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141.
Fine particles of cadmium carbonate (CdCO3) were prepared by heating aqueous solutions containing dissolved urea and cadmium sulfate at 85°C for 1 h. Effect of the composition of the reactant mixture on the morphology of the precipitated particles was investigated. It was found that the cadmium sulfate content of the reactant mixture significantly affected the shape and size of the precipitated particles. At certain range of reactant mixture composition, cauliflower-shaped uniform particles were obtained. The later particles were coated with basic copper carbonate (Cu2(OH)2CO3) by heating aqueous dispersions, containing CdCO3 particles, copper (II) nitrate, and urea at 85°C for various periods of time with constant stirring. The coating process was found sensitive to the experimental conditions and in most of the trials; mixtures of the coated and coating precursor particles were obtained. As such, extensive optimizations were carried out and conditions were established for the production of uniformly coated particles.On calcination at 700°C for 1 h, the CdCO3 particles converted into CdO, whereas the coated particles (CdCO3
(core)/Cu2(OH)2CO3
(coating) transformed into CdO(core)/CuO(coating)) without sintering. In the coated particles, the core and coating materials stayed mutually inert during the calcination reaction and independently converted into their respective oxides.All the calcined and uncalcined products were characterized by various physical and chemical methods. 相似文献
142.
143.
144.
145.
Yu. I. Golovin 《Journal of Materials Science》2004,39(16-17):5129-5134
An influence of steady, pulse and microwave magnetic fields on mechanochemical reactions between structural defects in doped ionic crystals has been studied. The effects of dislocation depinning, dislocation mobility increase, macroplastic unhardening and magnetoresonant softening in magnetic fields have been revealed. It is shown that the magnetosensitive spin-dependent reactions between structural defects is the reason of magnetoplastic effects in nonmagnetic crystals. It means that the electron and nuclear spin states of the paramagnetic defects play an important role in the formation of mechanical properties of crystals in magnetic fields and without them. 相似文献
146.
S. Zh. Davrenbekov E. S. Mustafin B. K. Kasenov S. T. Edil'baeva Sh. B. Kasenova E. K. Zhumadilov Zh. I. Sagintaeva 《Inorganic Materials》2004,40(9):976-978
NdMCr2O5 (M = Na, K, Cs) and NdMgCr2O5.5 are prepared by solid-state reactions between appropriate oxides and carbonates and are shown to have a tetragonal structure. The heat capacity of these chromites, measured from 298.15 to 673 K, exhibits sharp changes attributable to second-order phase transitions. The C
p
0(T) data are represented by quadratic best fit equations. The electrical resistivity of the chromites is measured between 303 and 493 K. The results attest to semiconducting behavior of the materials in certain temperature ranges. 相似文献
147.
I. A. Grishin V. A. Gur'ev E. B. Intyushin Yu. E. Elliev A. P. Savikin 《Inorganic Materials》2004,40(4):431-433
TeO2–WO3 glasses coactivated with Er3+ and Yb3+ are prepared. The effect of Yb content on the efficiency of Er photoluminescence (PL) in the visible and IR spectral regions is studied. The highest PL efficiency is achieved at an Er : Yb atomic ratio of 1 : 1. The PL lifetime for the Er3+
4
I
13/2 level is determined to be 7–9 ms. 相似文献
148.
Starting from plysical laws a four-dimensional nonlinear model for mecano-hydraulic servomechanisms is deduced. The stability of its equilibria is analysed using a theorem of Lyapunov and Malkin to handle the critical case due to the presence of zero in the spectrum of the matrix of the linear part around equilibria. Stability diagrams are drawn and simulation results are presented through phase diagrams. 相似文献
149.
The operation of a torsional oscillator for detection, of flow-driven textural transitions in, 3He-A is described. The detection technique, tracking the shift of the resonant frequency of the torsional oscillator, allows us to observe textural changes and the presence of vortices in zero magnetic field. It relies on. the anisotropic superfluid density of 3He-A and its change due to reorientation of the Î-texture caused by counterflow. 相似文献
150.
M. I. Danielyan K. S. Kulakov S. L. Kulakov V. L. Tumanov M. E. Kompan 《Technical Physics Letters》2007,33(7):597-599
A considerable (~1.4-fold) increase in the average output power of a chemical current source has been achieved by means of a periodic pulsed manipulation of the load. A scheme used for the pulse-train loading is presented and mechanisms ensuring an increase in the average output power of the current source are considered. 相似文献