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21.
Lu Shen Beng Jit Tan William S. Willis Francis S. Galasso Steven L. Suib 《Journal of the American Ceramic Society》1994,77(4):1011-1016
Amorphous boron nitride thin coatings (∼0.2 μm) have been formed on Nicalon and C-Nicaion (pre-carbon-coated Nicalon) yarns via dip coating in boric acid solution followed by heating and nitriding in NH3 gas at 1000°C. X-ray photoelectron spectroscopy (XPS) and Auger electron spec-troscopy (AES) studies have shown the formation of boron nitride. The coating was boron rich and contains oxygen. The N/B and O/B ratios range from 0.6 to 0.8 and from 0.1 to 0.25, respectively. Tensile strength measurements revealed that the BN-coated C-Nicalon yarn maintained ∼85% of its original strength while BN-coated Nicalon lost ∼85% of its original strength. Auger depth profiles showed that there was a consumption of carbon during the heating and nitridation process for both BN-coated Nicalon and C-Nicalon fibers. However, the depletion of carbon in BN-coated Nicalon fibers was much more severe than that in BN-coated C-Nicalon fibers. 相似文献
22.
RA Francis 《Canadian Metallurgical Quarterly》1996,93(11):685-686
23.
John S. Wright Joseph M. Schwartz Lanny D. Schmidt Lorraine Falter Francis 《Journal of the American Ceramic Society》1995,78(9):2360-2366
The crystalline phase development and microstructural changes with heating of sol-gel-derived lead titanate (PT) particles and films on silica with and without a fugitive (or removable) diffusion barrier layer were investigated. Amorphous gel-derived PT particles were deposited on SiO2 -coated TEM grids with and without polyimide (PI) or carbon barrier layers between SiO2 and PT. TEM analysis showed that PI or carbon barriers prevented reaction between the gel-derived PT particles and SiO2 . PT particles crystallize and then the PI or carbon film decomposes. Sol-gel-derived PT films were deposited on oxidized Si substrates (Si/SiO2 ) with and without a PI barrier layer. Perovskite PT films were prepared on Si/SiO2 substrates with a PI barrier; however, some porosity remained in the films. Identically prepared films without the PI barrier formed a mixture of pyrochlore and perovskite. X-ray photoelectron spectroscopy results indicate that the PI film pre- vents the diffusion of Si into the PT film. 相似文献
24.
Songhua Xu Haisheng Tan Xiantao Jiao Francis C.M. Lau Yunhe Pan 《Computer Graphics Forum》2007,26(3):609-618
We propose a generic pigment model suitable for digital painting in a wide range of genres including traditional Chinese painting and water-based painting. The model embodies a simulation of the pigment-water solution and its interaction with the brush and the paper at the level of pigment particles; such a level of detail is needed for achieving highly intricate effects by the artist. The simulation covers pigment diffusion and sorption processes at the paper surface, and aspects of pigment particle deposition on the paper. We follow rules and formulations from quantitative studies of adsorption and diffusion processes in surface chemistry and the textile industry. The result is a pigment model that spans a continuum from the very wet to the very dry brush stroke effects. We also propose a new pigment mixing method based on machine learning techniques to emulate pigment mixing in real life as well as to support the creation of new artificial pigments. To experiment with the proposed model, we embedded the model in a sophisticated digital brush system. The combined system exhibits interactive speed on a modest PC platform. http://www.cs.hku.hk/~songhua/pigment provides supplementary materials for this paper. 相似文献
25.
Kofi E. Aidoo Richard F. Tester Janet E. Morrison & David MacFarlane 《International Journal of Food Science & Technology》1996,31(5):433-438
Composition and microbiological contamination was measured in samples of pre-packed dates purchased from a number of stores and retail outlets in Greater Glasgow. The sugar content of dried pitted dates was c . 74%, about 10% more than reported on those packs where nutritional information was given. Potentially pathogenic bacteria like Escherichia coli, Staphylococcus aureus and Bacillus cereus were identified in some of the samples together with lactic acid bacteria, yeasts and moulds, Aspergillus flavus and A. parasiticus . Fresh dates were the most heavily contaminated of all samples, probably owing to the high moisture content. 相似文献
26.
Three months after the launch of the MMR programme in the United Kingdom and the Republic of Ireland, a postal questionnaire was sent to all GP scheme trainees in both Northern Ireland and the Republic of Ireland. The response rate was 81%. All trainees were enthusiastic about promoting MMR immunisation; with 27% favouring compulsory immunisation. 9% had never seen a patient with measles. This did not alter their attitude towards the beneficial effects of MMR immunisation. Of pre-practice year trainees 26% felt their level of knowledge of immunisation was inadequate, 59% claimed to have received no education on immunisation during their vocational training to date. This may reflects deficiencies in their medical curriculum to-date. 95% of third-year trainees indicated that their practice experience had been the source of at least some of their education on immunisation. Only 46% of trainees in the Republic of Ireland were aware of their Department of Health's aims in launching the MMR immunisation campaign. 相似文献
27.
Rheological Property and Stress Development during Drying of Tape-Cast Ceramic Layers 总被引:1,自引:0,他引:1
Jennifer A. Lewis Kimberly A. Blackman rea L. Ogden James A. Payne Lorraine F. Francis 《Journal of the American Ceramic Society》1996,79(12):3225-3234
Rheological property and stress development of tape-cast ceramic layers derived from nonaqueous alumina (A12 O3 )-poly(vinyl butyral) (PVB) suspensions were observed during drying. Casting suspensions exhibited strong shear-thinning behavior, with a low shear Newtonian plateau apparent viscosity >102 Pa. s. The apparent suspension viscosity displayed a power-law dependence on the A12 O3 volume fraction during the initial stage of drying (<30% solvent loss). Stress development, measured by a cantilever deflection method, and parallel weight loss measurements were performed during the drying of tape-cast layers and pure binder coatings. Maximum drying stresses (σmax ) of 1.37-0.77 MPa were observed for plasticized tapes cast at gap heights of 150-400 μm. In contrast, nonplasticized tapes of similar thickness displayed a more gradual stress increase, with σmax values approximately an order of magnitude higher than their plasticized counterparts. The stress histories of the corresponding binder coatings were quite similar to the tape-cast layers, albeit slightly lower σ max values were observed. Stresses decayed beyond σmax with a logarithmic time dependence to an almost constant value of 0.2-0.4 MPa for the plasticized tapes. Based on these observations, process methodologies have been offered to minimize stress development and retention in tape-cast ceramic layers 相似文献
28.
The reactions of two sets of lignin model compounds over a sulfided CoOMoO3/γ-Al2O3 catalyst were studied. The first set mimicked lignin methoxyphenol residues and comprised 4-methyl-guaiacol, 4-methyl catechol, eugenol and vanillin. Deoxygenation and hydrogenation were facile and led to ultimate molar yields of single-ring products as high as 0.70. The selectivity to single-ring products increased with increases in temperature, o-hydroxydiphenylmethane, phenyl ether and o,o'-biphenol constituted the second set that mimicked thermally stable lignin bonds.Fragmentation of o-hydroxydiphenylmethane and phenyl ether occurred readily; o,o'-biphenol reacted to dibenzofuran.
These results suggest that the single-ring products obtained from catalytic liquefaction of lignins should be more desirable than those obtained from pyrolysis because of both higher yields and reduced complexity. 相似文献
These results suggest that the single-ring products obtained from catalytic liquefaction of lignins should be more desirable than those obtained from pyrolysis because of both higher yields and reduced complexity. 相似文献
29.
JH Noseworthy P O'Brien BJ Erickson D Lee D Sneve GC Ebers GP Rice A Auty WJ Hader A Kirk P Duquette J Carter G Francis L Metz E Shuster 《Canadian Metallurgical Quarterly》1998,51(5):1342-1352
OBJECTIVE: To determine whether sulfasalazine is better than placebo in slowing disability progression in MS. METHODS: In this randomized, double-blind, placebo-controlled phase III trial, 199 patients with active relapsing-remitting (n = 151) or progressive (n = 48) MS were evaluated at 3-month intervals for a minimum of 3 years (94% completed 3 years of follow-up; mean follow-up, 3.7 years). MRI studies were performed at 6-month intervals on a subset of 89 patients. RESULTS: Sulfasalazine failed to slow or prevent disability progression as measured by the primary outcome (confirmed worsening of the Expanded Disability Status Scale [EDSS] score by at least 1.0 point on two consecutive 3-month visits). Sulfasalazine influenced favorably a number of secondary outcomes during the first 18 months of the trial (e.g., annualized relapse rate, proportion of relapse-free patients; progressive subgroup only: rate of EDSS progression at 1 and 2 years, median time to EDSS progression) but these positive findings were not sustained into the second half of the trial. CONCLUSIONS: Sulfasalazine does not prevent EDSS score progression in the subset of MS patients studied by this protocol. Treatments may improve relapse-related outcomes in MS, at least temporarily, without providing sustained slowing of EDSS progression. Phase III MS trials should be of sufficient length to determine a meaningful impact on disease course. 相似文献
30.
Given two processes, each having a total-ordered set ofn elements, we present a distributed algorithm for finding median of these 2n elements using no more than logn +O(logn) messages, but if the elements are distinct, only logn +O(1) messages will be required. The communication complexity of our algorithm is better than the previously known result which takes 2 logn messages. 相似文献