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排序方式: 共有2771条查询结果,搜索用时 15 毫秒
41.
Takashi Kojima Wataru Sakamoto Toshinobu Yogo Takashi Fujii Shin-ichi Hirano 《Journal of the American Ceramic Society》2002,85(9):2212-2216
An in situ composite composed of ceria-stabilized tetragonal zirconia polycrystals (Ce-TZP) and La{Co0.5 Fe0.5 (Fe0.9 Al0.1 )11 }O19 was synthesized from a powder mixture of Ce-TZP, La(Fe0.9 Al0.1 )O3 , Fe2 O3 , Al2 O3 , and CoO. The dense Ce-TZP dispersed with platelike La{Co0.5 Fe0.5 (Fe0.9 Al0.1 )11 }O19 crystals as a second phase were formed after sintering from 1250° to 1350°C. The saturation magnetization of the in situ composite Ce-TZP/La{Co0.5 Fe0.5 (Fe0.9 Al0.1 )11 }O19 was proportional to the mass fraction of the hexaferrite second phase in Ce-TZP. The coercivity of the composite with a 20 mass% of second phase decreased from 9.14 to 2.52 kOe (from 728 to 201 kA/m) after the pulverization of the composite. The susceptibility (χ) increased by 15%–25% under uniaxial stress on the composite. The change of the susceptibility (Δχ/χ) value increased with decreasing the mass fraction of the second phase in the composite. The Δχ was found to increase linearly with applied stress and abruptly change on cracking, which is expected for the application in fracture sensing of the composite. 相似文献
42.
At temperature above 300°C the glycosyl units of cellulose are simultaneously depolymerized to a tar and decomposed to a char by evolution of H2O, CO, and CO2. When the glycosyl units are depleted, a stable char is formed containing about 30% aliphatic and 70% aromatic components. The aliphatic component is formed first, but on further heating is converted to polycyclic aromatic structures. The chars formed at lower temperatures are more combustible because the aliphatic component of the char is highly pyrophoric and is oxidized almost at the same temperature at which it is formed (~360°C). The aromatic component, however, is less reactive and is oxidized at ~520°C. Consequently, the chars formed at higher temperatures are less combustible. It has been shown that (NH4)2HPO4, which is a well-known flame retardant and smoldering inhibitor, lowers the pyrolysis temperature and increases the char yield by accelerating the decomposition reactions. This affects the composition of the intermediate chars but the final products have about the same composition irrespective of additives. (NH4)2HPO4 also lowers the rate of oxidation of the aromatic component and the corresponding heat release. NaCl, which is an enhancer of smoldering combustion, has a slight stabilizing effect on pyrolysis of cellulose. It lowers the oxidation temperature of the aromatic component and dramatically increases its rate. The corresponding heat release is also increased due to complete oxidation to CO2. The rate of oxidation calculated from the dynamic thermal analysis data is more than tripled by NaCl and significantly reduced by (NH4)2HPO4. 相似文献
43.
Ping Shen Hidetoshi Fujii Taihei Matsumoto Kiyoshi Nogi 《Journal of the American Ceramic Society》2005,88(4):912-917
Wetting phenomena and the effect of alumina surface orientation on the wettability in Si/α-Al2 O3 system were studied by an improved sessile drop method using , , C(0001) faces of single crystals and polycrystals at 1723 K in a reducing Ar–3% H2 atmosphere. The contact angles show a vibration behavior for all the single crystals but to a less extent for the polycrystals. The extent of the vibration correlates not only with the reaction intensity but also with the stability of the Si droplet on the alumina surfaces. The interfacial reaction leads to the formation of a series of reaction rings, which is more serious at the single crystal surfaces. More importantly, the wettability is dependent on the alumina surface orientation, with the intrinsic contact angles being about 98±2°, 101±1°, 69±1°, and 98±2°, respectively, for the , , C(0001) and polycrystal α-Al2 O3 substrates. The much smaller contact angle for molten Si on the C(0001) surface is explained by the favorable reduction in the Si/α-Al2 O3 interfacial free energy by the terminated and enriched aluminum atoms at the reconstructed surface. The importance of the aluminum presence at the Si/α-Al2 O3 interface to the wettability of this system was further demonstrated by a substantial improvement in the wettability of the α-Al2 O3 substrates by Si–Al alloys. 相似文献
44.
Gopal P. Khanal Ichiro Fujii Shintaro Ueno Satoshi Wada 《Journal of the American Ceramic Society》2021,104(9):4649-4658
The <110>-oriented BaTiO3 ceramics were fabricated using BaCO3 matrix and H1.08Ti1.73O4.nH2O (HTO) template particles, and the mechanism of BaTiO3 phase formation was investigated. The dielectric, ferroelectric, and piezoelectric properties were also investigated. The transformation of the HTO phase into the TiO2 bronze or TiO2 (B) phase was observed at 600°C, where the BaTiO3 nucleation was accompanied by the formation of a Ba2TiO4 phase. The TiO2 phase reacted with the Ba2TiO4 phase at 800°C to give a BaTiO3 phase, whereas its reaction with the BaTiO3 resulted in the formation of BaTi2O5 phase that got decomposed into BaTiO3 and Ba6Ti17O40 phase at sintering temperature ≥1300°C. Sintering with samples’ embedding in BaTiO3 powders prevented the formation of the Ba6Ti17O40 secondary phase. The crystallographic orientation along the <110> direction (F110) was developed by the epitaxial grain growth mechanism. In addition to the contribution of the grain-size increment for enhancing the F110, the preservation of the platelike structure was also found to have a significant impact. The ceramics prepared by the embedded sintering (grain size ≈12.4 µm and F110 = 83%) exhibited the room-temperature dielectric constant of 1708 and piezoelectric strain constant of 445 pm/V, which are higher than those of the BaTiO3 ceramics with randomly oriented grains. 相似文献
45.
T. Nagira X. C. Liu K. Ushioda H. Fujii 《Science & Technology of Welding & Joining》2020,25(3):198-207
ABSTRACTThe microstructural evolutions of pure Ag and Ag-0.75 wt-%Sn during rapid cooling friction stir welding (FSW) were examined. At the lower welding temperature of FSW conditions, the annealing twinning was highly suppressed and the microstructural evolution was dominated by the discontinuous dynamic recrystallisation (DDRX) via the high angle boundary (HAB) bulging. The fully recrystallised microstructure was remarkably finer than that formed through the frequent annealing twinning at the higher welding temperature. Moreover, the Sn-addition caused the HAB bulging due to the inhibition of dynamic recovery and decreased mobility of grain boundaries. With decreasing the ratio of the peak temperature to the recrystallisation temperature, the dominant grain refinement mechanism is implied to change from the annealing twinning to the DDRX. 相似文献
46.
Yasuhiro Jimbo Yuki Tamatsukuri Minato Ito Kohei Yokoyama Yoshiharu Hirakata Shunpei Yamazaki 《Journal of the Society for Information Display》2015,23(7):313-318
To improve the reliability and mechanical durability of a flexible organic light‐emitting diode display, the entire flexible display is coated with an aluminum oxide film by atomic layer deposition (ALD). Because the step coverage of ALD is excellent, the AlOx film was deposited not only on the front and back surfaces but also on the side surfaces of the display. A high‐temperature and high‐humidity preservation test, repetitive bending tests, and a pencil hardness test were conducted on the flexible display with ALD‐AlOx coating. The display survived 500 h of a 65°C, 95% preservation test, endured a 100,000‐time repetitive bending test with a curvature radius of 4 mm, and was found to have a pencil hardness of 4H. 相似文献
47.
Computational Visual Media - Iris folding is an art-form consisting of layered strips of paper, forming a spiral pattern behind an aperture, which can be used to make cards and gift tags. This... 相似文献
48.
Senevirathna ST Tanaka S Fujii S Kunacheva C Harada H Shivakoti BR Dinh H Ariyadasa T 《Water science and technology》2011,63(10):2106-2113
Perfluorinated compounds (PFCs) have attracted global concern due to their ubiquitous distribution and properties of persistence, bio accumulation and toxicity. The process of adsorption has been identified as an effective technique to remove PFCs in water. Different non ion-exchange polymeric adsorbents were tested with regard to their sorption kinetics and isotherms at low PFCs concentrations. Selected PFCs were perfluorobutanoic acid (PFBA), perfluoroheptanoic acid (PFHpA), perfluorooctanoic acid (PFOA) and perfluorodecanoic acid (PFDA) and the tested polymers were three types of Dowex optopores (V-493, V503, and L493), Amberlite XAD-4, and Filtrasorb 400 (Granular Activated Carbon-GAC). We observed the selective adsorption of PFCs on synthetic polymers. For PFDA, Amberlite XAD-4 gave the Freundlich adsorption constant of 2,965 (microg PFCs/g sorbent)(microg PFCs/L)(-n), which was higher than that of GAC (121.89 (microg PFCs/g sorbent) (microg PFCS/L)(-n)). In the case of PFBA, GAC showed better performance (13.36) (microg PFCs/g sorbent) microg PFCS/L)(-n) than synthetic polymers (0.62-5.23) (microg PFCs/g sorbent) (microg PFCS/L)(-n). Adsorption kinetics of all adsorbents were well described (R2 = 0.85-1) by pseudo-second order kinetic model. Sorption capacity was influenced by initial PFCs concentration for all adsorbents. GAC reached the equilibrium concentration within 4 hours, Amberlite XAD 4 reached it within 10 hours and other polymers took more than 70 hours. 相似文献
49.
Yuki Takenaka Norihiro Abe Yoshihiro Tabuchi Hirokazu Taki Shoujie He 《Artificial Life and Robotics》2009,14(2):224-227
This research was aimed at making a robot that can go and get an object designated by the user. We produced a robot control
system that uses pointing and voice control. This control system is composed of two systems. One system is the object instruction
system that uses pointing, and the other is the object instruction system that uses voice. The approximate position of a designated
object is recognized by the object instruction system that uses pointing, and information about the object and instructions
about the operation are conveyed by the object instruction system that uses voice. This time, the object instruction system
that uses pointing has been designed and verified as the first step. A calculation resource to calculate the approximate position
of the designated object is obtained when the user points directly at the object. A robot can be moved around a designated
object by using this system. The object instruction system that uses voice will be constructed in future work. 相似文献
50.
The relationship between the characteristics of gradient-index rod lenses obtained by ion exchange and their mother glass compositions is studied. It is observed that Li(2)O content, R(2)O (Li(2)O + Na(2)O) content, and the Li(2)O/Na(2)O ratio are important factors in attaining a high acceptance angle and a small field curvature. Thus the gradient-index lens array is fabricated by the use of a newly developed glass composition and its optical performance; the modulation transfer function, luminous intensity, and chromatic aberration are precisely evaluated. The array is found to have a sufficiently high performance to be applicable for color use. 相似文献