Effect of acetic acid on electrochemical deposition of carbon-nitride thin film

Electrochemical deposition method was employed to prepare CNx thin film from methanol-urea solution,and it was shown that adding a little acetic acid in the solution significantly affected the deposition process.After optimizing the experiment conditions,we obtained polycrystalline grains with sizes of about 3―7μm on the faces of single crystal silicon.X-ray diffraction spectrua indicate that the grains are mainly composed of cubic phase mixed with a small amount of β and α phases.     

Asynchronous rotation scan for synthetic aperture interferometric radiometer

Synthetic aperture interferometric technique has wide applications in optics, radio astronomy and microwave remote sensing areas. With the increasing demands of high resolution imaging observation, a new time-sharing sampling scheme of asynchronous rotation scan is proposed to meet the technical challenge of achieving a large equivalent aperture and overcome the operating barriers of space borne application. This configuration is basically composed by two asynchronously and concentrically rotating antenna groups, whose revolving radii and speeds are different. The synthetic aperture system with asynchronous rotation scanning scheme can effectively solve the trade-off problem of system complexity, and greatly simplify the system hardware at the cost of sacrificing a certain time resolution. The basic rules and design methods of asynchronous rotation scan are investigated The Gridding method is introduced to inverse the spiral sampling data for image reconstruction. The potential applications of geostationary orbit (GEO) earth observation and solar polar orbit (SPO) plasma cloud observation are explored with numerical simulations to validate the significance and feasibility of this new imaging configuration. Supported by the National Natural Science Foundation of China (Grant No. 40574070, 40671121, 40701100 and 40801136) and the National High-Tech Research Program of China (“863” Program) (Grant No. 2006AA12Z141)     

Experiments and reaction characteristics of liquid phase simultaneous removal of SO<Subscript>2</Subscript> and NO

Experiments of simultaneous removal of SO₂ and NO from simulated flue gas, using NaClO₂ solution as the absorbent, were carried out in a self-designed bubble reactor, and high simultaneous removal efficiencies of SO₂ and NO were obtained under the optimal experimental conditions. The mechanism of simultaneous removal based on NaClO₂ acid solutions was proposed by analyzing the removal products. Possibility and limitation of the desulfurization and denitrification using NaClO₂ acid solutions were calculated by thermodynamic methods. Experimental results of reaction kinetics for simultaneous desulfurization and denitrification indicated that the oxidation-absorption processes of SO₂ and NO were divided into two zones, namely the fast and slow reaction zones. In the slow reaction zones both were zero order reactions, and in the fast reaction zones, the reaction order, rate constant and activation energy of SO₂ reaction with absorbent were 1.4, 1.22 (mol·L⁻¹)^−0.4·s⁻¹ and 66.25 kJ·mol⁻¹, respectively, and 2, 3.15×10³ (mol·L⁻¹) ⁻¹·s⁻¹, and 42.50 kJ·mol⁻¹ for NO reaction, respectively. Supported by the National High-Tech Research and Development Program of China (“863” Project) (Grant No. 2007AA061803)     

A process study of electron beam nano-lithography and deep etching with an ICP system

A systemic process study on an electron beam nanolithography system operating at 100 kV was present. The exposure conditions were optimized for resist ZEP520A. Grating structures with line/space of 50 nm/50 nm were obtained in a reasonably thick resist which is beneficial to the subsequent pattern transfer technique. The ICP etching process conditions was optimized. The role of etching parameters such as source power, gas pressure, and gas flow rate on the etching result was also discussed. A grating structure with line widths as small as 100 nm, duty cycles of 0.5, depth of 900 nm, and the side-wall scalloping as small as 5 nm on a silicon substrate was obtained. The silicon deep etching technique for structure sizes smaller than 100 nm is very important for the fabrication of nano-optical devices working in the visible regime. Supported by the National Basic Research Program of China (“973” Program) (Grant No. 2007CB935301)     

Multi-channel micro neural probe fabricated with SOI

Silicon-on-insulator(SOI) substrate is widely used in micro-electro-mechanical systems(MEMS).With the buried oxide layer of SOI acting as an etching stop,silicon based micro neural probe can be fabri-cated with improved uniformity and manufacturability.A seven-record-site neural probe was formed by inductive-coupled plasma(ICP) dry etching of an SOI substrate.The thickness of the probe is 15 μm.The shaft of the probe has dimensions of 3 mm×100 μm×15 μm with typical area of the record site of 78.5 μm2.The im...     

Emergency aero-photo survey after the 5.12 Wenchuan Earthquake,China

After the 5.12 Wenchuan Earthquake which took place on May 12, 2008, aerial remote sensing has rapidly covered all the influence sites of the earthquake, emergency aero-photo interpretation has revealed the disaster distribution limitation, and captured the information of location, dimension of the destroyed houses, roads and other structures, blocked rivers, etc, which provided destroying conditions of the time for rescuing lives, rebuilding traffic lines and estimating disaster situation. The further interpretation and analysis indicate that large scale second growth geological disasters mainly distribute in the distance of 0–300 km and 45°–50° orientation from the epicenter. About 137 latent large-scale landslides and debris-flows will occur in this rain season and coming several years, so how to avoid current geological disasters as well as the latent large disasters should be considered in making rebuilding and developing plan.     

The effect of hydrogen on the electronic structure of kink in bcc iron

The electronic structures of kinks in the [100](010) and 1/2[111](−110) edge dislocations in bcc iron containing hydrogen are investigated by means of the first-principles DMol method and the discrete variational method. The effects of hydrogen on the kinks are discussed. The results show that hydrogen forms weak bonding states with its neighboring host atoms, and since hydrogen draws charge from its neighboring host atoms, the interactions between most of the host atoms are weakened compared with those of the corresponding atomic pairs in the clean kinks. This indicates that the migration of kink, i.e. the motion of dislocation, is easier in the doping hydrogen kink than in the clean kink, which may be the solid solution softening effect resulting from the impurity hydrogen. Supported by the National Basic Research Program of China (Grant No. 2006CB605102) and Science Foundation of Central South University of Forestry & Technology (Grant No. 06y016)     

Investigation on extremal and critical characteristics of ignition time for H<Subscript>2</Subscript>/O<Subscript>2</Subscript> combustion system and their applications

The L, H and C curves in P-T phase are proposed to describe the minimal, maximal and critical characteristics of ignition time of H₂/O₂ combustion system, respectively. The features of H₂/O₂(Air) combustion system, including explosion or not as well as the time delay to achieve its explosion status, can be well shown by explosion limits and these proposed curves. These curves can be described by 1.2k ₁=k _s [M_s], (k ₁₁/k ₁₀+1)k ₁=k _s [M_s], and 2k ₁=k _s [M_s], respectively, which provide a physical explanation for these curves and give another way to establish them. Based on the contour of ignition time, the Z-type explosion limits can be explained by thermal explosion theory. Furthermore, the ignition distance of supersonic combustion is predicted according to the ignition time obtained in a Semenov system, which is very reasonable.     

Down-scaling LUCC based on the histo-variogram

In remote sensing applications, accurate extraction of land type area after classification is very important. But for images of land use/cover change (LUCC) obtained from the special spatial resolution remote sensing data, it will be of great significance to obtain the land type area information with higher resolution by making use of spatial distribution characteristcs information of the land type itself first and further scaling-down in a given scale threshold on the basis of the existing spatial resolution data. An explicit expression of the relationship between the measurement scale, global fractal dimension and the land type area corresponding to different measurement scales is obtained on the research basis of the authors’ histo-variogram using the standardized area index (SAI). A good attempt has been made to obtain the land type area information with higher resolution by merely using the spatial distribution characteristcs information of the land type in the image itself and further scaling-down in a given scale threshold on the basis of the existing spatial resolution data. Supported by the National Natural Science Foundation of China (Grant No. 40601068), the National Basic Research Program of China (“973” Project) (Grant No. 2007CB714402) and the Key Science and Technology R&D Program of Qinghai Province (Grant No. 2006-6-160-01)     

Safety evaluation and the static-dynamic coupling analysis of counter-arched slab in plunge pool

The stability of plunge pool slab of drainage structure is crucial to energy dissipation, but the working conditions of counter-arched slab are very complex and its stress procedure is considerably nonlinear and coupling. Therefore, a nonlinear static and dynamic coupling method to analyze the counter-arched slab configuration is put forward, which can reflect the coupling of dynamic loads, slab, anchor bars, groundwork and abutment as well as the dynamic procedure of instability. Various nonlinear factors and static-dynamic coupling are taken into consideration, and the working conditions, stress mechanism, dynamic instability procedure and influential instability factors are revealed. The proposed method thus provides a comprehensive safety evaluation method of plunge pool, which further provides an important theoretical basis for engineering design of counter-arched slab in plunge pool. Supported by the National Science Fund for Distinguished Young Scholars (Grant No. 50725929) and the National Natural Science Foundation of China (Grant Nos. 50539060, 50679052, 50779044)