IrO2-pH微电极的研制及钢筋/混凝土界面pH的测量

采用电化学阳极氧化和高温碳酸盐氧化两种方法制备 IrO2-pH微电极，其特点是对氢离子响应快、线性范围宽、机械性能好、具有长期稳定性 .考察了该电极的pH响应特性、化学成分、机械性能等.结果表明，这种IrO2-pH微电极 适用于钢筋/混凝土界面pH值的原位测量.     

钢铁酸洗时氢致裂开危险性检测新技术的研究

研究了一种新型的原子氢渗透速率测量传感器在酸洗液中的测量信号与A3钢在相应体系中的强度/脆性之间的对应关系,为发展钢铁酸洗除锈除垢时在线检测氢致腐蚀裂开危险性的智能化新技术,提供了软件设计的部分关键参数与判据。     

A3钢焊缝区在酸性介质中氢致腐蚀裂开行为的研究

本文应用慢应变速率拉伸试验法、金相和扫描电镜技术研究了带焊缝的A3钢试样在会缓蚀剂的盐酸溶液中的氢致腐蚀裂开行为。结果表明,在酸液中带焊缝试样的断裂均发生在热影响区;带焊缝A3钢试样的脆断敏感程度显著高于其母材;缓蚀剂的添加可以较大程度地改变带焊缝材料的脆断敏感性。     

Intelligent optimal control for lead-zinc sintering process state

The intelligent integrated predictive model of synthetical permeability was established using the fuzzy classifier to combine the time sequence predictive model with the craftwork parameter predictive model. Then, the estimation model of bum-through point（BTP） based on pipe stress point（PSP） method and the predictive model of BTP were proposed. The optimal control of permeability and heat states was implemented by using the fuzzy expert controller with self-studying mechanism. The application of the intelligent control technique suppresses 17% of the fluctuation of synthetical permeability and 12% of the fluctuation of BTP, stabilizes the output and quality of sinter and settles the basis for the optimization of output and quality of sintering process.     

Dependence of dielectric properties on BT particle size in EP/BT composites

The polymer-ceramic composites of epoxy resin (EP) and barium titanate (BT) were prepared.BT powders of different BT particle sizes from 100 nm to 1 μm were used in the preparation.The dielectric properties, such as dielectric constant, dielectric loss and electrical breakdown strength, of the EP/BT composites were studied.The morphology of the composites was characterized by the means of scanning electron microscopy (SEM).The results show that the dielectric constant of the composites is much higher than the epoxy matrix at frequency range from 1 kHz to 10 MHz, and it is also obviously dependent on the size of BT particles.The electrical breakdown strength of the composites decreases with the increase of the BT content.The dependence of electrical breakdown strength on BT particle sizes was also discussed.     

异形坯连铸坯壳应力与鼓肚变形分析

坯壳应力引起的鼓肚变形是影响铸坯质量的重要因素,为防止过大的鼓肚变形,依据湍动能理论、热流传递理论和粘弹性理论,建立了异形坯三维热-力耦合模型,开发了鼓肚分析软件,从而避免了漏钢事故的发生.该模型将温度场和应力场的计算相互耦合,交替进行.结果表明:异形坯截面最危险点位于腹板中部,其次为翼板中点,在两者相结合的圆角部,由于凝固坯壳比较薄,其应力值也比较大;当坯壳厚度小于20 mm时,两点的鼓肚变形量将分别超过其极限变形量,铸坯出结晶器时必然发生漏钢事故.该模型通过预测坯壳应力和鼓肚变形量为现场安全生产提供了理论依据.     

La在KCl-NaCl和LaCl_3-KCl-NaCl熔体中的溶解行为SCIEI

本文利用透明槽技术、电化学循环V-A法及量子化学EHMO三种方法,研究了La在KCl-NaCl(1:1mol)及LaCl_3-KCl-NaCl熔体中的溶解行为。初步认为:溶解在KCl-NaCl熔体中的La是以中性金属状态存在。在LaCl_3-KCl-NaCl熔体中,溶解的La与La^(3+)作用生成低价La^(2+)离子,La^(2+)又与周围的La^(3+)作用形成原子簇离子La_m^(n+)赋存于熔体之中。     

小波分析与漏磁检测信号处理

详细介绍了小波分析的基本理论,并将其引入到钢管漏磁探伤信号的分析中,可以去除噪声、压缩数据和检测奇异性,而且为缺陷的定性和定量分析提供了新的判定方法.     

水基淬火液用于汽车轴管零件的淬火冷却

在分析几种淬火液的基础上 ,选用冷却速度与快速淬火油相近的FEROQUENCH 2 0 0 0淬火液用于轴管淬火冷却 ,淬火后的轴管彻底消除了淬火裂纹 ,而且改善该零件热处理后的力学性能。