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71.
The degradation kinetics of poly(3‐hydroxybutyrate‐co‐3‐hydroxyhexanoate), a member of the Nodax family of polymers, were investigated using transient constant shear rate and dynamic time sweep rheological tests. The rate of chain scission at several times and temperatures was correlated with viscosity data and verified using molecular weight determination of the degraded samples. The experimental results show that the molecular weight and the viscosity of Nodax decrease with time over the range of temperatures that were studied (155–175°C). The degradation kinetics, which exhibited first‐order behavior, were determined as a function of the flow history and thermal history. An apparent activation energy of 189 ± 5 kJ/mol for thermal degradation was found by modeling variations in the rate with temperature using an Arrhenius law model. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 98: 66–74, 2005 相似文献
72.
The metabolism of α-linolenic acid from canola oil was studied in eight normolipidemic men. The 42-day study was divided into
three periods: a 6-day pre-experimental and two 18-day experimental. Approximately 75% of the dietary fat (28% of total energy)
was provided by a mixture of fats during the pre-experimental period and either canola oil (CO) or sunflower oil (SO) during
the experimental periods. The CO and SO diets were fed in a cross-over design. The ratios of linoleic to linolenic acid were
2.6∶1 and 73.9∶1 in the CO and SO diets, respectively. Dietary fat source had an effect on plasma phospholipid fatty acids:
18∶1n−9, 18∶3n−3 and 20∶5n−3 were higher (p<0.05), and 18∶2n−6 was lower in the phosphatidylcholine fraction; 18∶1n−9 was
higher and 20∶4n−6 lower in the phosphatidyl-ethanolamine fraction; and 18∶1n−9 and 20∶5n−3 were higher and 20∶4n−6 and 22∶6n−3
were lower in the alkenylacyl-ethanolamine phospholipid fraction on the CO diet as compared to the SO diet. Consumption of
the canola oil diet resulted in higher n−3 fatty acid levels and lower n−6 fatty acid levels in plasma phospholipids than
consumption of the sunflower oil diet. 相似文献
73.
Garrett BC Dixon DA Camaioni DM Chipman DM Johnson MA Jonah CD Kimmel GA Miller JH Rescigno TN Rossky PJ Xantheas SS Colson SD Laufer AH Ray D Barbara PF Bartels DM Becker KH Bowen KH Bradforth SE Carmichael I Coe JV Corrales LR Cowin JP Dupuis M Eisenthal KB Franz JA Gutowski MS Jordan KD Kay BD Laverne JA Lymar SV Madey TE McCurdy CW Meisel D Mukamel S Nilsson AR Orlando TM Petrik NG Pimblott SM Rustad JR Schenter GK Singer SJ Tokmakoff A Wang LS Wettig C Zwier TS 《Chemical reviews》2005,105(1):355-390
74.
75.
Resistance spot welds joining steel sheets were examined using air-coupled ultrasound at 1 MHz. Transmission C-scan images were obtained using two axially aligned transducers, with each focused on its adjacent surface of the specimen. Because of the enormous impedance mismatch between air and steel, the transmitted signal was exceedingly weak, requiring several hours to collect an image. Although the air-coupled images resembled the weld shapes as determined by an independent technique, surface topography introduced considerable image distortion. The smearing of the images was substantially less than the 5.9-mm wavelength in steel, with the steepness of the transition between welded and unwelded areas indicating a transverse resolution about 1 mm. Similarities to near-field imaging are mentioned as a possible explanation for the observed sub-wavelength resolution. 相似文献
76.
Bong-Kyu Chang Yong Lu Hongyun Yang Bruce J. Tatarchuk 《Journal of Materials Engineering and Performance》2006,15(4):439-441
In this study, a microfibrous carrier consisting of 3 vol.% of 8 μm (diameter) glass fibers is used to entrap 45 vol.% of
150 to 250 μm (diameter) SiO2 support particulates. ZnO is then nanodispersed onto the support by impregnation at the loading of 17 wt.%. At equivalent
bed volumes, ZnO/SiO2-entrapped materials provide twofold longer breakthrough times for H2S (with a 67% reduction in sorbent loading) compared with packed beds of 1 to 2 mm commercial extrudates. Five-log reductions
in H2S concentration with up to 75% ZnO utilization at breakthrough are achieved. H2S concentrations from 60 to 2000 parts per million in volume (ppmv) can be reduced to as little as 0.6 ppmv at 400°C in 30%
H2O at a face velocity of 1.7 cm/s for layers as thin as 1.0 mm. At 500 to 600°C, ZnO/SiO2-entrapped materials provide much higher regenerability in air than do 1 to 2 mm commercial extrudates. The use of glass fibers
permits greater than 50 regeneration cycles.
This paper was presented at the ASM Materials Solutions Conference & Show held October 18–21, 2004 in Columbus, OH. 相似文献
77.
We present the design, fabrication, and performance of the multi-specimen heated platform for linear in situ heating during the Temperature-Programmed XPS (TPXPS). The platform is versatile, compatible with high vacuum (HV) and bakeout. The heater platform is tested under in situ linear heating of typical high surface area sorbent∕catalyst support--nanoporous TiO(2). The platform allows the TPXPS of multiple samples located on specimen disk that can be transferred in and out of the TPXPS chamber. Electric characteristics, temperature and pressure curves are provided. Heating power supply, PID temperature controller, data-logging hardware and software are described. 相似文献
78.
We introduce the notion of ranking robustness, which refers to a property of a ranked list of documents that indicates how
stable the ranking is in the presence of uncertainty in the ranked documents. We propose a statistical measure called the
robustness score to quantify this notion. Our initial motivation for measuring ranking robustness is to predict topic difficulty
for content-based queries in the ad-hoc retrieval task. Our results demonstrate that the robustness score is positively and
consistently correlation with average precision of content-based queries across a variety of TREC test collections. Though
our focus is on prediction under the ad-hoc retrieval task, we observe an interesting negative correlation with query performance
when our technique is applied to named-page finding queries, which are a fundamentally different kind of queries. A side effect
of this different behavior of the robustness score between the two types of queries is that the robustness score is also found
to be a good feature for query classification.
相似文献
79.
Jungkyu Kim Michael Junkin Deok-Ho Kim Seunglee Kwon Young Shik Shin Pak Kin Wong Bruce K. Gale 《Microfluidics and nanofluidics》2009,7(2):149-167
Biosensors based on nanotechnology are rapidly developing and are becoming widespread in the biomedical field and analytical
chemistry. For these nanobiosensors to reach their potential, they must be integrated with appropriate packaging techniques,
which are usually based on nano/microfluidics. In this review we provide a summary of the latest developments in nanobiosensors
with a focus on label-based (fluorescence and nanoparticle) and label-free methods (surface plasmon resonance, micro/nanocantilever,
nanowires, and nanopores). An overview on how these sensors interface with nano/microfluidics is then presented and the latest
papers in the area summarized. 相似文献
80.
Sibylle Gruber Joy Kreeft Peyton Bertram C. Bruce 《Computer Supported Cooperative Work (CSCW)》1994,3(3-4):247-269
Research in computer-supported writing has traditionally compared electronic communication with oral, face-to-face communication to identify the benefits and weaknesses of each, as if they entailed dichotomous choices. In this article, we challenge that view and argue instead that any form of communication and its educational usefulness is shaped by the situation in which it is used, the backgrounds and goals of the participants, the institutional and technological setup, and the intended purpose of the medium. Three modes of communication in one graduate course are examined — oral discussion, synchronous written discussion on a local area network, and asynchronous written postings on an email list set up for the class. It was found that patterns of participation, topic introduction, and topic development differed across the three communication modes, but that the three were interwoven with each other and embedded within the larger classroom context and forms of knowledge creation in the class. Thus, rather than examining different communication media separately, researchers interested in understanding computer-supported collaborative writing need to look at how different media are used to create a meta-medium, which is established by the discourse community involved. 相似文献