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991.
992.
993.
Boon-Seang Chu Sosaku Ichikawa Sumiyo Kanafusa Mitsutoshi Nakajima 《Journal of the American Oil Chemists' Society》2007,84(11):1053-1062
This work was initiated to prepare protein-stabilized β-carotene nanodispersions using emulsification–evaporation. A pre-mix
of the aqueous phase composed of a protein and hexane containing β-carotene was subjected to high-pressure homogenization
using a microfluidizer. Hexane in the resulting emulsion was evaporated under reduced pressures, causing crystallization and
precipitation of β-carotene inside the droplets and formation of β-carotene nanoparticles. Sodium caseinate (SC) was the most
effective emulsifier among selected proteins in preparing the nanodispersion, with a monomodal β-carotene particle-size distribution
and a 17-nm mean particle size. The results were confirmed by transmission-electron microscopy analysis. SC-stabilized nanodispersion
also had considerably high ζ-potential (−27 mV at pH 7), suggesting that the nanodispersion was stable against particle aggregation.
Increasing the SC concentration decreased the mean particle size and improved the polydispersity of the nanodispersions. Nanodispersions
prepared with higher β-carotene concentrations and higher organic-phase ratios resulted in larger β-carotene particles. Although
increased microfluidization pressure did not decrease particle size, it did improve the polydispersity of the nanodispersions.
Repeating the microfluidization process at 140 MPa caused the nanodispersions to become polydisperse, indicating the loss
of emulsifying capacity of SC due to protein denaturation. 相似文献
994.
The objective of this work is to study the transfer of oxygen from gas to liquid phase in an electroflotation cell. The measurements
were performed in a laboratory scale cell using insoluble electrodes, titanium coated with ruthenium oxide as anode and stainless
steel as cathode. The volumetric mass transfer coefficient K
L
a, was characterized for clean tap water as liquid phase for different values of current density (J). The global coefficient
of mass transfer based on the liquid film, K
L
, and the specific interfacial area, a, were characterized. A model which relates K
L
a to current density was established. Different evaluation criteria of oxygen transfer in electroflotation process were determined
and compared with other aeration process. 相似文献
995.
Jose Gerde Connie Hardy Walter Fehr Pamela J. White 《Journal of the American Oil Chemists' Society》2007,84(6):557-563
Two extruded-expelled physically refined soybean oils with reduced contents of linolenic acid, ultra-low- linolenic acid (ULL,
1.5%) and low-linolenic acid (LL, 2.6%), and a extruded-expelled physically refined control oil (control, 5.3% linolenic acid)
were evaluated by frying French fries in a commercial-like setting for 6 h day−1 during 23 days. The oils became darker, increased in yellow color at the beginning, and became redder and less green throughout
the process. Free fatty acids levels were not different among the oils until day 14, after which, ULL was different from the
control for the remainder of frying. The conjugated dienoic acid values were greatest in the control. Generally, ULL and LL
oils had lower percentages of polar compounds than did the control, providing a frying life 2 days longer than the control
and ~30% increase in frying time. A trained sensory panel evaluated the French fries on days 2, 5, and 6. Buttery and potato
flavors decreased, and rancid and painty flavors increased over frying time for all products. Rancid flavor was highest in
the fries from the control oil. Overall, the ULL and LL oils performed better than did the control oil and ULL tended to perform
better than the LL. 相似文献
996.
Ming Cheng Weinong Chen Jianping Jiang 《Journal of the American Ceramic Society》2005,88(6):1666-1668
A novel microscopy is developed for evaluating the fracture toughness of thin ceramic sheets using the micro-indentation method. This microscopy overcomes the theoretical limit of measurement resolution associated with optical microscopes. Using a modified optical microscope, the crack lengths produced by micro-indentation on the surface of an as-fired ceramic sheet can now be measured. Experimental results on an 8 mol% yttria-stabilized zirconia ceramic substrate show that the accuracy of the fracture toughness evaluation is satisfactory. This micro-indentation fracture toughness evaluation method is efficient and economical for thin ceramic substrate surfaces, either polished or as-fired. 相似文献
997.
Raúl Quijada Juan Luis Guevara Mehrdad Yazdani-Pedram Griselda B. Galland Daniel Ribeiro 《Polymer Bulletin》2002,49(4):273-280
Summary
1-Octadecene (C18) was polymerized by using different metallocene catalysts. The rac-Et(Ind)2ZrC12/MAO (I) and rac-Me2Si(Ind)2ZrC12/MAO (III) presented the highest activity as compared with ra-Et(2-Me-Ind)2ZrCl2/MAO (II) and Ph2C(Flu)(Cp)ZrC12/MAO (IV) catalysts. Catalyst IV produced polymers with highest molecular weights. The microstructure of the polymers was
determined by 13C-NMR spectroscopy. Catalyst systems I, II and III produced isotactic polymers while catalyst IV produced polymers with mainly
syndiotactic structures but with large amount of stereoregular error.
Received: 21 June 2002/Revised version: 4 November 2002/ Accepted: 4 November 2002 相似文献
999.
1000.
The new dust removal technical route using the carbon-granular bed filter,packed of carbon particles with appropriate grade derive from an online-process vibration sieve,to replace the traditional baggy filter had been developed successfully for capturing the micro-carbon dusts produced from pulverization of petroleum coke,and the green close loop of carbon materials is thus completed in the combined pulverizing and classifying system and pulverized carbon dust removal process.The high dust removal efficiency greater than 99%,low outlet dust concentration less than 100 mg.m-3,low pressure drop through dust filtration chamber less than 980 Pa,simple and easy design,and flexible and stable operation were achieved also with the carbon-granular bed filter in both bench and industrial scale operations. 相似文献