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71.
The basic concept of a novel frequency-based on-line expert system (FBOLES) approach for on-line fault diagnoses in nuclear power plants has been presented previously. This paper reports further progress, and includes how to express the uncertainties of expert opinion in knowledge-bases and propagate then in inferences, and how to deal with imperfect knowledge-bases. It also describes the main elements of FBOLES and outlines how the system works under complex conditions including the dynamic behavior of signals during accidents, multiple failures, and on-line changes of plant operation mode. Its ability to diagnose root causes of accidents has been tested using the main steam and feedwater condensate systems of a full-scale, three-loop, 950 MW nuclear power plant simulated by the Tsinghua simulator. So far the results seem good. 相似文献
72.
用红外、质谱、核磁共振等手段确证了江阴农药厂合成的苯菌灵的化学结构,并进行了该化合物核磁共振谱线的归属。 相似文献
73.
74.
结合化肥厂丁辛醇装置薄管板换热器的设计 ,着重分析薄管板的特点 ,应用合理的计算方法对薄管板进行强度校核 ,验证这一新型换热器的安全性和经济实用性 相似文献
75.
Shufang Wang Yuanhui Ma Yanji Wang Wei Xue Xinqiang Zhao 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(11):1466-1471
BACKGROUND: A single‐step conversion of nitrobenzene (NB) to p‐aminophenol (PAP) through catalytic hydrogenation is a widely used synthesis route for PAP. The main shortcoming of this route is the use of sulfuric acid for rearrangement of the phenylhydroxylamine (PHA) intermediate. In this paper, S2O82?/ZrO2 (PSZ) solid acid and Pt‐S2O82?/ZrO2 (Pt‐PSZ) bifunctional catalysts were prepared for the synthesis of PAP in non‐acid medium. RESULTS: Calcination temperature has a substantial effect on the acidity, structure and activity for PHA rearrangement of PSZ. The highest PAP yield was 33.8% over PSZ calcined at 823 K when the reaction was carried out in water at 423 K. A high PAP yield of 23.9% was achieved by a single‐step reaction of nitrobenzene over Pt‐PSZ bifunctional catalysts. CONCLUSION: PSZ solid acid exhibits high activity for PHA rearrangement. Perfect tetragonal ZrO2 and much stronger acid sites play important roles in catalytic activity. Inhibiting the hydrogenation activity by reducing the amount of Pt loading on Pt‐PSZ can improve the competition of PHA rearrangement on acid sites with hydrogenation of PHA on metal active sites, resulting in better selectivity to PAP. Copyright © 2008 Society of Chemical Industry 相似文献
76.
阐述了以“三个代表”要求建设高素质施工管理人员队伍的必要性 ,指出只要尊重知识、尊重人才 ,建立和完善激励机制 ,就能激发广大管理人员的积极性、主动性和创造性 相似文献
77.
生产电子工业用高纯氮的制氮装置 ,其要点和难点是一氧化碳和氢的清除。采用一氧化碳转换炉和特殊的冷箱内流程组织 ,可以生产纯度为 99 9999%以上的高纯氮。对制取电子工业用高纯氮制氮装置与常规制氮装置加氮终端净化器两种流程进行了比较。 相似文献
78.
79.
A non-destructive and in-situ technique for the measurement of tritium in materials, namely β-ray-induced X-ray spectrometry (BIXS), has been developed recently. In the present study a V-4Cr-4Ti alloy was pre-heated at 1000℃ for 2 h to form a recrystallization structure before the tritium absorption experiments were conducted. Firstly the hydrogen isotope gas was charazterized by means of a quadrupole mass spectrometer (QMS) and a small-sized ionization chamber. Then hydrogen isotope absorption tests of V-4Cr-4Ti alloy were performed at 400 ℃ and the atomic concentration of hydrogen isotope in V-4Cr-4Ti alloy was estimated as 0.17% with a tritium content of approximately 2.5 ppm. Experimental results indicate that BIXS is a quite useful tool for quantitatively measuring the tritium content and tritium distribution in the surface layers of vanadium alloys and no strong trapping effects of tritium exist in the pre-heated V-4Cr-4Ti alloy. 相似文献
80.