Preparation of V/ZrO2 catalysts by the sol-gel method: Physical and structural characterization

Some zirconia-supported vanadium oxides have been prepared by sol-gel method and characterized by different techniques. The vanadium content exerts an effect on the area and pore-size of precursors and samples calcined. The presence of vanadium also affects the decomposition of precursors into ZrO₂ and to its phase transformation, as well as the formation of fibres, as shown by SEM-EDX. XPS analyses show the presence of two species of vanadium at the surface, V^5– and V⁴⁺, the percentage of each one depending on the load of vanadium in the catalyst.     

Study on phase behavior–impact strength relationship of unsaturated polyester/polyurethane hybrid polymer network

The phase behavior of a hybrid polymer network (HPN) composed of poly[(propylene glycol maleate)-co-(propylene glycol phthalate)] crosslinked with styrene and polyester–urethane crosslinked with methylene-bis-ortho-chloroaniline was examined. The correlation between phase separation and impact strength of the HPNs is discussed. The composition of HPNs has an effect on their properties.     

对单件小批铸造生产作业计划进行计算机辅助控制

为有效控制单件小批铸造生产计划的科学制定,石家庄煤矿机械有限责任公司铸造生产中的调度与生产管理方法、生产经验与计算机应用简易结合,取得了良好的效果。促进了公司在铸造工序的管理进步,很好地将经济指标、生产指标、管理目标相统一,提高了铸造的市场适应力与反应力。     

东丽湖邻里中心

在承接这个项目之前，我们不知道天津东部还有东丽湖这么一大片保存完好的湿地，夕阳映照着辽阔的水面，芦苇中闪现着轻盈的水鸟。邻里中心——作为这片宝地旁边200hm^2大型低密度社区第一个登台亮相的小组团，对参与其中的所有人来说，既有动人的诱惑，又有切实的压力。     

以对硝基氯苯为原料合成对氨基苯甲醚

以对硝基氯为原料，利用相转移催化反应，先制备对硝基苯甲醚，然后用铁屑粉还原对硝基苯甲醚合成氨基苯甲醚。第一步反应在70-80℃下回流5h，对硝基苯甲醚的收率可达97%，第二步反应在102℃下回流2h，对氨基苯甲醚的收率为82%，纯度为99%。