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991.
M.P. Gaukroger P.M. Martineau M.J. Crowder I. Friel S.D. Williams D.J. Twitchen 《Diamond and Related Materials》2008,17(3):262-269
X-ray topography has been used to study single crystal diamond samples homoepitaxially grown by microwave plasma-assisted chemical vapour deposition (CVD) on high pressure high temperature (HPHT) and CVD synthetic diamond substrates. Clusters of dislocations in the CVD diamond layers emanated from points at or near the interface with the substrate. The Burgers vectors of observed dislocations have been determined from sets of {111} projection topographs. Dislocations have line directions close to the [001] growth direction and are either edge or 45° mixed dislocations. Where groups of dislocations originated at isolated points they tended to be of the edge variety. Where the substrate surface was deliberately damaged before growth, two sets of dislocations were observed to have propagated from each line of damage and there was a tendency for dislocations to be of the 45° mixed variety with a component of their Burgers vector parallel to the polishing direction. It is demonstrated that X-ray topography can be used to deduce the growth history of CVD synthetic diamond samples produced in multiple growth stages. 相似文献
992.
Muhammad Maqbool Hugh H. Richardson Martin E. Kordesch 《Journal of Materials Science》2007,42(14):5657-5660
Thin films of Praseodymium doped AlN are deposited on silicon (111) substrates at 77 K and 950 K by rf magnetron sputtering
method. About 500–1000 nm thick films are grown at 100–200 watts RF power and 5–8 mTorr nitrogen, using a metal target of
Al with Pr. X-rays diffraction results show that films deposited at 77 K are amorphous and those deposited at 950 K are crystalline.
Cathodoluminescence studies are performed at room temperature and luminescence peaks are observed in a wide range from ultraviolet
to infrared region. The most intense peak is obtained in green at 526 nm from amorphous films as a result from 3P1→3H5 transition. In crystalline films the intense peak was obtain in red at 648 nm as a result from 3P0→3F2 transition. Films are thermally activated at 1300 K for half an hour in a nitrogen atmosphere. Thermal activation enhances
the intensity of luminescence. Two peaks at 488 nm and 505 nm merged after thermal activation, giving rise to a single peak
at 495 nm. 相似文献
993.
Myrtveit I. Stensrud E. Shepperd M. 《IEEE transactions on pattern analysis and machine intelligence》2005,31(5):380-391
Empirical studies on software prediction models do not converge with respect to the question "which prediction model is best?" The reason for this lack of convergence is poorly understood. In this simulation study, we have examined a frequently used research procedure comprising three main ingredients: a single data sample, an accuracy indicator, and cross validation. Typically, these empirical studies compare a machine learning model with a regression model. In our study, we use simulation and compare a machine learning and a regression model. The results suggest that it is the research procedure itself that is unreliable. This lack of reliability may strongly contribute to the lack of convergence. Our findings thus cast some doubt on the conclusions of any study of competing software prediction models that used this research procedure as a basis of model comparison. Thus, we need to develop more reliable research procedures before we can have confidence in the conclusions of comparative studies of software prediction models. 相似文献
994.
V.A. Brezhnev V.M. Abramson A.M. Zemelman S.N. Vlasov N.I. Koulaguin V.E. Merkin V.N. Razbeguin 《Tunnelling and Underground Space Technology incorporating Trenchless Technology Research》2005,20(6):595-599
Sustained world economic development trends characteristic with international trade annual growth rate of 7–8% along with considerable dynamics in the interregional goods circulation sphere on one hand and vast territory of Russia combined with a relatively developed railway network on the other hand provide a unique chance for this country to arrange land transportation routes alternative and competitive in comparison with existing marine routes. Construction of rail tunnels seems to be most efficient means for transportation corridors to cross-wide water areas like Nevelsky Strait (10.5 km) between the mainland and the Sakhalin Island in Russia, Bering Strait (92 km) between Chukotka Peninsula (Russia) and Alaska (USA). The tunnels construction conditions, structures and technologies planned to be used are considered in the paper. 相似文献
995.
In office buildings, the use of passive cooling techniques combined with a reduced cooling load may result in a good thermal summer comfort and therefore save cooling energy consumption. This is shown in the low-energy office building ‘SD Worx’ in Kortrijk (Belgium), in which natural night ventilation and an earth-to-air heat exchanger are applied. In winter, the supply air is successively heated by the earth-to-air heat exchanger and the regenerative heat exchanger, which recovers the heat from the exhaust air. In summer, the earth-to-air heat exchanger cools the ventilation air by day. In addition, natural night ventilation cools down the exposed structure which has accumulated the heat of the previous day. In this article the overall thermal comfort in the office building is evaluated by means of measuring and simulation results. Measurements of summer 2002 are discussed and compared to simulations with a coupled thermal and ventilation simulation model TRNSYS-COMIS. The simulations are used to estimate the relative importance of the different techniques. The evaluation shows that passive cooling has an important impact on the thermal summer comfort in the building. Furthermore, natural night ventilation appears to be much more effective than an earth-to-air heat exchanger to improve comfort. 相似文献
996.
C. G. Gwie R. J. Griffiths D. T. Cooney M. L. Johns D. I. Wilson 《Journal of the American Oil Chemists' Society》2006,83(12):1053-1062
The spray-freezing of two food fats, tripalmitin (PPP) and cocoa butter (CB) and mixtures thereof, has been modeled experimentally
using a novel single droplet freezing apparatus configured so that temperature profiles or samples for microstructure analysis
can be obtained. For 2 mm diameter droplets suspended in a cold air flow at temperatures around 2–15°C, initial cooling rates
were on the order of 10 K s−1 and the temperature profiles could be correlated directly to DSC data collected at 20 K min−1, indicating that minimal supercooling of the materials occurred in the droplet form. Microstructure analysis confirmed that
PPP crystallized preferentially in mixtures, and that the surface structure was very sensitive to storage conditions. The
bulk structure was much less sensitive, and the internal microstructure of the PPP droplets revealed distinct nucleation sites,
which were absent from the CB: These persisted in the mixtures up to 50 wt%. X-ray analysis indicated that the fats crystallized
in their more stable forms, namely, β for PPP and Form V/V1 in CB. 相似文献
997.
Two types of CdTe quantum dots of different sizes (4 and 5 nm) were successfully deposited on optical fibers using the layer-by-layer electrostatic self-assembly method. The sensors showed a linear and reversible variation of the emission wavelength for a temperature range from 30 degC to 100 degC, with a sensitivity of 0.2 nm/degC 相似文献
998.
We report the growth of highly C-axis orientation of Sr
x
Ba1−x
Nb2O6 (SBN) thin films on p-type (100) Si substrates by using a potassium-substituted SBN template layer with the sol–gel method. The crystallization of SBN thin films was found closely related to the potassium ion doping concentration and the postannealing temperature of the K-SBN template layer. Secondary ion mass spectrometry analysis showed that potassium elements were accumulated at the interface of the template layer and silicon substrate. SBN films postannealed at 750 °C with K-SBN template layer has a smaller full width at half maximum of X-ray rocking curve of 2.45° than that of 5.40° for the pure SBN films. By introducing a template layer, the surface morphologies of SBN films fabricated on silicon substrate were greatly improved. 相似文献
999.
Synthesis of 21R AlN polytypoids was investigated using Al and ultrafine SiO2 powder in a flowing nitrogen atmosphere by means of thermal gravity (TG), differential scanning calorimeter (DSC), X-ray diffractometer (XRD) and scanning electronic microscope (SEM) linked with energy dispersive spectrometer (EDS). The results showed that the formation mechanism of AlN polytypoids was different from that in reaction sintering process using Si3N4, AlN, Al2O3 and other sintering additive as raw materials. It was suggested that firstly Al reduce SiO2 into Si and is also nitrided into AlN, then AlN, Al2O3 and SiO2 dissolve into silicon liquid until the AlN polytypoids precipitate in saturated liquid in a flowing nitrogen atmosphere at lower than 1700 °C. 相似文献
1000.
The structural properties and hydrogen bonding of undoped and phosphorous doped polycrystalline silicon produced by step-by-step laser dehydrogenation and crystallization technique were investigated using Raman spectroscopy and hydrogen effusion measurements. At low laser fluences, EL, a two-layer system is created. This is accompanied by the change in hydrogen bonding. The intensity of the Si–H vibration mode at 2000 decreases faster than the one at 2100 cm−1. This is even more pronounced in phosphorous-doped specimens. The laser crystallization results in an increase of the hydrogen binding energy by approximately 0.2–0.3 eV compared to the amorphous starting materials. 相似文献