一种新型特级防火卷帘的研究与开发——3J特级防火卷帘

介绍3J特级防火卷帘的各种重要功能特点,讨论其实用性与易用性以及推广该产品的必要性与可行性。     

半刚性连接节点对有侧移钢框架稳定承载力的影响

随着对梁柱节点性能研究的深入,发现连接性能对结构性能有着很大的影响,同时在进行结构柱构件稳定计算时必须考虑柱端约束条件,因此需要将柱端连接性能的影响反映到约束条件中去.现有规范并未就如何考虑连接半刚性性能对柱构件计算长度的影响作出可供直接采用的计算方法.结合规范的制订依据提出了考虑连接性能对柱计算长度影响的计算方法;全盘考虑连接性能对层间整体稳定的影响.     

Architectural Control of Hierarchical Nanobelt Superstructures in Catanionic Reverse Micelles

BaXO₄ (X = Mo, W) nanobelts and a variety of hierarchical superstructures assembled from the nanobelts have been synthesized in a catanionic reverse‐micelle system. The effects of various factors, such as the mixing ratio (r) between the anionic and cationic surfactants, the temperature, and the presence of polymeric additives, on the formation of the nanobelts and their hierarchical assembly have been examined in detail. In particular, r has been shown to be powerful in modulating the formation and assembly of the BaMoO₄ and BaWO₄ nanobelts. Architectural control of the penniform nanobelt superstructures has been readily achieved by changing the experimental parameters. A plausible two‐stage growth mechanism has been proposed for the formation of penniform BaXO₄ nanobelt superstructures in catanionic reverse micelles.     

Hydrothermal synthesis of hexagonal ZnO clusters

Hydrothermal process was applied to synthesize zinc oxide nanocrystals. X-ray powder diffraction and scanning electron microscopy were used to analyze the crystal structure and surface morphology. XRD pattern analysis showed that the ZnO clusters are single hexagonal phase of wurtzite structure (space group P63 mc) with no impurity of Zn and Zn(OH)₂. Also, SEM images revealed that the size of a single ZnO crystal is between 200-500 nm in diameter and 2-5 μm in length. The influence of potassium iodide (KI) as a surfactant on the crystallinity of ZnO has been investigated.     

MHD simulation of high-current subsonic vacuum arc under different distributed axial magnetic fields

Based on two-temperature magnetic hydrodynamic (MHD) model, the influence of saddle-shaped distributed axial magnetic field (AMF, linearly increases along radial position) and bell-shaped distributed AMF (linearly decreases along radial position) on plasma loss and heat flux density to anode in subsonic high-current vacuum arc (HCVA) is simulated and analyzed. According to the simulation results, the saddle-shaped AMF can more effectively inhibit plasma loss from arc column than that of bell-shaped AMF. Comparisons between simulation results and experimental results further verify the correctness of model and simulation.     

8字形管角部裂纹问题研究

冷弯异型管在角部存在应力集中现象，有时存在裂纹倾向。通过对沈阳东洋异型管有限公司一异型管产品——8字形管产生裂纹的原因进行分析，确定了解决方案：①修理轧辊，加大有开裂倾向的内陷角；②选用塑性更好的板材。实践证明，该措施能有效地防止管角角部裂纹的产生。     

回龙电站地下厂房开挖施工技术

回龙电站地下厂房设计开挖尺寸为112m×42m×16m(长×高×宽),采用岩壁吊车梁新型结构形式。厂房结构布置自上而下共分6层,结构复杂;施工面相互交叉,干扰因素多,爆破施工安全隐患大。通过精心组织,结合优质的施工技术和周密的措施,较好地完成了开挖任务。图1幅,表3个。     

锌(Ⅱ)-氨基酸配合物分子内配体间疏水作用

应用 p H电位滴定法研究了配合物 Zn( Aa) 2 [Aa-=L- val(缬氨酸根 ) ,L- phe(苯丙氨酸根 ) ,L- trp(色氨酸根 ) ,L- tyr(酪氨酸根 ) ]在水和 2 0 %、40 %及 60 %二氧六环 /水溶液中的稳定性 [t=2 5℃ ,c=0 .1 mol/L Na Cl O4]。配合物 Zn( Aa) 2 相对于母体配合物 Zn( Aa) + 稳定性用Δlog K=log KZn( Aa)Zn( Aa) 2 - log KZn Zn( Aa) 表示。结果表明 :与 L-丙氨酸 ( L- ala)配合物 Zn( L- ala) 2 相比 ,所有这些氨基酸配合物 Zn( Aa) 2 均具有相对较大的 Δlog K值 ,表明这些配合物分子内存在着额外的稳定化作用。这种稳定性化作用可能主要归因于配合物分子内氨基酸侧链之间的疏水作用 ,并且这种作用随着氨基酸侧链结构及溶剂极性变化而变化     

Formation of ordered microporous films with water as templates from poly(D,L‐lactic‐co‐glycolic acid) solution

Recently a method that uses water droplets at the air–solution interface as an ordered template was reported for the preparation of ordered micrometer‐size honeycomb structures. Here we show that the method can also be used for formation of honeycomb‐like porous films from random copolymers with certain hydrophilicity, besides those polymers with defined structures such as block copolymers, starlike homopolymers, amd amphiphilic polymers. This demonstrates that the stabilization of water droplets is the key factor for the regular structure. Also we indicate that size and structure of the films can be regulated by such variables as concentration and atmospheric humidity. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 1846–1850, 2003