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971.
Fumagalli L Ferrari G Sampietro M Casuso I Martínez E Samitier J Gomila G 《Nanotechnology》2006,17(18):4581-4587
Nanoscale capacitance imaging with attofarad resolution (~1?aF) of a nano-structured oxide thin film, using ac current sensing atomic force microscopy, is reported. Capacitance images are shown to follow the topographic profile of the oxide closely, with nanometre vertical resolution. A comparison between experimental data and theoretical models shows that the capacitance variations observed in the measurements can be mainly associated with the capacitance probed by the tip apex and not with positional changes of stray capacitance contributions. Capacitance versus distance measurements further support this conclusion. The application of this technique to the characterization of samples with non-voltage-dependent capacitance, such as very thin dielectric films, self-assembled monolayers and biological membranes, can provide new insight into the dielectric properties at the nanoscale. 相似文献
972.
Sobrino-López A Raybaudi-Massilia R Martín-Belloso O 《Journal of dairy science》2006,89(10):3739-3748
Staphylococcus aureus is an important milk-related pathogen that is inactivated by high-intensity pulsed electric fields (HIPEF). In this study, inactivation of Staph. aureus suspended in milk by HIPEF was studied using a response surface methodology, in which electric field intensity, pulse number, pulse width, pulse polarity, and the fat content of milk were the controlled variables. It was found that the fat content of milk did not significantly affect the microbial inactivation of Staph. aureus. A maximum value of 4.5 log reductions was obtained by applying 150 bipolar pulses of 8 μs each at 35 kV/cm. Bipolar pulses were more effective than those applied in the monopolar mode. An increase in electric field intensity, pulse number, or pulse width resulted in a drop in the survival fraction of Staph. aureus. Pulse widths close to 6.7 μs lead to greater microbial death with a minimum number of applied pulses. At a constant treatment time, a greater number of shorter pulses achieved better inactivation than those treatments performed at a lower number of longer pulses. The combined action of pulse number and electric field intensity followed a similar pattern, indicating that the same fraction of microbial death can be reached with different combinations of the variables. The behavior and relationship among the electrical variables suggest that the energy input of HIPEF processing might be optimized without decreasing the microbial death. 相似文献
973.
Energy saving is a high-priority in developed countries. For this reason, energy-efficient measures are being increasingly implemented in all sectors. The residential sector is responsible for an important part of the energy consumption in the world. Most of this energy is used in heating, cooling, and artificial ventilation systems.With a view to developing energy-efficient structures, this article provides an overview of building design criteria that can reduce the energy demand for the heating and cooling of residential buildings. These criteria are based on the adoption of suitable parameters for building orientation, shape, envelope system, passive heating and cooling mechanisms, shading, and glazing. An analysis was made of previous studies that evaluated the influence of these parameters on the total energy demand and suggested the best design options. This study is useful for professionals who are responsible for decision-making during the design phase of energy-efficient residential buildings. 相似文献
974.
The performance of chromatographic systems to mimic aquatic toxicity to the fathead minnow fish is evaluated taking into account the factors that contribute to the variance of biological-chromatographic correlations. These factors are the precision to measure the fathead minnow toxicity, the precision of the surrogate chromatographic system, and the error from the dissimilarity between the fathead minnow and chromatographic systems. The precisions are estimated through the characterization of the systems by the solvation parameter model. Several chromatographic systems as well as the common reference octanol-water partition system have been selected to test their ability to model the nonspecific toxicity to the fathead minnow by means of the proposed approach. Predictions and experimental tests show that the micellar electrokinetic chromatography system of sodium taurocholate and chromatographic measurements using an immobilized artificial membrane column provide the most precise estimations of this biopartitioning property. The octanol-water partition system, the conventional C18 high-performance liquid chromatography systems, and the micellar electrokinetic chromatography system of sodium dodecylsulfate show worse performances. 相似文献
975.
González-Mariño I Quintana JB Rodríguez I González-Díez M Cela R 《Analytical chemistry》2012,84(3):1708-1717
For the first time, a mixed-mode solid-phase extraction with fractionation of basic analytes from neutral and acidic species during cartridge elution and liquid chromatography-quadrupole-time-of-flight mass spectrometry (LC-QTOF-MS) was combined for the quantitative determination of 24 illicit drugs and metabolites in urban sewage samples. The effects of several sample preparation and instrumental parameters in the sensitivity and selectivity of the quantitative method are thoroughly discussed. Under final working conditions, recoveries above 63% and 82% were attained for all species in raw and treated sewage, respectively; whereas, the limits of quantification of the method, defined for a signal-to-noise of 10 (S/N = 10), ranged from 2 to 50 ng L(-1). Sequential elution of mixed-mode cartridges allowed a significant reduction of matrix effects observed during electrospray ionization of basic drugs versus those measured for hydrophilic balance reversed-phase sorbents and the same mixed-mode polymer without fractionated elution. Analysis of raw wastewater samples confirmed the ubiquity of cocaine (COC), benzoylecgonine (BE), and 11-nor-9-carboxy-Δ(9)-tetrahydrocannabinol (THCCOOH) in this matrix. The capability of the above methodology to identify new illicit drugs and/or metabolites in sewage samples is also discussed. With this aim, a two step strategy is proposed. First, high-resolution MS chromatograms, acquired throughout each chromatographic run, are automatically searched against an in-house built database, a reduced list of candidate drugs is generated, and the corresponding extracted ion chromatograms are obtained. In a further LC run, the tandem mass spectrometry (MS/MS) spectra of unknown peaks are acquired using different collision energies and compared with those existing in public libraries, or interpreted, to assign the unknown peak to one of the previously selected candidates. 相似文献
976.
In photonic force microscopes, the position detection with high temporal and spatial resolution is usually implemented by a quadrant position detector placed in the back focal plane of a condenser. An objective with high numerical aperture (NA) for the optical trap has also been used to focus a detection beam. In that case the displacement of the probe at a fixed position of the detector produces a unique and linear response only in a restricted region of the probe displacement, usually several hundred nanometers. There are specific experiments where the absolute position of the probe is a relevant measure together with the probe position relative the optical trap focus. In our scheme we introduce the detection beam into the condenser with low NA through a pinhole with tunable size. This combination permits us to create a wide detection spot and to achieve the linear range of several micrometers by the probe position detection without reducing the trapping force. 相似文献
977.
We suggest and study experimentally a time-sharing protocol for acousto-optical deflectors (AODs) that permits one to map the radial optical trapping force of optical tweezers without using a controllable flux control or an additional beam. Variations of the trapping potential due to modifications of the optical system are easily detected in terms of the force map. The protocol can be used in optical tweezers that already include an AOD without adding new elements in the existing optical system. 相似文献
978.
This paper proposes a combined method for two-dimensional temperature and velocity measurements in liquid and gas flow using a schlieren system. Temperature measurements are made by relating the intensity level of each pixel in a schlieren image to the corresponding knife-edge position measured at the exit focal plane of the schlieren system. The same schlieren images were also used to measure the velocity of the fluid flow. The measurement is made by using particle image velocimetry (PIV). The PIV software used in this work analyzes motion between consecutive schlieren frames to obtain velocity fields. The proposed technique was applied to measure the temperature and velocity fields in the natural convection of water provoked by a heated rectangular plate. 相似文献
979.
C. Ginestra N. Coron E. García P. de Marcillac M. Martínez Y. Ortigoza T. Redon L. Torres 《Journal of Low Temperature Physics》2012,167(5-6):973-978
We present the analysis of the data obtained with a 53?g SrF2 scintillating bolometer operated at 20?mK. We have analyzed its heat and light response (time constants, linearity and energy resolution) and measured its scintillation relative efficiency factor for different particles (alpha, beta/gamma and neutrons). We have studied the spatial uniformity of the light output profiting from its internal contamination. The light amplitude of alphas from the delayed coincidence 224Ra→220Rn→216Po (emitted from the same crystal position) shows a positive correlation, evidence of a non-uniformity that worsens the light signal energy resolution by more than?50%. 相似文献
980.
Mitsuo Ramos Azpeitia E. Elizabeth Martínez Flores Gabriel Torres Villase?or 《Journal of Materials Science》2012,47(17):6206-6212
The effects of deformation temperature and strain rate on the superplastic behavior of the Zn–21Al–2Cu alloy (Zinalco alloy) were investigated by uniaxial tensile tests. Results were compared with those of the Zn–22Al eutectoid alloy without Cu. It was observed that additions of 2 % Cu leads to a decrease of the maximum strain attainable from 2600 % to 1000 %. The maximum strain in Zinalco alloy is obtained at lower strain rates. The presence of Cu increases the values of flow stress up to 600 % compared with those reported in the Zn-22Al alloy. Grain size sensitivity (p), true activation energy (Q t ), and constant A of the constitutive equation were not affected by presence of Cu unlike the stress exponent (n) which increased from 2.5 to 3.9. The main effect of Cu was to decrease the plastic flow stability of the Zn–22Al alloy. The results indicate that presence of Cu in the Zinalco alloy causes a hardening effect at low strain rates leading to a decrease in the strain rate sensitivity which promotes the formation and growth of sharp necks. Microstructural characterization suggests that the large deformations at necking could possibly be due to the substantial elongation capability of the Zn-rich phase (η). 相似文献