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271.
Yoshio Oyumi Toshiyuki Anan Hakobu Bazaki Tadamasa Harada 《Propellants, Explosives, Pyrotechnics》1995,20(3):150-155
The site and mechanism by which iron oxide catalyst acted to enhance burning rate and produced plateau burning behavior at high pressure was studied. The condensed phase chemistry study was conducted by isothermal thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC), and rapid-scan FTIR spectroscopic technique. Uncatalyzed ammonium perchlorate (AP) based azide composite propellant showed unstable combustion at relatively lower pressure region. The heat balance at the buring surface would be unstable at these pressures. However, iron oxide altered the burning property of the propellant and enhanced the burning rate with the plateau-mesa burning characteristics. Such pressure insensitiveness of the burning rate indicated that the condensed phase chemistry played important role in the catalytic mechanism of action. According to the microrocket motor tests, physical effect, melted fuel binder covered the AP particles and prevented the further decomposition of AP, had not affected the plateau burning. Fe2O3 was more effective on the burning rate augmentation than Fe3O4. However, the pressure exponent of the burning rate point of view Fe3O4 was favored catalyst to the propellant used here. 相似文献
272.
舰载导弹在值班状态时被认为是一种舰上设备,在飞行状态时被认为是一种飞行器。GJB151B-2013中明确了舰载平台设备需进行CS106项目检测,而导弹由于并非直接与舰上电网连接,如若仍按照GJB151B-2013中规定的尖峰信号指标进行考核,明显存在过试验的情况。针对舰载导弹在电磁兼容CS106指标的裁剪需求,对其考核要求进行了充分的分析和研究,并给出了试验的裁剪建议。 相似文献
273.
The effects of storage temperature (4, 20, 30, 40, 50 °C) and atmospheric conditions in packages (vacuum, atmospheric) on degradation kinetics of monacolin K, an antihypercholesterolemic agent, in red yeast rice powder were investigated using multiresponse modeling approach. Storage of red yeast rice powder at 4 °C under vacuum package was found to enhance retention of monacolin K. Multiresponse modeling revealed degradation path of monacolin K acid form into their dehydromonacolin K and unknown product under vacuum package, while oxidized product was also formed under atmospheric package. Monacolin K lactone form and precursor were degraded into dehydromonacolin K lactone form, while degradation of dehydromonacolin K lactone form to unknown was more pronounced at temperature higher than 30 °C. Oxidized product was also generated from monacolin K lactone form in atmospheric package. High activation energy of monacolin K degradation in acid form indicated that degradation of monacolin K to their dehydromonacolin K was more susceptible to temperature change as compared to lactone form. 相似文献
274.
Hidetoshi Kawasaki Toshiyuki Anan Eishu Kimura Yoshio Oyumi 《Propellants, Explosives, Pyrotechnics》1997,22(2):87-92
In order to improve of mechanical properties at low temperature region, 3,3-bis(azidomethyl)oxetan (BAMO), 3-nitratomethyl-3-methyloxetane (NMMO) and polyester (PE) copolymer were synthesized by using polyester initiator with boron trifluoride etherate. The molar ratio of each units in the BAMO/NMMO/PE copolymer was 7.4/2.6/0.39 according to the 1H-NMR spectrum analysis and was almost exactly the same composition as the monomer fed (7/3/0.33). The relative composition of triad microstructures was same as theoretical value and they were randomly arranged. The PE, which was a replacement of 1,4-butanediol, acted as an excellent soft segment in the copolymer, and the glass transition point of the elastomer was 4.8 degrees lowered by the replacement. This effect was also verified in the mechanical properties of the composite propellant and the tensile elongation was increased from 15% to 40%percnt; at −40 °C. 相似文献