The oxidation state of sulfur detected in Na2O-CaO-SiO2 float glass by X-ray absorption near edge structure spectra

The oxidation state of sulfur is detected in Na2O-CaO-SiO2 float glass by synchrotron radiation X-ray absorption near edge structure (XANES) spectra at the sulfur K edge. The measured spectra show the only presence of S6+ in the Na2O-CaO-SiO2 float glass and the oxidation state of sulfur do not change with the increase of glass depth. It is also found that, after the melt has gone through the molten tin bath, the S6+ is the dominant species, but S2- is also present on both surfaces. It is not certain whether cation bonds to S2- or not, because there are many cations dissolved in the melted tin which makes the spectrum complicated.     

Pressure-induced non-bulk superconductivity in Eu1.2Mo6(S1−x Se x )8

High-pressure study has been made both resistively and magnetically on Eu_1.2Mo₆(S_1–x Se _x )₈. Superconductivity was detected at a lower pressure in samples forx0 than forx=0 in spite of the larger unit cell volume of the former. The superconductivity observed remains non-bulk up to 20 kbar. The maximum onset temperature of the superconductivity transition decreases withx.On leave from the Physics Institute, Chinese Academy of Sciences, Peking, China.     

基于随机有限元的梁单元反应变异性分析

针对工程中由于不确定因素的影响而导致的结构反应的变异,利用随机有限元推导了在多个随机变量作用下梁单元结构反应变异的公式,以镗刀杆工作的位移变异为例,详细地介绍了其计算过程,并将其与解析法和Monte-Carlo法进行了对比,分析了各自的适用范围,为不确定性结构的可靠性分析奠定了基础。     

自然循环锅炉汽包寿命计算及影响因素分析

文中叙述了汽包寿命的计算方法，并针对各种运行工况计算出寿命消耗量，根据理论计算结果分析影响汽包寿命的主要因素，提出了增加汽包寿命的方法。     

自动化专业的学科属性及主干课程设置探讨

本文对自动化专业的学科属性、主干课程设置、教学改革建议等进行了讨论，提出了加强数学和工程背景基础，以适应未来社会需求等建议，对教师素质的提高也进行了探讨。     

在PowerBuilder中提高数据录入效率的方法研究

以数据窗口控件为实现对象,介绍提高数据录入效率的主要处理方法.     

基于支持向量机方法的压电智能结构系统辨识

支持向量机(SVM)是一种基于统计学习理论和结构风险最小化原则的新型机器学习方法,克服了传统机器学习方法在训练中的局部极小问题,过学习和欠学习等问题,具有很好的泛化能力.本文介绍了应用于回归分析的最小二乘支持向量机(LS-SVM)的基本理论,然后以随机激励下压电智能结构的响应数据作为训练样本集,采用LS-SVM方法辨识系统,仿真结果验证了这种方法的有效性.     

银川部分污灌区生产大米铅含量分析

采用电感耦合等离子体-原子发射光谱(ICP-AES),测定分析了银川地区紫金花造纸厂污灌区生产大米的铅的质量分数.分析结果显示:该污灌区生产大米中铅的质量分数平均值为4.5mg/kg(n=5),RSD<1%,超过国家对食品中铅的质量分数规定的最高限定值10倍,说明该大米已不能食用;由于尚未超过国家对动物饲料规定的铅的质量分数的最高限定值,因此它尚可作为饲料,但已接近临界状态.     

激光电视全息技术及其在无损检测中的应用

激光电视全息技术是一种测量物体表面微小变形的非接触式测量技术.与常规检测方法相比,它具有高精度、全场、实时测量等特点,有着重要的理论研究和实用价值,是当前无损检测领域研究热点之一.本文介绍了激光电视全息技术的基本原理和特点、国内外在无损检测领域的应用成果和最新研究进展,并探讨了未来的发展趋势.     

Properties of Magnetic Nanoparticles about Doped Rare Earth and Its Composites

The magnetic liquid was prepared with ferric salt by inorganic gel technology. The effect of the doped rare earth elements on the properties of magnetic particles was analyzed. The magnetic liquid was composed with clay mineral into magnetic mineral composites. The crystal structure and micro-morphology of the nanoparticles were studied by XRD and TEM. The results show that the crystal structure of the magnetic particles doped 0.5 % of lanthanum is more complete, and the magnetic response capability is higher with doping agent. At the same time, the possibility of the clay mineral magnetic composites as the carrier of target drug was probed.