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21.
Chloride doped polyaniline conducting polymer films have been prepared in a protic acid medium (HCl) by potentiodynamic method
in an electrochemical cell and studied by cyclic voltammetry and FTIR techniques. The FTIR spectra confirmed Cl- ion doping in the polymers. The polymerization rate was found to increase with increasing concentration of aniline monomer.
But the films obtained at high monomer concentration were rough having a nonuniform flaky polyaniline distribution. Results
showed that the polymerization rate did not increase beyond a critical HCl concentration. Cyclic voltammetry suggested that,
the oxidation-reduction current increased with an increase in scan rate and that the undoped polyaniline films were not hygroscopic
whereas chloride doped polyaniline films were found to be highly hygroscopic. 相似文献
22.
B. Pantchev P. Danesh K. Antonova B. Schmidt D. Grambole J. Baran 《Journal of Materials Science: Materials in Electronics》2003,14(10-12):751-752
The hydrogen content, its depth distribution, and its bonding configuration have been studied in hydrogenated amorphous silicon prepared by plasma-enhanced chemical vapor deposition with hydrogen-diluted silane. Nuclear reaction analysis and infrared spectroscopy were used to determine the total amount of hydrogen and its bonded component, respectively. It has been established that the total concentration of hydrogen does not depend on the film thickness, and has a uniform depth profile. The concentration of bonded hydrogen changes with the film thickness within the measurement accuracy. The data obtained suggest the presence of molecular (non-bonded) hydrogen, uniformly distributed in concentration across the film thickness. 相似文献
23.
V. O. Yablonskii 《Chemical and Petroleum Engineering》2006,42(11-12):611-617
A mathematical model for separation of suspensions with a non-Newtonian disperse medium by dual-stage pressurized flotation in a cylindrical-conical hydrocyclone is developed. A system of differential equations of the convective diffusion and movement of a complex of particles-bubbles is solved by a numerical method. The concentration field is modeled, and integral separation indicators are determined. Values of structural parameters of the hydrocyclone for which the separation indicators depend heavily on the taper angle of the conical section of the housing and the rheological properties of the disperse medium are established. It is demonstrated that dual-stage pressurized flotation makes it possible to reduce considerably the residual concentration of solid-phase particles as compared with single-stage flotation. 相似文献
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26.
Quasi-static stress fields for a crack inclined to the property gradation in functionally graded materials 总被引:3,自引:0,他引:3
Summary. Quasi-static stress fields for a crack inclined to the direction of property gradation in functionally graded materials (FGMs)
are obtained through an asymptotic analysis coupled with Westergaard's stress function approach. The elastic modulus of the
FGM is assumed to vary exponentially along the gradation direction. The mode mixity due to the inclination of the property
gradient is accommodated in the analysis through superposition of opening and shear modes. The first four terms in the expansion
of the stress field are derived to explicitly bring out the influence of nonhomogeneity on the structure of the stress field.
Using these stress field contours of constant maximum shear stress, constant maximum principal stress, constant first stress
invariant and constant out of plane displacement are generated, and the effect of inclination of the property gradation direction
on these contours is discussed.
Received September 22, 2002
Published online: May 20, 2003
The financial support of National Science Foundation (NSF) under grant no. CMS 99000138 is gratefully acknowledged. 相似文献
27.
28.
V. N. Tsygankov V. V. Safonov A. I. Kozlov V. P. Gavrilov 《Inorganic Materials》2003,39(10):1076-1078
The GeO2–NiO system is studied in the stability range of Ni2GeO4 by temperature-dependent resistivity measurements, in combination with x-ray diffraction, differential thermal analysis, and thermogravimetry. The resistivity of the starting mixtures and heat-treated samples is measured in the composition range 55–90 mol % NiO. The effect of air humidity on the resistivity of the samples is examined. 相似文献
29.
Thomy V. Dubois L. Vanoverschelde C. Sozanski J.P. Pribetich J. 《IEEE sensors journal》2004,4(6):772-778
This paper describes a novel planar antenna sensor created for the purpose of noninvasive temperature measurements using microwave radiometry. In order to improve radiometric measurements in industrial applications, a new generation of sensors is introduced, composed of a metallic sheet. Simulations based upon the method of moments is used both to design and to determine their electromagnetic performances. This paper also describes a radiometric device using these sensors to measure and control the temperature of food products during deep freezing processes. The results and discussions are presented. 相似文献
30.