. From electrode potential measurements obtained with the Scanning Kelvin Probe it can be concluded that cathodic delamination from this alloy is completely inhibited. This behaviour is attributed to the electronic properties of the magnesium‐rich oxidic passive layer, that inhibits the oxygen reduction reaction at the metal oxide/polymer interface. 相似文献
79.
Crystallization of Polymer-Derived Silicon Carbonitride at 1873 K under Nitrogen Overpressure 总被引:1,自引:0,他引:1
Martin Friess Joachim Bill Jerzy Golczewski re Zimmermann Fritz Aldinger Ralf Riedel Rishi Raj 《Journal of the American Ceramic Society》2002,85(10):2587-2589
The chemical stability of an amorphous silicon carbonitride ceramic, having the composition 0.57SiC·0.43Si3 N4 ·0.49C is studied as a function of nitrogen overpressure at 1873 K. The ceramic suffers a weight loss at p N2 < 3.5 bar (1 bar = 100 kPa), does not show a weight change from 3.5 to 11 bar, and gains weight above 11 bar. The structure of the ceramic changes with pressure: it is crystalline from 1 to 6 bar, amorphous at ∼10 bar, and is crystalline above ∼10 bar. The weight-loss transition, at 3.5 bar, is in excellent agreement with the prediction from thermodynamic analysis when the activities of carbon, SiC, and Si3 N4 are set equal to those of the crystalline forms; this implies that the material crystallizes before decomposition. The amorphous to crystalline transition that occurs at ∼10 bar, and which is accompanied by weight gain, is likely to have taken place by a different mechanism. A nucleation and growth reaction with the atmospheric nitrogen is proposed as the likely mechanism. The supersaturation required to nucleate α-Si3 N4 crystals is calculated to be 30 kJ/mol. 相似文献
80.
C Benz WR Martin J Arnold R Jakobs JF Riemann 《Canadian Metallurgical Quarterly》1997,122(13):391-395
OBJECTIVE: To evaluate whether push enteroscopy of the small bowel (PES), undertaken after extensive previous investigations in suspected intestinal bleeding from an uncertain site, chronic diarrhoea or lymphoma of the small intestine, contributes to the diagnosis, and to ascertain the results of PES and its clinical significance. PATIENTS AND METHODS: 56 consecutive patients (29 men, 27 women; mean age 63 years) were investigated prospectively. The main indications for PES were the search for the source of intestinal bleeding in 79% of patients (group A), chronic diarrhoea or tropical sprue in 16% (group B) and search for tumour of lymphoma in 5% (group C). PES was always performed in fasting patients under sedation/analgesia using a video PES, which contrary to catheter enteroscopy provides a channel for intervention. RESULTS: In group A 27% of patients were found to have lesions, in particular angiodysplasias, or (in once case) leiomyoma. Half of these patients were successfully treated endoscopically without later surgical intervention being required (mean follow-up of six months). In the other half operation became necessary, either because the disease itself indicated it or the bleeding persisted, the source being in the more distant small intestine and thus not accessible to endoscopic intervention: only 50% of the length of the small intestine proved to be within reach of the instrument. No abnormalities were discovered in patients of groups B and C. CONCLUSION: In cases of gastrointestinal bleeding from an uncertain source PES should be performed first, because in many cases it may obviate surgical intervention. But PES seems to contribute little of diagnostic value in other indications. 相似文献