挤压力对晶体生长速度及枝晶间距的影响

研究了挤压铸造时挤压力对宏观晶体生长速度的影响，给出了晶体生长速度表达式。结果表明：挤压力对合金宏观晶体生长速度的影响除与合金成分有关外，在某些挤压条件下，当形核率的增加幅度超过长大速度时，则挤压力可使宏观晶粒细化；反之，会使宏观晶粒变粗。随着挤压力的提高，合金凝固速度加快，一次枝晶间距和二次枝晶间距都随之减小，从而细化了树枝晶。     

Dy3+激活的几种硼酸盐在VUV-VIS范围的光谱性质

本文报道了SrAl2B2o7:Dy^3 、BaAl2B2O7:Dy^3 、SrAl3BO7:Dy^3 、La2CaB10O19:Dy^3 的紫外－真空紫外（UV－VUV）激发光谱和UV激发下的发射光谱。根据发射光谱讨论了Dy^3 离子在这几种基质中发光的黄蓝比（Y／B）。在VUV激发光谱中推测了Dy^3 的f-d跃迁及电荷迁移态（CTS）和基质吸收的位置。     

混凝土渠道糙率原型观测

糙率是渠道水力设计的关键技术参数之一，其值的准确选取决于已建工程原型观测成果的类比。选择3条不同衬砌特性的混凝土渠道进行糙率原型观测，对观测方法及步骤做了较详细描述；计算出了3条渠道的糙率，对其存在误差进行了分析探讨，可为今后进一步开展相关课题研究积累经验并供同行参考。     

小型雷管生产工艺方法与质量保证措施

小型雷管的结构特点是体积小，装药量少．要保证小型雷管在传爆序列中可靠作用．除设计时已确定的结构形式、装压药条件、管壳材料等关键技术外，生产过程中工艺方法不同对产品质量具有不同的影响．本文从装药、压药、退模三道工序选用不同的工艺方法和设备对小型雷管装配生产质量的影响进行了对比分析，从而找出了最佳的生产工艺方法．并提出了相应的质量保证措施。     

复合绝缘子老化评估方法浅析

复合绝缘子老化是用户十分关心的问题。笔者介绍了两种判别复合绝缘子老化程度的方法,并通过实例,分析了这两种方法的优点以及存在的问题。     

论坛消息的语义漂移分析

引入多维文档模型来组织论坛消息的描述性特征和语义性特征，并在多维索引的基础上，提出了加窗分析技术。目的在于分析论坛站点中语义漂移现象，进而发现论坛中的完整语义信息单元。     

在役超高压水晶釜主要检测方法

介绍了在役超高压水晶釜的常见缺陷以及应用超声波探伤、磁粉探伤、金相分析等无损检测方法对其进行在役检验的要点.     

A new efficient method for one‐pot conversions of aryl carboxylic acids into nitriles without solvent

A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry     

Facile modifications of polyimide via chloromethylation: II. Synthesis and characterization of thermocurable transparent polyimide having methylene acrylate side groups

From chloromethylated polyimide, a useful starting material for modification of aromatic polyimides, a thermocurable transparent polyimide having acrylate side groups was prepared. In the presence of 1,8‐diazabicyclo[5,4,0]undec‐7‐ene, chloromethylated polyimide was esterified with acrylic acid to synthesize poly(imide methylene acrylate). The polymer was soluble in organic solvent, which makes it possible to prepare a planar film by spin coating. The polymer film became insoluble after thermal treatment at 230 °C for 30 min. Optical transparency of the film at 400 nm (for 1 µm thickness) was higher than 98 % and not affected by further heating at 230 °C for 250 min. Adhesion properties measured by the ASTM D3359‐B method ranged from 4B to 5B. Preliminary results of planarization testing showed a high degree of planarization (DOP) value (>0.53). These properties demonstrate that poly(imide methylene acrylate) could be utilized as a thermocurable transparent material in fabricating display devices such as TFT‐LCD. Copyright © 2004 Society of Chemical Industry     

第二代反坦克导弹射击训练计算机成绩评定方法

文中应用数理统计方法并结合教学及实弹射击实践,提出了在第二代反坦克导弹模拟训练器材中实现智能化评定射击训练成绩的主要方法.