稀土锆酸盐的制备和热膨胀性能

采用固相反应法制备了稀土锆酸盐材料.通过XRD图谱和SEM对材料的显微结构进行分析,并测试了不同温度下材料的热膨胀系数.结果表明稀土锆酸盐材料的热膨胀系数大约为11×10-6/℃,其值随着温度的升高而升高,升高的速率逐渐减小.随着原子序数的增大,热膨胀系数是逐渐减小的,这说明稀土锆酸盐材料的热稳定性是随着原子序数的增大逐渐增强的.     

液压伺服系统常用的干扰抑制方法

本文介绍了目前常见的抑制干扰的几种方法，分析了它们各自的特点和适用范围，为合理选择不同抑制干扰的方法提出了一些参考意见。     

In situ technique for synthesizing multiple ceramic particulates reinforced titanium matrix composites (TiB + TiC + Y2O3)/Ti

In situ synthesized titanium matrix composites reinforced with multiple ceramic particulates including TiB, TiC and Y₂O₃ were fabricated by non-consumable arc-melting technique utilizing the chemical reaction among Ti, B₂O₃, B₄C and Y. The thermodynamic feasibility of the in situ reactions has been considered. X-ray diffraction (XRD) was used to identify the phases in the composites. Microstructures of the composites were observed by means of optical microscope (OM), scanning electron microscope (SEM) and electron probe. It is concluded that multiple reinforcements are synthesized and they show different shapes: TiB grows in needle shape; TiC grows in near-equiaxed and rod-like shapes; Y₂O₃ grows in near-equiaxed shapes when the content of Y is 0.6 wt.% and grows in dendritic shapes when the content of Y increases to 1.8 wt.%. Reinforcements TiB, TiC and Y₂O₃ are distributed uniformly in the titanium matrix.     

CALCULATION OF TRANSFORMATION VOLUME FRACTION TO HQ590 HOT ROLLED STRIP STEEL DURING CONTINUOUS COOLING

On the basis of phase transformation kinetics, the transformation of γ→α,P,B have been investigated through considering the effect of deformation. The calculation methods of volume fraction have also been given. Comparing with common method, the simulated results are in more agreement with experiment results.     

新型缓蚀剂TG500在高CO2和Cl-环境中的缓蚀行为

在高温高压高CO2和Cl^-环境中，用静态高温高压模拟试验方法对不同浓度的TGS00新型咪唑啉季铵盐缓蚀剂进行了缓蚀效率测试．结果表明，TGS00缓蚀效率随加入量增加而增加，浓度增加到0．3g／L后，缓蚀速率提高不明显．同时研究N80套管钢表面的腐蚀产物，缓蚀剂浓度较低时，以均匀腐蚀为主，加入量提高到0．3g／L时，除局部少量点蚀外，无其它明显腐蚀特征．     

PLC在六关节工业机器人控制中的设计应用

本文介绍了应用可编程控制器PLC对六关节工业机器人进行位置控制的方法及其软件硬件系统的设计与实现。     

EFFECT OF RESIDUAL STRESS ON THE MARTENSITIC TRANSFORMATION OF SPUTTER-DEPOSITED SMA THIN FILMS

TiNi thin films were sputter-deposited on circular single-cry stal silicon substrates un-der various sputtering parameters. The crystal structure and residual stress of the as-deposited films were determined by X-ray diffraction and substrate-curvature method. The phenomenon of stress-suppressed martensitic transformation was observed. R is considered that the residual stresses in SMA thin films based on circular substrates act as balanced biaxial tensile stresses. The status of equilibrant delays the align-ment of self-accommodated variants and the volume shrinkage during the martensitic transformation.     

THEORETICAL INVESTIGATION ON BY-ONLY-CURRENT ELECTROMAGNETIC SEPARATION OF INCLUSION FROM MOLTEN METALS

The electromagnetic field under applied AC and DC current in round and rectangular pipe was systematically investigated, then a concept of "equivalent current density" was proposed for evaluating the inhomogeneous electromagnetic pinch force, and the mono-component removal efficiency and the overall removal efficiency of inclusion were formulated. It is founded that flat pipe is superior to round pipe for the electromagnetic removal of inclusion, and DC current can get a higher removal efficiency than A C current due to absence of skin phenomenon. Under usual condition, a removal efficiency of 52% for 10μm inclusion or more than 92% for 20μm inclusion can be achieved by imposing a current density of 3×106A/m2 in a flat pipe.     

A STUDY OF B-P UNIFIED VISCOPLASTIC CONSTITUTIVE MODEL

By combining the Bodner-Partom constitutive model and equivalent stress function, finite element methods and program on analyzing non-elastic deformation and stress for thermal viscoplastic material are studied in this paper, and it's the first time that this material model is used in a kind of engineering software-MARC. Thermal viscoplastic behavior of high temperature alloy GH536 specimen with gap is analyzed by this program. The research results show it is feasible to analyze thermal viscoplastic behavior of specimen or structure by applying B-P model.     

Effect of laser fluences on the structure of carbon nitride films deposited by direct current plasma assisted pulsed laser ablation

Carbon nitride films were deposited by direct current plasma assisted pulsed laser ablation of a graphite target under a nitrogen atmosphere at room temperature. The surface morphology, composition and bonding structure of the deposited films were characterized by atomic force microscopy (AFM), Fourier transform infrared (FTIR) spectroscopy, Raman, and X-ray photoelectron spectroscopy (XPS). The effect of laser fluences in the range 0.5–3 J/cm² on the surface morphology, composition and bonding structure of the carbon nitride films were systematically studied. As laser fluence is increased, AFM results show a great decrease in the surface roughness of carbon nitride films. FTIR and XPS results indicate an increase in the N/C ratio and the content of N atoms bonded to sp³ C, as well as a decrease in the content of H atoms and the content of N atoms boned to sp² C in the deposited films, and Raman spectra indicate an increase in the content of disordered sp² C atoms and the sp² cluster size. The increase in the film density and the decrease in the particle fraction contribute to the decrease of surface roughness with increasing laser fluence.