中原高温高盐油藏疏水缔合聚合物凝胶调剖剂研究

针对中原油田高温(>80℃)、高盐度(>50 g/L)、高硬度(>1 g/L)砂岩油藏,研制了地下成胶的高热稳定性聚合物凝胶调剖剂。所用聚合物为疏水缔合聚合物AP-P4,M=9.0×106,HD=27%,疏水基摩尔分数0.2%;交联剂为可生成酚醛树脂的3种化合物;调剖剂胶液用矿化度160 g/L的马寨油田污水配制;实验温度95℃。根据形成的凝胶黏度(95℃,1.1 s-1)确定交联剂各组分用量为:MZ-YL 0.429%,MZ-BE 0.060%,MZ-XS 0.012%;酸度调整剂用量0.12%;成胶时间10~15小时。2.5、3.0、3.5 g/L AP-P4的凝胶在95℃老化100天后黏度保持在~40 Pa.s及以上。初配制胶液在3000 r/min下剪切15分钟后黏度降低87.5%~89.0%,但成胶后和老化过程中凝胶黏度只比未剪切样降低17.1%~6.6%。3.5 g/L AP-P4的调剖剂对~1μm2的6支储层岩心的堵塞率在88.1%~95.8%范围,平均93.3%,造成的残余阻力系数在15.2~28.6范围,平均19.8,使渗透率级差2.3~8.0的4组双人造岩心的注水流量比发生不同程度的反转。认为该凝胶调剖剂高温下稳定性好的原因,是强化学交联密度低,因而凝胶脱水收缩作用弱。图2表5参5。     

一种控制盐层段井眼闭合率的钻井液密度新公式

针对钻井过程中钻遇的盐层段井眼蠕变缩径问题,利用弹塑性力学理论,蠕变本构方程采用Heard蠕变方程,在平面应变和均匀地应力假设下,推导出控制井眼收缩的钻井液密度新公式,该公式与前人推导的公式不同。通过理论分析,指出产生差异的根本原因在于蠕变应力差(极坐标下表示的径向应力与切向应力之差)公式的推导上,用有限元法计算结果对理论公式进行检验,证明是可行的。对文中的力学模型采用有限元法建模、求解,利用求解结果对各应力差公式进行验证,得出:根据文中公式计算结果与有限元法计算结果完全一致,而据前人公式计算结果偏离有限元计算值较大,从而间接证明了该钻井液密度新公式的推导更严密,更准确。     

Pb/Sn凸剪切性能研究

在实际使用条件下,Pb/Sn凸点会由于承受温度循环而产生剪切应力,剪切应力导致的主要失效方式是开裂.通过对倒装焊后Pb/Sn凸点剪切强度的测量及对剪切后断口的分析,发现破坏主要发生在凸点下金属(UBM)层内部或UBM与Al焊盘之间,平均剪切强度受凸点尺寸影响很小,范围在21～24MPa。     

Exciton photoluminescence in doped quasi-1D structures based on silicon

The dependence of carrier density in silicon quantum wires sheathed with SiO₂ on the wire diameter and the position of impurity atoms in respect to the wire center is analyzed theoretically. It is shown that, as the diameter of wires and nanocrystals decreases, the ionization energy of a dopant increases; therefore, the free carrier density decreases, and the screening of the Coulomb attraction becomes ineffective. As a result, the photoluminescence is defined by the radiative recombination of excitons even in the case of heavily doped Si. These conclusions are supported by the data of experimental study of spectral, excitation-power, and temperature dependences of photoluminescence in porous silicon structures fabricated on lightly and heavily doped Si substrates.     

用两亲聚合物制备大颗粒苯丙乳液

分别以两亲聚合物P(C9-AA)和P(DCPD-St-α-St-AA)作乳化荆，研究了制备大颗粒(约1μm)及具有一定稳定性的苯丙乳液的方法，讨论了乳化剂，温度及引发剂用量对乳液性能的影响。结果表明，以P(C9-AA)作乳化剂时，引发剂用量为单体质量的1．2％，90℃时可以合成性能良好的苯丙乳液；以P(DCPD-St-α-St-AA)作乳化荆时，引发剂用量为单体质量的1．2％，80℃时可以合成性能良好的苯丙乳液。     

浅论太阳电池在通信工程中的应用

介绍了太阳电池应用的一般要求和太阳能供电系统的组成及运行，给出了工程设计个常用的太阳电池容量计算方法，并提出太阳能供电系统运行维护注意事项。     

Preparation of trichlorosilane by plasma hydrogenation of silicon tetrachloride

We have studied silicon tetrachloride hydrogenation in an rf (40.68 MHz) plasma and have determined the trichlorosilane yield as a function of the molar energy input, H₂: SiCl₄ molar ratio, and pressure. The highest trichlorosilane yield achieved is 60%, and the minimum energy input is 0.3 kW h per mole of SiHCl₃.     

IGBT无损吸收网络的设计

提出一种模块化IGBT无损吸收网络，介绍了其缓冲吸收原理、元件参数计算及一些注意事项。     

高压电动机定子线圈匝间绝缘问题的探讨

在实践经验的基础上，分析了我国匝间绝缘短路的主要原因，提出在匝间绝缘的设计，制造工艺及耐压试验等工序采取合理措施，以提高匝间绝缘的可靠性。     

Soft X-ray emission from the plasma of a conductor exploding in a strong longitudinal magnetic field

Previous experiments with the electric explosion of conductors in a strong (50 T) longitudinal magnetic field showed the formation of a relatively low-density plasma around the central part of the explosion channel, which exhibited expansion at a velocity on the order of 10–20 km/s [1, 2]. Expansion of the plasma was accompanied by displacement of the magnetic field from the explosion channel, which was manifested by a diamagnetic signal. An analysis of the plasma energy balance is hindered by the lack of reliable data about radiative energy losses. Here, we report the first experimental results on the radiation pulse kinetics and the first estimates of the radiation energy.