有机锡催化、无中和水洗合成DOP

以有机锡(Fascat4102)作催化剂,苯酐和辛醇(2-乙基己醇)酯化反应生成邻苯二甲酸二辛酯(DOP),其最佳工艺条件为:酯化温度215～225℃,催化剂加入量2.0‰,过量醇含量17%,脱醇真空为20KPa(绝压),脱醇温度为155℃,活性炭加入量为1‰,省却中和水洗和汽提工序,产品质量可以达到优级品.     

如何掌握印刷压力

<正> 一、印刷压力的概念与作用 印刷的过程,从某种意义上讲,是解决油墨与纸张之间矛盾的过程。要将印版上图文处的油墨转移到承印物上,就必须施加一定的力,即所谓的印刷压力。它在印刷中具有重要的作用。 1.保证粗糙的印刷面完全接触 纸张、橡皮布、印版的表面均成粗糙微孔状。对这些粗糙表面,必须在一定的压力作用下,使其受     

吉林省特大干旱灾害对粮食的影响及其对策

本文通过分析我省历史发生的特大干旱灾害事件，论述了不同时期特大干旱对粮食产量的严重影响。提出了21世纪特大干旱的研究与对策。     

Improvement of RCA transistor using RTA annealing after theformation of interfacial oxide

A polysilicon emitter RCA transistor (an ultra-thin interfacial oxide layer exists between polysilicon and silicon emitter) is presented which can operate at 77 K for the first time. An ultra-thin (1.5 nm) interfacial oxide layer is grown deliberately between polysilicon and silicon emitter using RCA oxidation and excellent device stability is obtained after rapid thermal annealing (RTA) treatment in nitrogen atmosphere. The RCA transistor exhibits good electrical performance at very low temperature for an emitter area of 3 × 8 μm². The maximum toggle frequency of a 1:2 static divider is 1.2 GHz and 732 MHz at 300 K and 77 K, respectively     

对国际岩石力学委员会J_V公式的质疑

通过对国际岩石力学委员会JV 公式的论证 ,指出了该公式不符合数理逻辑。结合工程勘察实践 ,拟建了Ky新公式 ,提高了工程岩体完整程度评价方法的科学性。     

设计从艺术与技术的结合走向艺术与科学的结合

艺术与科学的问题一直是设计界普遍关注的问题之一。技术与艺术的分离与结合，推动了设计的发展，但设计最终必将走向科学与艺术的结合之路。     

四川南桠河一期工程姚河坝水电斜井开挖施工技术浅论

以姚河坝水电站引水隧洞50°倾角、长度为194.734m的斜井开挖为实例,从施工测量、开挖方法、通风防尘、临时支护斜井及安全施工等方面探讨长洞身、大倾角斜井在无爬罐条件下的人工开挖方法.     

熔融-固相缩聚法中固相聚合对聚乳酸合成的影响

以L 乳酸单体为原料 ,熔融 -固相缩聚法合成了聚乳酸 ,重点研究了固相聚合的工艺条件。结果表明 ,绝对压力 60Pa ,氯化亚锡为催化剂 ,分段控温 ,可使聚乳酸的粘均分子量提高到固相聚合反应前的 5 3倍。通过对固相聚合产物的结晶度和熔点的分析 ,探讨了固相聚合的机理。     

Parameters evaluation of SOLA algorithm for time scale modification

Successful operation of the Synchronous Overlap and Add (SOLA) algorithm for Time Scale Modification (TSM) of speech is closely tied to the proper choice of parameters. This paper investigates the quality of time scale modified speech under different values of primary parameters. Based on Mean Opinion Score (MOS) tests and Bark Spectral Distortion (BSD) measure, the proper choices of synthesis shift (Ss) and the duration of the shift search interval (K _max?) are given experimentally. The conclusions can be helpful for operating the SOLA algorithm for time scale modification of speech.     

Robust Distributed Source Coding

We consider a distributed source coding system in which several observations must be encoded separately and communicated to the decoder by using limited transmission rate. We introduce a robust distributed coding scheme which flexibly trades off between system robustness and compression efficiency. The optimality of this coding scheme is proved for various special cases.