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排序方式: 共有648条查询结果,搜索用时 15 毫秒
31.
Jean‐Thomas Fonné Ekaterina Burov Emmanuelle Gouillart Sergey Grachev Hervé Montigaud Damien Vandembroucq 《Journal of the American Ceramic Society》2018,101(4):1516-1525
Interdiffusion processes between aluminum enriched PVD‐sputtered silica thin films and industrial float soda‐lime silicate glass substrates are quantitatively studied using SIMS analysis. Heat treatments are performed at temperatures close or above the glass transition temperature of the float glass. Aluminum doping of the film is shown to strongly increase the migration of alkali from the glass substrate to the silica thin film. In particular the final alkali content in the film exhibits a linear scaling with the aluminum concentration. An interdiffusion process is evidenced between bulk alkali ions and protons originating from a significant water content in the as‐deposited silica film. Experimental measurements of sodium concentration are shown to be consistent with a simple thermodynamic model based on the equilibration of the activity of sodium between the film and the glass substrate. 相似文献
32.
Performance of selected anion exchange resins for the treatment of a high DOC content surface water 总被引:4,自引:0,他引:4
The objective of this study was first to compare the performance of four strong anion exchange resins (AERs) (MIEX from Orica Pty Ltd, DOWEX-11 and DOWEX-MSA from DOW chemical and IRA-938 from Rohm and Haas) for their application in drinking water treatment (natural organic matter (NOM), mineral anions (nitrate, sulfate and bromide) and pesticide removal) using bench-scale experimental procedures on a high DOC content surface water. The efficiency of MIEX for NOM and mineral anions removal was furthermore evaluated using bench-scale dose-response experiments on raw, clarified and post-ozonated waters. NOM removal was assessed using the measurement of dissolved organic carbon (DOC), UV absorbance at 254 nm (UV254) and the use of high-performance size exclusion chromatography with UV (HPSEC/UV) and fluorescence detection (HPSEC/FLUO). The MIEX and IRA938 anionic resins exhibit a faster removal of NOM and mineral anions compared to the DOWEX11 and MSA AERs. All the resins were found to be very effective with similar performances after 30 to 45 min of contact time. As expected, only limited sorption of atrazine and isoproturon (C0=1 microg/L) occurred with MIEX, DOWEX11 and MSA AERs. MIEX resin proved to be very efficient in eliminating NOM of high-molecular weight but also a large part of the smallest UV absorbing organic compounds which were refractory to coagulation/flocculation treatment. Remaining DOC levels after 30 min of contact with MIEX were found similar in raw water, clarified water and even post-ozonated water implying no DOC benefit can be gained by employing conventional treatment prior to MIEX treatment. Removal of bromide (initial concentration 110 microg/L) was also observed and ranged from 30% to 65% for resin dose increasing from 2 to 8 mL/L. T 相似文献
33.
Mechanochemical degradation of poly(vinyl fluoride) by sodium hydroxide measured by microindentation
Mohamad Alchikh Christophe Fond Yves Frère Hervé Pelletier 《Journal of Materials Science》2010,45(9):2311-2316
The degradation of the mechanical properties of deformed PVDF during its mechanochemical ageing in sodium hydroxide (soda) was followed by microindentation measurements, especially the local reduction of the elastic modulus and the hardness. This allows measurements on a local scale of the mechanical properties on the surface and in-depth as a function of the strain level and the ageing time. Microindentation tests with Berkovich indenter have been performed with a Nanoindenter XP® (MTS). Measurements are made at penetration depth less than 2 μm for an applied load of 10 mN. During ageing in soda (Ph 14) at 90 °C up to 16 days, various deformations ε (0, 22 and 38%) are imposed on PVDF tensile specimen. For the first two imposed deformations (ε = 0 and ε = 22%), mechanical degradation is limited to some percent (less than 7%). For the greatest deformation (ε = 38%), mechanical degradation continues to decrease with ageing time (more than 21%). Microindentation tests show that a range of low deformations exists in which the mechanochemical degradation is limited and no limitation is observed for larger imposed deformation. 相似文献
34.
German Castillo Hervé Wargnier Michel Danis Yves Brechet 《Advanced Engineering Materials》2009,11(11):938-944
After translation, the first stages traditionally involved in the materials selection are filtration and classification, which require formulation of criteria (constraints or objectives) deduced from information written in the set of material requirements. These criteria, which are representative of the behavior of the material and the studied structure, must be formulated analytically in order to be used during selection stage. However, for complex behavior, analytical processing of models is no longer possible and it can be replaced by a combination of numerical resolution methods and an optimization method which make it possible to obtain approximate formal expressions of the criteria. In this paper, a complete selection method is proposed. The method is applied to the constraints as well as the objectives, in order to carry out the filtration and classification stages at the same time. The study of the thermomechanical behavior of a machine tool frame has been used to demonstrate the validity of the proposed method. 相似文献
35.
A liquid-cell shearing interferometer was developed to measure refractive-index variations (delta n) in transparent materials. The cell was filled with a liquid having a matched refractive index. The achieved resolution was better than 1/1000 of a fringe shift and resulted in a delta n measurement sensitivity down to 10(-7) for 1-mm-thick samples. A refractive-index increment in photothermorefractive glass of up to 5 x 10(-6) was observed after UV exposure at 325 nm. A refractive-index decrement of up to 1 x 10(-3) was observed after thermal development of the exposed sample. It was proved that photothermorefractive glass obeys the reciprocity law; i.e., delta n depends on the UV dosage but does not depend on the irradiance. 相似文献
36.
37.
New compounds MIIThNb2O8 with MII = Ca, Sr, Cd, and CaUNb2O8 have been prepared by solid state reaction. These compounds isotypic with the rare-earth niobates LnNbO4 cristallize in a monoclinic system with space group I2/c. Like the niobates LnNbO4, they present a displacive and non quenchable transition (monoclinic to tetragonal) which is probably of second order. 相似文献
38.
A pseudojoint estimation of time scale and time delay between an unknown deterministic transient type signal and a reference signal is proposed. The method is based on the separation between the estimations of the two dependent parameters. The time autocorrelation function (TACF) preserves the time scale and is invariant with respect to the time delay between the signals. The time scale factor can, thus, be estimated independently from time delay using the TACFs of the two signals. After estimating the time scale factor, the signal can be scaled by the estimated amount. The time delay is then estimated without bias due to the time scale factor. To obtain high resolution joint estimates, the time scale factor is estimated in the scale domain from the scale transforms of the TACFs of the two signals. The proposed method has low computational cost. Moreover, the results on synthetic signals show good performance of the method with respect to the Cramér-Rao Lower Bound and the joint Maximum Likelihood Estimation. A possible application of the technique to the analysis of electromyogram (EMG) signals detected during electrically elicited contractions is also presented. In a few representative cases, it is shown that the time scale estimate reveals myoelectric manifestations of muscle fatigue and is less affected by M-wave truncation than spectral EMG attributes. 相似文献
39.
In order to face new regulation directives regarding the environment and also for improving their customer relationship, enterprises
have to increasingly be more able to manage their product information during the entire lifecycle. One of the objectives among
others in this paper is to deal with product traceability along the product lifecycle. To meet this objective, the information
system has to be designed and, further built in such a way all information regarding products is recorded. The IEC 62264 standards
define generic logical models for exchanging product and process information between business and manufacturing levels of
enterprise applications. Thus, it can be a base for product information traceability. However, its complexity comes from the
fact it mixes conceptual and implementation details while no methodology exists that defines how to instantiate it. Product
traceability is then needed to increase its abstraction level in order to concentrate on its concepts and managing its application
by providing a methodology for its instantiation. In this paper, we propose to map the IEC 62264 standard models to a particular
view of Zachman framework in order to make the framework concrete as a guideline for applying the standard and for providing
the key players in information systems design with a methodology to use the standard for traceability purposes. 相似文献
40.
Harunori Yoshikawa Pascal Kurowski Philippe Petitjeans Farzam Zoueshtiagh Hervé Caps 《Microgravity science and technology》2007,19(3-4):155-156
The response of an air bubble surrounded by a liquid in a sealed cell submitted to vibrations was investigated experimentally under microgravity conditions and compared to experiments under normal gravity conditions. As in normal gravity [1], it was observed that the bubble split into smaller parts when the acceleration of the vibrations reached a threshold. This threshold in microgravity is substantially smaller than that in normal gravity. Experimental results are presented in terms of an acceleration based Bond number which has been found to characterize the bubble behaviour in the laboratory experiments [1]. 相似文献