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991.
砂带用酚醛树脂粘合剂的合成研究 总被引:1,自引:0,他引:1
本文讨论了砂带用酚醛树脂粘合剂的合成工艺和条件。研究了反应投料比,温度及增塑剂对反应过程和树脂性能的影响。磨削性能证明合成树脂性能良好。 相似文献
992.
We prepared poly(p‐phenylene pyromellitimide) (PMDA–PDA), poly(p‐phenylene 4,4′‐hexafluoroisopropylidene diphthalimide), and their copolyimides with various compositions to explore the relationship between the water sorption and structure. The water sorption behaviors were gravimetrically investigated as a function of composition and temperature and interpreted with a Fickian diffusion model in films. Overall, the water sorption behaviors were strongly dependent on the changes in morphological structure, which originated from the variations in composition. When the content of the bulky hexafluoroisopropylidene group (6FDA) was increased, the water uptake decreased from 5.80 to 3.18 wt %, whereas the diffusion coefficient increased from 3.6 × 10?10 to 11.3 × 10?10 cm2/s. The relatively high water uptake in the PMDA–PDA polyimide film was successfully healed by the incorporation of 6FDA, which may have resulted from the increases in the intermolecular packing order and hydrophobicity. The degree of orientation and crystallinity, which are in‐plane characteristics, were directly correlated to the diffusion coefficient and activation energy in the polyimide film. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 3442–3446, 2003 相似文献
993.
Huabin Wang Derek O. Northwood Jiecai Han Shanyi Du 《Journal of the American Ceramic Society》2006,89(2):501-508
AlN–SiC solid solution particles with a variety of morphologies including faceted polyhedrons with or without ledges; hexagonal platelets; hexagonal columns with a hexagonal plate or a pyramidal cap; and interpenetrating cones, have been found in the combustion products of a mixture of Al, Si, and carbon black under a nitrogen pressure of 10 MPa. Combustion temperature (the growth temperature of crystals) is the most important factor controlling the morphology of crystals formed in the combustion product. When temperatures are close to the melting point of the solid solutions, a small driving force for nucleation and long distances of surface migration make nucleation on the basal plane difficult, and thus the solid solution particles tend to grow as platelets. Supersaturation is the second key factor influencing crystal growth. At relatively low temperatures, a low supersaturation at the large pores renders nucleation difficult and the solid solution particles tend to grow as platelets. At relatively low temperatures and high supersaturation, a relatively high driving force for nucleation and short mean distances of surface migration promote the growth of AlN–SiC solid solutions as polyhedrons. The formation of the ledges on the polyhedral particles is attributed to the differences in the evaporation rates and the deposition rates between Al and Si. At relatively low temperatures and an intermediate supersaturation, the solid solution particles grow as prismatic columns. The formation of the prismatic columns with a hexagonal plate, or a pyramidal cap, is attributed to a sudden change of temperature during combustion. A possible growth mechanism for the AlN–SiC solid solution cones is proposed. 相似文献
994.
为正确有效地分割出髋关节的外轮廓,提出了一种基于最佳分割线的股骨近端外轮廓的提取方法。该方法利用自底向上CT序列图像的帧间相似性找到一条分割目标股骨与其他骨骼的闭合分割线,从而利用该分割线来精确定位目标骨骼的位置,并搜索边缘点。实验结果表明,该方法能够准确地识别出股骨近端的外轮廓,自适应强,抗干扰性好。 相似文献
995.
996.
A wireless sensor network (WSN) commonly whilst a body sensor network (BSN) must be secured with requires lower level security for public information gathering, strong authenticity to protect personal health information. In this paper, some practical problems with the message authentication codes (MACs), which were proposed in the popular security architectures for WSNs, are reconsidered. The analysis shows that the recommended MACs for WSNs, e.g., CBC- MAC (TinySec), OCB-MAC (MiniSec), and XCBC-MAC (SenSee), might not be exactly suitable for BSNs. Particularly an existential forgery attack is elaborated on XCBC-MAC. Considering the hardware limitations of BSNs, we propose a new family of tunable lightweight MAC based on the PRESENT block cipher. The first scheme, which is named TukP, is a new lightweight MAC with 64-bit output range. The second scheme, which is named TuLP-128, is a 128-bit variant which provides a higher resistance against internal collisions. Compared with the existing schemes, our lightweight MACs are both time and resource efficient on hardware-constrained devices. 相似文献
997.
Rheological behavior of dispersed two-phase polymer melts has been investigated by means of a capillary rheometer. The two-phase systems chosen for study were blends of two polymers: high-density polyethylene and polystyrene, which are incompatible in the molten state. In order to investigate the state of dispersion, photographs were taken of the microstructure of extrudate samples, showing that the polystyrene forms long fibers or droplets as a discrete phase dispersed in the polyethylene which forms a continuous phase. Measurements were made of the axial pressure distributions of the two-phase molten polymers flowing through circular tubes, which permit one, according to the theory advanced by Han, to determine viscous and elastic properties of the melts. Also measured was melt die swell ratio. It has been found from the two independent experimental techniques that there exist a maximum and/or minimum elastic property at a certain blending ratio, and that the elastic property decreases first with L/D ratio of a capillary and then levels off. 相似文献
998.
999.
Do‐Hung Han Jae‐Hyuk Jang Hye‐Young Kim Byung‐Nam Kim Boo‐Young Shin 《Polymer Engineering and Science》2006,46(4):431-437
The high melt viscosity of polypropylene was studied by grafting bifunctional monomers, 1,6‐hexanediol diacrylate (HDDA) and tripropylene glycol diacrylate (TPGDA), onto homopolypropylene (HPP) and random ter‐polypropylene (RTPP) under electron‐beam irradiation. Creation of the high‐melt‐viscosity polypropylene was possible at low radiation dosage and low monomer content, under a prohibition of both radiation degradation and homopolymerization. TPGDA monomer was more effective in increasing the melt viscosity of HPP compared with RTPP, whereas HDDA monomer was more effective for enhancing the melt viscosity of RTPP. Such different effects of monomers on melt viscosity may arise from different monomer structures, namely, TPGDA has additional three methyl groups, but HDDA has no methyl groups. Electron‐beam radiation technology, on an increase of the melt viscosity, was much more effective in HPP than RTPP, when compared with virgin polymers. Modified RTPP and HPP with high melt viscosity were capable of foaming with numerous fine cells, of which the modified HPP with 1.5 mmol TPGDA and 0.5 kGy could create more spherical foam cells and its bending strength was 1.5 times more than that of the foamed RTPP. POLYM. ENG. SCI., 46:431–437, 2006. © 2006 Society of Plastics Engineers. 相似文献
1000.