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101.
Albrethsen J Kaas A Schönle E Swift P Kocova M Gammeltoft S Hansen L Mortensen HB 《Proteomics. Clinical applications》2009,3(3):383-393
Proteomics analysis of serum from patients with type 1 diabetes (T1D) may lead to novel biomarkers for prediction of disease and for patient monitoring. However, the serum proteome is highly sensitive to sample processing and before proteomics biomarker research serum cohorts should preferably be examined for potential bias between sample groups. SELDI‐TOF MS protein profiling was used for preliminary evaluation of a biological‐bank with 766 serum samples from 270 patients with T1D, collected at 18 different paediatric centers representing 15 countries in Europe and Japan over 2 years (2000–2002). Samples collected 1 (n = 270), 6 (n = 248), and 12 (n = 248) months after T1D diagnosis were grouped across centers and compared. The serum protein profiles varied with collection site and day of analysis; however, markers of sample processing were not systematically different between samples collected at different times after diagnosis. Three members of the apolipoprotein family increased with time in patient serum collected 1, 6, and 12 months after diagnosis (ANOVA, p<0.001). These results support the use of this serum cohort for further proteomic studies and illustrate the potential of high‐throughput MALDI/SELDI‐TOF MS protein profiling for evaluation of serum cohorts before proteomics biomarker research. 相似文献
102.
K. Levin Y. Zha R. J. Radtke Q. Si M. R. Norman H. -B. Schüttler 《Journal of Superconductivity》1994,7(3):563-570
We review the spin dynamics of the normal state of the cuprates with special emphasis on neutron data in both the YBa2Cu3O7– and La2–x
Sr
x
CuO4 systems. When realistic models of the Fermi surface shapes are incorporated, along with a moderate degree of spin fluctuations, we find good semiquantitative agreement with experiment for both cuprates. Building on the success of this Fermi-liquid-based scheme, we explore the implications ford-wave pairing from a number of vantage points. We conclude that our present experimental and theoretical understanding is inadequate to confirm or refute thed-wave scenario. 相似文献
103.
We have produced a multilayer transmission filter with 100 periods of Cr/C to achieve a significant phase retardation while maintaining good transmission for photon energies just below the carbon K edge. This device was installed into a polarimeter behind the SX700/3 monochromator at the Berlin synchrotron radiation laboratory, BESSY. The phase-retardation properties were observed as theoretically predicted. Agreement between experiment and calculation could be obtained by introduction of a rather small interface roughness in the simulation code (σ = 0.65 nm rms). An observed phase retardation of 5° was sufficient to permit, for the first time we believe, a complete and unambiguous polarization analysis of soft-x-ray synchrotron radiation (265-eV photon energy) with primary standards. 相似文献
104.
Schäfer M 《Applied optics》1994,33(28):6591-6596
The optical properties of highly chirped gratings of broadband reflection-type volume phase holograms are evaluated by a ray-tracing approach. The deformation of the fringes as well as the change of refractive index is attributed to swelling during processing. For high-efficiency holograms the problem can be reduced to geometric optics. The power density distribution in the focus of an on-axis mirror is calculated by a Monte Carlo integration. The results are discussed for replay conditions that are relevant for photovoltaic applications. 相似文献
105.
Lukas Schäfer Konstantin Skokov Fernando Maccari Iliya Radulov David Koch Andrey Mazilkin Esmaeil Adabifiroozjaei Leopoldo Molina-Luna Oliver Gutfleisch 《Advanced functional materials》2023,33(4):2208821
Permanent magnets based on neodymium-iron-boron (Nd-Fe-B) alloys provide the highest performance and energy density, finding usage in many high-tech applications. Their magnetic performance relies on the intrinsic properties of the hard-magnetic Nd2Fe14B phase combined with control over the microstructure during production. In this study, a novel magnetic hardening mechanism is described in such materials based on a solid-state phase transformation. Using modified Nd-Fe-B alloys of the type Nd16Febal-x-y-zCoxMoyCuzB7 for the first time it is revealed how the microstructural transformation from the metastable Nd2Fe17Bx phase to the hard-magnetic Nd2Fe14B phase can be thermally controlled, leading to an astonishing increase in coercivity from ≈200 kAm−1 to almost 700 kAm−1. Furthermore, after thermally treating a quenched sample of Nd16Fe56Co20Mo2Cu2B7, the presence of Mo leads to the formation of fine FeMo2B2 precipitates, in the range from micrometers down to a few nanometers. These precipitates are responsible for the refinement of the Nd2Fe14B grains and so for the high coercivity. This mechanism can be incorporated into existing manufacturing processes and can prove to be applicable to novel fabrication routes for Nd-Fe-B magnets, such as additive manufacturing. 相似文献
106.
Wanwan Qiu Jenny Gehlen Margherita Bernero Christian Gehre Gian Nutal Schädli Ralph Müller Xiao-Hua Qin 《Advanced functional materials》2023,33(20):2214393
Tomographic volumetric bioprinting (VBP) enables fast photofabrication of cell-laden hydrogel constructs in one step, addressing the limitations of conventional layer-by-layer additive manufacturing. However, existing biomaterials that fulfill the physicochemical requirements of VBP are limited to gelatin-based photoresins of high polymer concentrations. The printed microenvironments are predominantly static and stiff, lacking sufficient capacity to support 3D cell growth. Here a dynamic resin based on thiol–ene photo-clickable polyvinyl alcohol (PVA) and thermo-sensitive sacrificial gelatin for fast VBP of functional ultrasoft cell-laden hydrogel constructs within 7–15 s is reported. Using gelatin allows VBP of permissive hydrogels with low PVA contents of 1.5%, providing a stress-relaxing environment for fast cell spreading, 3D osteogenic differentiation of embedded human mesenchymal stem cells and matrix mineralization. Additionally, site-specific immobilization of molecules-of-interest inside a PVA hydrogel is achieved by 3D tomographic thiol–ene photopatterning. This technique may enable spatiotemporal control of cell-material interactions and guides in vitro tissue formation using programmed cell-friendly light. Altogether, this study introduces a synthetic dynamic photoresin enabling fast VBP of functional ultrasoft hydrogel constructs with well-defined physicochemical properties and high efficiency. 相似文献
107.
108.
S. Matthiesen T. Gwosch T. Schäfer P. Dültgen C. Pelshenke H.-J. Gittel 《Forschung im Ingenieurwesen》2016,80(1-2):17-27
This article shows by experimental studies on angle grinders, how application-equivalent stresses on the components can be determined. For this purpose a distance measurement technique is applied with which the movement of the shaft is detected while the angle grinder is in operation. The research results support validation activities in product development and contribute to early validation. It helps to analyzing the dynamic and working life of the power tool and therefore construction targets are derived. The related applications are considered and power tools with measuring equipment in the lab are tested. The measurement results are presented and possible causes and effects on the life of the components are discussed. With the method of investigation it is possible to study the behavior of subsystems already in development phases in which the overall system is not physically present. 相似文献
109.
R. Strauss G. Angloher A. Bento C. Bucci L. Canonica X. Defay A. Erb F. v. Feilitzsch N. Ferreiro Iachellini P. Gorla A. Gütlein D. Hauff J. Jochum M. Kiefer H. Kluck H. Kraus J. C. Lanfranchi J. Loebell A. Münster C. Pagliarone F. Petricca W. Potzel F. Pröbst F. Reindl K. Schäffner J. Schieck S. Schönert W. Seidel L. Stodolsky C. Strandhagen A. Tanzke H. H. Trinh Thi C. Türkoglu M. Uffinger A. Ulrich I. Usherov S. Wawoczny M. Willers M. Wüstrich A. Zöller 《Journal of Low Temperature Physics》2016,184(3-4):866-872
110.
T. Dubberstein M. Schürmann H. Chaves H.-P. Heller C. G. Aneziris 《International Journal of Thermophysics》2016,37(10):100
A novel vibrating finger viscometer for high-temperature measurement in liquid metals and alloys up to 1823 K was constructed. The dynamic viscosity (\(\eta \)) of the liquid fluid is measured as a product of \((\rho \cdot \eta )^{0.5}\) and the relative change of the field coil input for a constant amplitude recording at the resonant frequency of the oscillator. The viscometer was calibrated at 298 K using reference silicon oils with varying kinematic viscosities (\(\nu \)), \((0.79\hbox { to } 200)\times 10^{-6}\hbox { m}^{2}\cdot \hbox {s}^{-1}\). In the present study, the viscosity of liquid gold (\(99.99\,\%\) Au), silver (\(99.9\, \%\) Ag), and tin (\(99.9\,\%\) Sn) was measured. The viscosities expressed as an Arrhenius function of temperature are: The viscosity values are consistent within the range of available literature data.
相似文献
$$\begin{aligned} \hbox {for Au:}\quad \quad \hbox {ln }\eta= & {} -0.1990+\frac{2669}{T}\\ \hbox {for Ag:} \quad \quad \hbox {ln }\eta= & {} -0.4631+\frac{2089}{T}\\ \hbox {for Sn:} \quad \quad \hbox {ln }\eta= & {} -0.5472+\frac{671}{T} \end{aligned}$$