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91.
The synthesis, structural characterization, photo and electroluminescence, thermal and electrochemical properties of a new fluorinated fluorene-containing copolymer are described. The copolymer is formed by alternating mers of [2,3,5,6 tetrafluoro-1,4 phenylene] and [9,9′-dihexyl-2,7 fluorene] and emits blue light with low turn on voltages. The EL performance of the fluorinated copolymer was superior to those of the non-fluorinated analog copolymer and of the corresponding poly(9,9′dihexyl-2,7 polyfluorene) homopolymer. 相似文献
92.
Rodrigues Christian M. G. Ludwig Andreas Wu Menghuai Kharicha Abdellah Vakhrushev Alexander 《Metallurgical and Materials Transactions B》2019,50(3):1334-1350
Metallurgical and Materials Transactions B - A two-phase Eulerian–Eulerian volume-averaged model is used to predict the formation of macrosegregation during the twin-roll casting of... 相似文献
93.
The evidence that biologically active food components are key environmental factors affecting the incidence of many chronic diseases is overwhelming. However, the full extent of such components in our diet is unknown, as is our understanding of their mechanisms of action. Beyond the interaction of these food components with the gut and intestinal immune functions, whey proteins such as lactoferrin are being tested as anticancer agents. Lactoferrin is an iron-binding protein that has been reported to inhibit several types of cancer. In the present work, the effects of bovine milk lactoferrin on human breast cancer HS578T and T47D cells were studied. The cells were either untreated or treated with lactoferrin concentrations ranging from 0.125 to 125 μM. Lactoferrin decreased the cell viability of HS578T and T47D by 47 and 54%, respectively, and increased apoptosis about 2-fold for both cell lines. Proliferation rates decreased by 40.3 and 63.9% for HS578T and T47D, respectively. For the T47D line, cell migration decreased in the presence of the protein. Although the mechanisms of action are not fully known, the results gathered in this work suggest that lactoferrin interferes with some of the most important steps involved in cancer development. 相似文献
94.
Physical properties of spray dried acerola pomace extract as affected by temperature and drying aids
Germano Éder Gadelha Moreira Arthur Cláudio Rodrigues de Souza Maria de Fátima Dantas de Medeiros 《LWT》2009,42(2):641-645
The objective of this study was to assess the impact of some processing parameters on moisture content, flowability, hygroscopicity and water solubility of spray dried acerola pomace extract using maltodextrin and cashew tree gum as drying aids. The experiment was conducted according to Response Surface Methodology, with the independent variables being: inlet temperature (170-200 °C), drying aid/acerola ratio (2:1-5:1), and percent replacement of maltodextrin by cashew tree gum (0-100%). Higher inlet temperatures favored the desired physical properties of the powders, decreasing their moisture contents and hygroscopicity, and increasing flowability. The drying aids decreased the powder hygroscopicity, especially cashew tree gum (CTG), which also enhanced the powder flowability. The best processing conditions to obtain a free-flowing and least hygroscopic acerola pomace extract powder by spray drying were: inlet temperature above 194 °C; drying aid/acerola solid ratio, 4:1; percent replacement of maltodextrin by CTG, at least 80%. 相似文献
95.
Roasting,Grinding, and Storage Impact on Thermodynamic Properties and Adsorption Isotherms of Arabica Coffee 下载免费PDF全文
96.
Dbora Drummond Hauss Monteiro Henrique Limboro Rodrigo Guimares Porto Allyson Nogueira Moreira Wagner Nunes Rodrigues Cludia Silami de Magalhes 《Microscopy research and technique》2020,83(6):597-603
The MeX? software is a useful tool for tridimensional data collection for surface evaluation and could be relevant to evaluate the same specimen in different phases of the study, assuming repeated measures of dental enamel roughness. The aim of this study was to evaluate the influence of sample metallization for dental enamel roughness analysis with 3D images reconstructed using MeX? software from Scanning Electron Microscopy (SEM) images. The influence of 74.98% (%mol/mol) argon?oxygen plasma for carbon layer removal on surface roughness of the metallized specimen was also evaluated. Dental enamel specimens were prepared for SEM analysis with and without carbon metallization using conventional or environmental modes. Argon?oxygen plasma for carbon layer removal was used and surface roughness was re‐evaluated. Roughness obtained by SEM and MeX? reconstructed images, with or without metallization, did not differ. No significant alteration on surface roughness after carbon layer removal using plasma was found. SEM baseline evaluation using conventional mode without sample preparation and in environmental mode were not comparable. Roughness of enamel 3D images reconstructed with MeX? software from SEM images, with or without metallization was similar. The 74.98% (%mol/mol) argon?oxygen plasma removed the carbon layer with no effect on enamel roughness. 相似文献
97.
Reversible Formation of g‐C3N4 3D Hydrogels through Ionic Liquid Activation: Gelation Behavior and Room‐Temperature Gas‐Sensing Properties 下载免费PDF全文
Jia Yan Marco‐Tulio F. Rodrigues Zhilong Song Hongping Li Hui Xu Huan Liu Jingjie Wu Yuanguo Xu Yanhua Song Yang Liu Peng Yu Wei Yang Robert Vajtai Huaming Li Shouqi Yuan Pulickel M. Ajayan 《Advanced functional materials》2017,27(22)
Many unique properties arise when the 3D stacking of layered materials is disrupted, originating nanostructures. Stabilization, and further reorganization of these individual layers into complex 3D structures, can be essential to allow these properties to persist in macroscopic systems. It is demonstrated that a simple hydrothermal process, assisted by ionic liquids (ILs), can convert bulk g‐C3N4 into a stable hydrogel. The gelation occurs through delamination of the layered structure, driven by particular interactions between the IL and the carbon nitride sheets, forming an amphiphilic foam‐like network. This study employs spectroscopic and computational tools to unravel the gelation mechanism, and provides a rational approach toward the stabilization of 2D materials in hydrogels. The solution‐processable hydrogels can also be used as building blocks of complex devices. Chemiresistive gas sensors employing g‐C3N4 3D hydrogels exhibit superior response at room temperature, enabling effective gas sensing under low power conditions. 相似文献
98.
A Complete Separation of Hexane Isomers by a Functionalized Flexible Metal Organic Framework 下载免费PDF全文
Patricia A. P. Mendes Patricia Horcajada Sébastien Rives Hong Ren Alírio E. Rodrigues Thomas Devic Emmanuel Magnier Philippe Trens Hervé Jobic Jacques Ollivier Guillaume Maurin Christian Serre José A. C. Silva 《Advanced functional materials》2014,24(48):7666-7673
The separation ability of branched alkane isomers (nHEX, 3MP, 22DMB) of the flexible and functionalized microporous iron(III) dicarboxylate MIL‐53(Fe)‐(CF3)2 solid is evaluated through a combination of breakthrough experiments (binary or ternary mixtures), adsorption isotherms, X‐ray diffraction temperature analysis, quasi‐elastic neutron scattering measurements and molecular dynamics simulations. A kinetically controlled molecular sieve separation between the di‐branched isomer of hexane 22DMB from a mixture of paraffins is achieved. The reported total separation between mono‐ and di‐branched alkanes which was neither predicted nor observed so far in any class of porous solids is spectacular and paves the way towards a potential unprecedented upgrading of the RON of gasoline. 相似文献
99.
Marcelo Pereira da Silva Rafael Rodrigues Obelheiro 《International Journal of Parallel, Emergent and Distributed Systems》2017,32(4):348-367
With the ever increasing dependence on computers and networks, many systems are required to be continuously available in order to fulfil their mission. Virtualization technology enables high availability to be offered in a convenient, cost-effective manner: with the encapsulation provided by virtual machines (VMs), entire systems can be replicated transparently in software, obviating the need for expensive fault-tolerant hardware. Remus is a VM replication mechanism for the Xen hypervisor that provides high availability despite crash failures. Replication is performed by checkpointing the VM at fixed intervals. However, there is an antagonism between processing and communication regarding the optimal checkpoint interval: while longer intervals benefit processor-intensive applications, shorter intervals favour network-intensive applications. Thus, any chosen interval may not always be suitable for the hosted applications, limiting Remus usage in many scenarios. This work introduces Adaptive Remus, a proposal for adaptive checkpointing in Remus that dynamically adjusts the replication frequency according to the characteristics of running applications. Experimental results indicate that our proposal improves performance for applications that require both processing and communication, without harming applications that use only one type of resource. 相似文献
100.