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91.
Crystallization behaviours around the glass transition temperature in an amorphous Fe70Nb10B20 alloy were investigated by means of transmission electron microscopy. Dense bcc-Fe nanocrystals initially appeared as the primary phase, followed by the dense formation of the (Fe,Nb)23B6 nanocrystalline phase. The bcc-Fe nanocrystals were formed even by annealing at a temperature that is 38 K lower than the glass transition temperature. A difference of the low temperature behaviours between the present conventional amorphous alloy and a bulk metallic glass was discussed. 相似文献
92.
93.
Hitoshi Ohta Susumu Okubo Shojiro Kimura Tsuyoshi Tanaka Hikomitsu Kikuchi Hiroshi Nagasawa 《Journal of Infrared, Millimeter and Terahertz Waves》2001,22(3):387-391
Developments of the high field ESR system in Kobe University is presented. Using Gunn oscillators and backward traveling oscillators (BWO), we can cover the frequency region from 30 to 1183.6 GHz with the use of InSb detector. Pulsed magnetic field up to 30 T is available and we are now trying to extend the field up to 40 T. Temperature range is from 1.8 to 300 K. Using this system, we studied S=1/2 ladder like system Cu2(C5H12N2)2Cl4, and found a new magnetic transition at 10.1 T at 1.8 K. The temperature dependence of ESR in Cu2(C5H12N2)2CI4 shows g-shift below 8 K which corresponds to the maximum of the magnetic susceptibility. The g-shift below 8 K suggests the increase of the quantum fluctuation in the system, and the role of the quantum fluctuation in Cu2(C5H12N2)2CI4 is discussed. 相似文献
94.
T Funabiki T Matsubara M Ochiai Y Marugami Y Sakurai S Hasegawa H Imazu 《Canadian Metallurgical Quarterly》1997,46(4):169-172
Theory-driven investigations are necessary for generalization of findings and development of health care policy. Within the environments where nurses practice, however, there often is insufficient time to develop a theory base that supports practice changes or the investigation of their effects. Theories that support such investigations need to incorporate elements associated with both the structure and the process of care delivered as well as the outcomes expected. These same theories also need to specify the focal level of interest for research questions. Incorporating a research template to guide practice investigations facilitates decision making and collection of data. 相似文献
95.
Radical polymerization of captodatively substituted alkyl acylamidoacrylates was studied by pulsed laser polymerization using a N2 laser. Propagation rate coefficient of the acrylates was varied with solvents used in spite of a radical mechanism, but little varied with methyl, n-propyl, and isopropyl substituents on the acrylates. Arrhenius parameters for the propagation indicated that a solvent affected mostly on a frequency factor rather than a activation energy. In addition, it was suggested that these captodatively substituted propagating radicals were thermodynamically persistent but kinetically active in propagation, which resulted in rather smooth propagation in spite of bulky 1,1-disubstituted olefins. The mechanism of the polymerizations was discussed in detail on the basis of the kinetic studies and ESR spectroscopy. 相似文献
96.
Takahiro Yokoyama Akito Masuhara Tsunenobu Onodera Hitoshi Kasai Hidetoshi Oikawa 《Synthetic Metals》2009,159(9-10):897-899
Core/shell hybridized nanocrystals composed of Ag nanoparticle core and polydiacetylene shell were fabricated successfully by means of “co-reprecipitation/microwave irradiation method”. The hybridized nanocrystals were characterized using transmission electron microscopy (TEM) observation and UV–vis absorption spectroscopy. UV–vis spectral measurements revealed that polydiacetylene shell was the red phase while π-conjugated backbone is distorted. Detailed mechanism of formation of the red phase was discussed. 相似文献
97.
98.
Yoshikazu Horino Miki Sugata Hitoshi Abe 《Advanced Synthesis \u0026amp; Catalysis》2016,358(7):1023-1028
A three‐component reaction of 3‐(tri‐n‐butylstannyl)allyl acetates, aldehydes, and triorganoboranes in the presence of a palladium‐Xantphos catalyst system predominately gave (E)‐anti‐homoallylic alcohols with high diastereoselectivity and good to high levels of alkene stereocontrol. An efficient chirality transfer was observed when an enantioenriched substrate was employed. The reaction was initiated by the formation of an allylic gem‐palladium/stannyl intermediate, which subsequently underwent allylation of the aldehyde by an allyltributyltin followed by a coupling reaction of the in‐situ‐generated (E)‐vinylpalladium acetate with the triorganoborane.
99.
During pulse discharge sintering (PDS) of Ti/SiC/C powder mixture, combustion synthesis reactions occurred at heating rates above 20 °C/min. With an increase in heating rate, combustion synthesis occurred at higher temperatures. The essential of this combustion reaction is the liquid reaction between Ti and formed Ti5Si3. The exothermic TiC formation during PDS process promotes this liquid reaction. We have found that the combustion reactions alone did not finish the formation reactions for Ti3SiC2, and further heating following the combustion reactions is necessary for the synthesis process of Ti3SiC2. 相似文献
100.
It is demonstrated that resonance surface X-ray scattering (RSXS), in which incident X-ray energy close to the Pt LIII absorption edge (11.55 keV) is used, is very useful for the determination of the structure of electrodeposited Pt thin layers on a Au(1 1 1) surface. This technique was applied to characterize the structure of electrodeposited Pt layers on Au(1 1 1) substrates prepared under two extreme conditions, which are known to provide rough and atomically flat layers. Detailed structural information was obtained by RSXS measurements and it was confirmed that the structures of the Pt layers were as reported. Pt atoms of the atomically flat monolayer were found to be situated at the threefold hollow cubic closest packing (ccp) sites of the Au(1 1 1)-(1 × 1) surface. 相似文献