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21.
Animesh Chakrabarti Man Mohan Sharma 《Journal of the American Oil Chemists' Society》1992,69(12):1251-1253
Anhydrous esterification of myristic acid with propylene was carried out in the temperature range of 110–145°C and pressure
from 190–195 psig in the presence of Amberlyst-15 (cation exchange resin) and Filtrol-24 (acid-treated clay) as catalysts.
The product ester, isopropyl myristate finds use in cosmetic and topical medicinal preparations where good absorption through
the skin is desired. Filtrol-24 is the catalyst of choice, and the recommended operating temperature is 130°C with a pressure
of 190 psig. 相似文献
22.
Chia‐Yin Chen Yu‐Chi Cheng Shau‐Wei Tsai 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2002,77(6):699-705
A lipase‐catalyzed enantioselective hydrolysis process under in situ racemization of the remaining (R)‐thioetser substrate with trioctylamine as the catalyst was developed for the production of (S)‐fenoprofen from (R,S)‐fenoprofen 2,2,2‐trifluoroethyl thioester in isooctane. Detailed investigations of trioctylamine concentration on the enzyme activation and the kinetic behavior of the thioester in racemization and enzymatic reactions were conducted, in which good agreement between the experimental data and theoretical results was observed. © 2002 Society of Chemical Industry 相似文献
23.
24.
The energy release rate, which is the total derivative of the energy with respect to crack length, is recognized as corresponding to the shape sensitivity analysis with the crack length change represented by the tangential component of design velocity. In this paper the sensitivity formula recently developed for a changing boundary condition has been further extended to cover crack kinking under mixed mode loading. Due to difficulty in defining the velocity field at the corner, the energy release rate at the onset of crack kinking is obtained by extrapolating the energy release rates for finite length kinked cracks. A rectangular plate with a single edge slant crack under uniform tension is taken as a numerical example. The multi-region technique in the numerical implementation of the boundary integral equation is adopted to consider the asymmetry of the problem. Excellent accuracy is observed as compared with reference analytic solutions. 相似文献
25.
The humidity response characteristics of La doped BaTiO3 with different sintered densities and room temperature electrical conductivities were investigated using complex impedance measurement. The samples with low density and high resistivity showed the large and nearly linear sensitivity to the change of humidity. The impedance spectra of samples, when exposed to high humidity, can exhibit microstructure-related features, even though they do not give rise to a noticeable characteristic change when exposed to low humidity. The observed impedance patterns were dependent upon the density, and hence the oxidation kinetics of BaTiO3. 相似文献
26.
27.
Balasa F. Catthoor F. Hugo De Man 《Very Large Scale Integration (VLSI) Systems, IEEE Transactions on》1995,3(2):157-172
Memory cost is responsible for a large amount of the chip and/or board area of customized video and image processing system realizations. In this paper, we present a novel technique-founded on data-flow analysis which allows one to address the problem of background memory size evaluation for a given nonprocedural algorithm specification, operating on multidimensional signals with affine indexes. Most of the target applications are characterized by a huge number of signals, so a new polyhedral data-flow model operating on groups of scalar signals is proposed. These groups are obtained by a novel analytical partitioning technique, allowing to select a desired granularity, depending on the application complexity. The method incorporates a way to tradeoff memory size with computational and controller complexity 相似文献
28.
刍议小型水电站项目收购风险管理 总被引:1,自引:0,他引:1
相对于其他项目的收购风险评估,小型水电站(电站总装机容量5万kW以下)收购有其特殊性。在总结和归纳小型水电站特点的基础上,结合一般项目收购风险评估方法,分析项目收购各个阶段存在的风险和对策。为有收购水电项目意向的企业和个人提供决策依据。图1幅。 相似文献
29.
Degradation Behaviors of Metal-Induced Laterally Crystallized n-Type Polycrystalline Silicon Thin-Film Transistors Under DC Bias Stresses 总被引:1,自引:0,他引:1
Min Xue Mingxiang Wang Zhen Zhu Dongli Zhang Man Wong 《Electron Devices, IEEE Transactions on》2007,54(2):225-232
Device degradation behaviors of typical-sized n-type metal-induced laterally crystallized polycrystalline silicon thin-film transistors were investigated in detail under two kinds of dc bias stresses: hot-carrier (HC) stress and self-heating (SH) stress. Under HC stress, device degradation is the consequence of HC induced defect generation locally at the drain side. Under a unified model that postulates, the establishment of a potential barrier at the drain side due to carrier transport near trap states, device degradation behavior such as asymmetric on current recovery and threshold voltage degradation can be understood. Under SH stress, a general degradation in subthreshold characteristic was observed. Device degradation is the consequence of deep state generation along the entire channel. Device degradation behaviors were compared in low Vd-stress and in high Vd-stress condition. Defect generation distribution along the channel appears to be different in two cases. In both cases of SH degradation, asymmetric on current recovery was observed. This observation, when in low Vd-stress condition, is tentatively explained by dehydrogenation (hydrogenation) effect at the drain (source) side during stress 相似文献
30.
Application of model predictive control strategy based on fuzzy identification to an SP-100 space reactor 总被引:1,自引:0,他引:1
In this work, a model predictive control method combined with fuzzy identification, is applied to the design of the thermoelectric (TE) power control in the SP-100 space reactor. The future TE power is predicted by using the fuzzy model identified by a subtractive clustering method of a fast and robust algorithm. The objectives of the proposed fuzzy model predictive controller are to minimize both the difference between the predicted TE power and the desired power, and the variation of control drum angle that adjusts the control reactivity. Also, the objectives are subject to maximum and minimum control drum angle and maximum drum angle variation speed. The genetic algorithm that is effective in accomplishing multiple objectives is used to optimize the fuzzy model predictive controller. A lumped parameter simulation model of the SP-100 nuclear space reactor is used to verify the proposed controller. The results of numerical simulations to check the performance of the proposed controller show that the TE generator power level controlled by the proposed controller could track the target power level effectively, satisfying all control constraints. 相似文献