原子吸收光谱法测定保护渣中锰含量

采用原子吸收光谱法测定保护渣中锰含量,进行了酸度对测定的影响、试样分解、共存离子干扰、加标回收、精密度分析等试验。结果表明,锰可完全溶解于混合酸溶液中;加入氯化锶,可以消除钠、钙对锰测定的干扰;锰质量浓度在0~12.0μg/mL的范围,工作曲线线性关系良好;加标回收率较高,在97%~102%;测定结果准确度较高,与高碘酸钠光度法分析结果一致性较好。     

Wearing prediction of stellite alloys based on opposite degree algorithm

In order to predict the wearing of stellite alloys,the related methods of rare metals data processing were discussed. The method of opposite degree(OD) algorithm was put forward to predict the wearing of stellite alloys.OD algorithm is based on prior numerical data, posterior numerical data and the opposite degree between numerical forecast data. To compare the performance of predicted results based on different algorithms, the back propagation(BP) and radial basis function(RBF) neural network methods were introduced. Predicted results show that the relative error of OD algorithm is smaller than those of BP and RBF neural network methods. OD algorithm is an effective method to predict the wearing of stellite alloys and it can be applied in practice.     

微制造平台微振动的最优控制

采用混合隔振技术建立了微制造平台隔振系统。该系统以空气弹簧和橡胶层作为被动隔振元件、超磁致伸缩致动器作为主动隔振元件，并采用最优控制理论设计其主动控制器。研究了在不同的性能指标加权阵的情况下，该主动振动控制系统对基础干扰和由微制造设备产生的直接干扰所引起的微制造平台振动的控制效果。研究表明性能指标加权阵对振动控制效果影响非常大。通过大量的仿真实验确定了一组性能指标加权阵，使所设计的主动控制系统能在较宽的频率范围对基础干扰和直接干扰所引起的微制造平台振动进行有效的控制。     

电视新闻拍摄也需要美感

分析电视新闻拍摄美感的重要性和必要性,提出在实地拍摄过程中如何体现电视新闻的美感。     

数值试井在白6-2井测试资料分析评价中的应用

数值试井是在近来发展的一项新的试井解释技术，具有处理非均质，复杂边界油气藏问题的优点，弥补了常规解析试井技术的不足。运用数值试井解释技术，结合动、静态资料，通过对白6-1断块白6-2井测试资料的综合分析评价，确定了储层渗流参数，落实了该气藏的边界情况，为该断块下一步开发提供可靠依据。     

高水头弧形闸门止水型式研究

介绍了高水头弧形闸门止水型式,在此基础上,论述了突扩门槽的水力学问题。结合一些国内工程实例,探讨了高水头闸门常用的3种止水型式(偏心铰压紧式、液压伸缩式、滑动转铰式)的结构特点和适用范围。     

预处理工艺对硬质合金与金刚石膜间粘结力的影响

在两种经不同预处理的硬质合金YG8基底上，采用微波等离子体化学气相沉积法，在微波功率2kW，压强4.0kPa和6.5kPa，CH4和H2流量分别为1.6cm/s和100.0cm/s的条件下生长金刚石薄膜。利用X射线衍射检测了金刚石薄膜是否存在，用拉曼光谱分析了薄膜的质量，用金相显微镜观察了薄膜的洛氏硬度压痕，标定并比较了不同预处理工艺膜与基底的结合力。实验结果表明，不同的预处理方法对于粘结力的影响不大，最主要的因素是钴含量的多少。     

Protein binding study of isoflavone, perillyl alcohol and S-ibuprofen by high-performance frontal analysis

High-performance frontal analysis (HPFA) was used for a protein binding study of isoflavones (daidzein, genistin, and genistein), enantiomers of perillyl alcohol and S-ibuprofen to human serum albumin (HSA). The analyses were performed on a Develosil and Inertsil 100-Diol-5 column (10 cm×4.6mm). Sodium phosphate solution (pH 7.4, ionic strength 0.17) was used as the mobile phase at a flow rate of 1 ml/min. To ensure the drug to be eluted as a trapezoidal peak with a plateau, injection volumes were each fixed up the zonal profile with an evident plateau appears. The unbound drug concentration was determined from a plateau height of the plateau region after that experimental data were fitted by Scatchard equation. The binding constants (K) and total binding affinities (nK) of drugs to HSA were calculated, respectively.