奇偶间隔基短链双季铵膨润土的制备及结构表征

以六甲基丙二铵二甲硫酸盐(PDAS)和六甲基丁二铵二甲硫酸盐(BDAS)为改性剂制备奇偶间隔基短链双季铵有机膨润土,通过X-射线衍射(XRD)、红外光谱(FT-IR)、热分析(TG)和电镜(SEM/TEM)等手段表征其结构.结果表明,PDAS和BDAS改性膨润土层间距分别为1.380 nm和1.413 nm,两种双季铵盐在层间只能以单层平卧的方式排列;有机膨润土中,PDAS是分步分解的,BDAS是一步分解,PDAS和BDAS的开始热分解温度和最大质量损失率对应温度(tpeak)相比其季铵盐固体分别提高了15,30℃和30,80℃;PDAS和BDAS有机膨润土的表面形貌有明显差异.     

梯级电站建设对水质的影响

采用一维水动力数学模型和水质数学模型,对梯级电站建设前后的CJ江干、支流的水质变化进行研究,预测CJ江2020年5个梯级电站建设后干流水质主要参数的变化情况。结果表明,各梯级电站水库蓄水后各坝址处平均DO质量浓度将较建库前略有下降,BOD5和NH3-N的质量浓度呈下降趋势,TP质量浓度变化较小。     

Optimal design of butterfly-shaped linear ultrasonic motor using finite element method and response surface methodology

A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to realize the optimal design of the butterfly-shaped linear ultrasonic motor. First, the operation principle of the motor was introduced. Second, the finite element parameterized model of the stator of the motor was built using ANSYS parametric design language and some structure parameters of the stator were selected as design variables. Third, the sample points were selected in design variable space using latin hypercube Design. Through modal analysis and harmonic response analysis of the stator based on these sample points, the target responses were obtained. These sample points and response values were combined together to build a response surface model. Finally, the simplex method was used to find the optimal solution. The experimental results showed that many aspects of the design requirements of the butterfly-shaped linear ultrasonic motor have been fulfilled. The prototype motor fabricated based on the optimal design result exhibited considerably high dynamic performance, such as no-load speed of 873 mm/s, maximal thrust of 27.5 N, maximal efficiency of 43%, and thrust-weight ratio of 45.8.     

氮苷1-(2'''',3'''',4'''',6''''-O-四乙酰基-β-D-吡喃葡萄糖基)-咪唑的制备

以D-葡萄糖(Ⅰ)、醋酸酐为原料,在无水吡啶中制得中间体1,2,3,4,6-O-五乙酰基-D-葡萄糖(Ⅱ),收率为87.5%.在HBr/CH3COOH条件下对Ⅱ异头碳上的乙酰基进行溴代,制得1-溴-2,3,4,6-O-四乙酰基-D-葡萄糖(Ⅲ),不经分离,在相转移催化剂TEBA催化下,Ⅲ直接与2,4-二硝基苯酚反应得到酚苷1-O-(2',4'-二硝基苯)-2,3,4,6-O-四乙酰基-β-D-葡萄糖苷(Ⅳ),最后Ⅳ与1-三甲基硅基-咪唑在无水四氯化锡的催化下,室温反应52 h制得氮苷1-(2',3',4',6'-O-四乙酰基-β-D-吡喃葡萄糖基)-咪唑(Ⅴ),此步反应收率为90%.     

用流延法制备优质陶瓷基片的研究

本文概括了流延成型工艺的现状，介绍了有机基流延成型工艺中溶剂及添加剂的作用和选择原则，同时介绍了几种新的流延成型工艺。     

基于Pro/ENGINEER轮毂模具分型面的建立方式

基于Pro/ENGINEER环境介绍了分型面的建立方法及其分类,概括了设计中的注意事项;提出一种建立轮毂模具分型面的新方法,即侧面影像曲线方法。该方法易于掌握,在轮毂模具的设计中有广泛的应用前景。     

一种LDO稳压器内部动态频率补偿电路的设计

针对LDO稳压器需要进行频率补偿的特点,本文在分析了LDO稳压器利用输出电容等效串联电阻(ESR)进行频率补偿原理的基础上,提出了一种新颖的LDO稳压器动态频率补偿方法。     

双电源水位控制系统中模/数转换的实现

针对双电源供电测控系统中电源切换和电池供电时存在电压纹波较大以及电压值随着时间的推移而变小,从而引起A/D转换结果和实际测量之间误差较大的问题,提出了一种即时校准A/D转换的方法.在检测过程中实时检测供电电压的变化情况,计算电压系数,并根据该系数对实际检测结果进行校正,以减小供电电压对A/D转换的影响.在水位控制系统中对该方法进行了实验验证.结果表明,在150~950 mm水位测量过程中,在不同的供电电压下,检测偏差在1%左右.该方法具有很强的稳定性,完全满足多电源供电系统中对测量精度的要求.     

PCI总线的未来发展

随着计算机的发展，L／O带宽的需求日益增加，现有PCI总线已经无法满足其需求。PCI—X总线和PCI Express总线是PCI总线的两个发展方向。PCI—X总线目前已占据服务器领域，而PCI Express总线最终将在整个计算机行业占据主导地位。     

基于CAN总线的电子垃圾无害处理监控系统

介绍了一种基于CAN总线的电子垃圾无害处理监控系统,详细描述了系统的总体结构原理、硬件电路组成和软件的设计。该系统不仅能实时监测温度和湿度,而且还能监测粮食虫害的发生情况。