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81.
Experimental Data Highlighting the Role of Surface Fracture Energy in Quasi-Static Confined Comminution 总被引:1,自引:0,他引:1
Carlos Ovalle Christophe Dano Pierre-Yves Hicher 《International Journal of Fracture》2013,182(1):123-130
Since the pioneering work of Griffith, Linear Elastic Fracture Mechanics has been widely experimentally validated and successfully developed in solid mechanics modeling. However, recent theoretical models applying the energy balance found in Griffith theory specifically for quasi-static confined comminution have until now not been systematically confronted to experiments. In this study, we analyze data of compression tests on crushable sand, where grain breakage has been triggered by flooding the initially dry material at constant stresses. We consider a partition of the dissipation between surface fracture energy and the rearrangement of fragments and grains surrounding crushed particles. Our results show that the role of the surface fracture energy is stressdependent and that its influence becomes less significant at high stresses. 相似文献
82.
The use of glass fibre reinforced polyester composites raises many health and safety and environmental questions. One alternative is the development of high performance bio-based bio-composites with low environmental impact. Improved understanding of interfacial properties is essential to optimise the mechanical properties and durability of these materials, but so far few data are available. The present work describes the interfacial characterization of Flax fibre/Poly(lactic) acid (PLLA) system at the micro-scale using the microbond test. Different thermal treatments have been carried out (cooling rate and annealing) in order to evaluate the influence of matrix and interfacial morphologies as well as residual stress on interfacial properties. Micromechanical models have been used to determine the interfacial shear strength. When cooling rate is slow, improved interfacial properties are observed. 相似文献
83.
Christophe Chlique David Lambertin Pascal Antonucci Fabien Frizon Philippe Deniard 《Journal of the American Ceramic Society》2015,98(4):1308-1313
The purpose of this work was to study the role of cesium in sodium‐based geopolymer and its thermal stability for nuclear waste management. A series of mixed sodium and cesium geopolymer samples (Na1?x Cs x )2O·Al2O3·SiO2·12H2O (referred to as (Na1? x Cs x )‐GP, where x = 0, 0.08, 0.15, 0.42, 1) have been prepared. All geopolymer samples were heated at 1100°C for 24 h. Pollucite (CsAlSi2O6) and feldspathoid (CsAlSiO4) were crystallized from Cs‐GP. Nepheline (NaAlSiO4) and a small amount of crystallized silica were obtained from Na‐GP. The other geopolymers (Na1? x Cs x )‐GP (x = 0.08, 0.15, 0.42) led to pollucite and nepheline main phases. Amorphous silica phase was observed in all the geopolymer samples with various amounts. Phase quantification and scanning electron microscope revealed that higher Cs concentrations in Na‐GP tend to decrease the amorphous phase while improving pollucite and nepheline phase quantification. The amorphous geopolymers have also been studied by pair distribution function analysis. Tetrahedral chains formed by T–O bonding (with T = Si, Al) were shown to be more tighten around Cs+ than around Na+. It led to shorter Cs–T bond than Na–T bond matching the higher solvation property of Na+. Furthermore, thermal study analysis pointed out the fact that geopolymer samples (Na1? x Cs x )‐GP, can be considered as solid solutions. 相似文献
84.
Localized Neuron Stimulation with Organic Electrochemical Transistors on Delaminating Depth Probes 下载免费PDF全文
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87.
Lukas C. Buelens Vladimir V. Galvita Hilde Poelman Christophe Detavernier Guy B. Marin 《化学,工程师,技术》2016,88(11):1684-1692
The kinetics of redox reactions of iron oxide in oxygen carrier 50Fe2O3/MgAl2O4 are examined using different time‐resolved techniques. Reduction kinetics are studied by H2 temperature‐programmed reduction (H2‐TPR) monitored by time‐resolved in situ XRD. In contrast to conventional TPR, in situ XRD distinguishes the three‐stage reduction of Fe2O3 → Fe3O4 → FeO → Fe. It also shows that the oxidation of Fe → Fe3O4 by CO2 has no intermediate crystalline phases, explaining why its kinetics can easily be investigated by conventional CO2 temperature‐programmed oxidation (CO2‐TPO). A shrinking core model which takes into account solid state diffusion allows describing the experimental data. 相似文献
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An overview of recent developments in volatile compounds analysis from edible oils: Technique‐oriented perspectives 下载免费PDF全文
90.
Analysis of target volatile compounds related to fishy off‐flavor in heated rapeseed oil: A comparative study of different headspace techniques 下载免费PDF全文