新型耐酸料的研制

以石英砂、硅酸钠、粘土、硅微粉和水泥为原料制备了新型耐酸料,对比分析了新型耐酸料与传统耐酸料的物理性能及耐酸性能.试样自然干燥24h脱模后,再经110℃烘干24h,分别于500℃和800℃热处理3h.检测各温度下热处理后试样的体积密度、线变化率、抗折强度、耐压强度以及耐酸性能.研究结果表明:新型耐酸料与传统耐酸料的性能相当.对环境无污染,可部分替代传统耐酸料进行应用.     

Influence of addition of styrene–ethylene/butylene–styrene copolymer on rheological,mechanical, and tribological properties of polyamide nanocomposites

To develop new tribomaterials for mechanical sliding parts, investigations were carried out on the influence of adding styrene–ethylene/butylene–styrene block copolymer (SEBS) on the rheological, mechanical, and tribological properties of polyamide 6 (PA6) nanocomposite, which is a commercial product of layered silicate (clay) filled polyamide 6 (PA6/Clay). Two kinds of block copolymers, unmodified SEBS (SEBS) and maleic anhydride‐grafted SEBS (SEBS‐g‐MA), were added with PA6/Clay nanocomposite. Dynamic viscoelastic properties in the molten state of these nanocomposites and their tensile, impact, and tribological properties of these nanocomposites were evaluated. Dynamic viscoelastic properties were found to increase with the addition of SEBS and were influenced, in particular, by block copolymers containing SEBS‐g‐MA. Influence of the addition of SEBS on mechanical properties of these systems differed for each mechanical property. Although tensile properties decreased with SEBS, Izod impact properties were improved with the addition of SEBS‐g‐MA. Tribological properties were improved with the addition of block copolymer, and the influence of the amount of addition was higher than the type of block copolymer used. These results indicate that new tribomaterials developed have sufficient balance amongst moldability, mechanical, and tribological properties. POLYM. COMPOS., 2010. © 2009 Society of Plastics Engineers     

热处理温度对焦宝石基喷涂料性能的影响

以焦宝石颗粒及细粉为主要原料,以硅微粉、铝酸钙水泥为结合剂,研究了不同热处理温度对焦宝石基喷涂料性能的影响。结果表明,随着热处理温度的提高,焦宝石基喷涂料的体积密度无明显变化,线变化率随热处理温度的提高而增大。焦宝石基喷涂料的抗折强度和耐压强度随着热处理温度的提高呈现先减小后增大的趋势。     

Continuously Frequency Tunable High Power Sub-THz Radiation Source—Gyrotron FU CW VI for 600 MHz DNP-NMR Spectroscopy

A high frequency gyrotron with a 15 T superconducting magnet named Gyrotron FU CW VI has achieved continuous frequency tuning through the relatively wide range of 1.5 GHz near 400 GHz. The operation is at the fundamental cyclotron resonance of the TE₀₆ cavity mode with many higher order axial modes. The output power measured at the end of the circular waveguide system ranges from 10 to 50 watts at the low acceleration voltage of 12 kV for beam electrons. The beam current is also low. It is around 250 mA. This gyrotron is designed as a demountable radiation source for the 600 MHz DNP-NMR spectroscopy. The design and operation results of the gyrotron FU CW VI are presented.     

Phytanic acid α-hydroxylation by bacterial cytochrome P450

Fatty acid α-hydroxylase, a cytochrome P450 enzyme, from Sphingomonas paucimobilis, utilizes various straight-chain fatty acids as substrates. We investigated whether a recombinant fatty acid α-hydroxylase is able to metabolize phytanic acid, a methyl-branched fatty acid. When phytanic acid was incubated with the recombinant enzyme in the presence of H₂O₂, a reaction product was detected by gas chromatography, whereas a reaction product was not detected in the absence of H₂O₂. When a heat-inactivated enzyme was used, a reaction product was not detected with any concentration of H₂O₂. Analysis of the methylated product by gas chromatography-mass spectrometry revealed a fragmentation pattern of 2-hydroxyphytanic acid methyl ester. By single-ion monitoring, the mass ion and the characteristic fragmentation ions of 2-hydroxyphytanic acid methyl ester were detected at the retention time corresponding to the time of the product observed on the gas chromatogram. The K _m value for phytanic acid was approximately 50 μM, which was similar to that for myristic acid, although the calculated V _max for phytanic acid was about 15-fold lower than that for myristic acid. These results indicate that a bacterial cytochrome P450 is able to oxidize phytanic acid to form 2-hydroxyphytanic acid.     

Polyethyleneimine/chitosan hexamer-mediated gene transfection into intestinal epithelial cell cultured in serum-containing medium

In search of an efficient nonviral vector, polyethyleneimine (PEI)-based vectors were examined. In general, the transfection efficiency of nonviral vectors is suppressed by serum. Here we show that PEI based vectors, particularly, the chitosan hexamer-PEI vector, could perform efficient gene transfection into intestinal epithelial cells (IEC-6) in the presence of serum. The conjugation order of the two polymers with a plasmid (first, chitosan hexamer; second, PEI) was found to be an important factor in enhancing transfection efficiency.     

AC Drive System for Tension Reel Control

Recently, adjustable-speed ac drive systems have been employed successfully for blowers, pumps, table rollers, etc., in steel plants instead of the more conventional dc drives. In processing lines many drives require speed and tension control. To confirm the suitability of an ac drive for tension control, the tension reel of an existing pilot processing line has been equipped with an adjustable-speed ac drive. An ac drive system for tension reel control, its characteristics, and performance are described and compared with a dc tension control.     

Computational Ability of Cells based on Cell Dynamics and Adaptability

Learning how biological systems solve problems could help to design new methods of computation. Information processing in simple cellular organisms is interesting, as they have survived for almost 1 billion years using a simple system of information processing. Here we discuss a well-studied model system: the large amoeboid Physarum plasmodium. This amoeba can find approximate solutions for combinatorial optimization problems, such as solving a maze or a shortest network problem. In this report, we describe problem solving by the amoeba, and the computational methods that can be extracted from biological behaviors. The algorithm designed based on Physarum is both simple and useful. Tutorial series of three invited papers

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Formation of layer-like voids in irradiated polytrioxane

The formation of voids and defects is investigated by X-ray diffraction methods, by weight loss measurement and by electron microscopy, for an irradiated polytrioxane (PTOX) obtained by the-ray-induced polymerization of trioxane in the solid state. The main reasons for the formation of the layer-like voids are transverse decomposition at a selective point accessible to the radiation in the micro-fibrils, and the subsequent extensible depolymerization which may occur from the unstable chain end with increase of the radiation dose. The analysis of the SAXS curve for the irradiated PTOX, according to Tsvankin's method gives reasonable results for the void structure, where the reduction of the sub-crystal fraction and also the weight loss of the sample by irradiation are taken into account.     

Changes in the drift and the settlement of the freshwater mussel Limnoperna fortunei along a headrace channel

The nuisance species Limnoperna fortunei is a freshwater mussel whose infestations have harmed water intake facilities, such as water supply systems. We investigated the changes in the drift and the settlement of L. fortunei along a headrace channel. The densities of the drift and the settlement both decreased dramatically with the downstream distance from the L. fortunei source (a reservoir). In comparison with larval densities in the reservoir, drift densities decreased by 10 to 25% at 0.5 km downstream from the reservoir, and were less than 2% at sites more than 4.8 km downstream. Although larval densities at midnight (0:00-2:00) were approximately 1.5 times higher than those at noon (12:00-14:00) in a shallow layer (3 m depth) of the reservoir, we found no diurnal variation of drift densities in the headrace channel. Settlement densities at the site nearest the intake gate were much higher than those of the other sites further downstream in the headrace channel. The L. fortunei adult population in the channel could reduce drift individuals by attracting the larva. The attraction probably induces the massive aggregation at the location of the channel immediately below the drift source, resulting in biofouling.