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881.
Chun Lin Ma Qing Feng Wang Rufen Zhang Jikun Li 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(2):229-235
Six triorganotin(IV) complexes of the type {(R3Sn)2[C3S3(COO)2]}n (R = C6H5 1; n-Bu 2; PhCH2 4; p-F-PhCH2 5; o-F-PhCH2 6) and {(R3Sn)2[C3S3(COO)2]}n·[EtOH] (R = Me 3) have been synthesized by the reaction of bis(carboxymethyl)trithiocarbonate with triorganotin(IV) chloride
in the presence of sodium ethoxide. All complexes were characterized by elemental analysis IR, 1H, 13C and 119Sn NMR spectroscopy. Except for 4–6, all complexes were also characterized by X-ray crystallography. The X-ray date revealed
that complexes 1–3 show two-dimensional network polymeric structure in which the geometries of tin atoms are trigonal bipyramid
with the axial positions occupied by carboxylic oxygen atoms. 相似文献
882.
Veysel T. Yilmaz Evrim Senel Canan Kazak 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(3):407-413
The reaction of [Cu(sac)2(H2O)4] · 2H2O with 2-methylpyrazine (mpyz) leads two complexes, concomitant crystallization of a mononuclear complex [Cu(sac)2(mpyz)(H2O)2] (1) and a polymeric complex [Cu(sac)2(μ-mpyz)]n (2). Both complexes have been characterized by elemental analyses, magnetic measurements, FT-IR and ESR, TG-DTA and single-crystal
X-ray diffraction analyses. Single-crystal X-ray analyses show that complex 1 consists of discrete molecules in which the copper(II) ions exhibits a square-pyramidal coordination geometry. The individual
molecules of 1 are connected into a hydrogen-bonded chain structure, which is further assembled to form a three-dimensional network by π–π stacking interactions.
Complex 2 is an 1D coordination polymer in which copper(II) centers are bridged by the mpyz ligand. The chains are further assembled
to form two-dimensional frameworks by π–π and C–H···π stacking interactions. 相似文献
883.
884.
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886.
Rudolf Felix 《Soft Computing - A Fusion of Foundations, Methodologies and Applications》2008,12(2):129-135
Real world applications of a decision model of relationships between goals based on fuzzy relations are presented. In contrast
to other approaches the relationships between decision goals or criteria for each decision situation are represented and calculated
explicitly. The application fields are decision making for financial services and optimization of production sequences in
car manufacturing. 相似文献
887.
A novel online technique for monitoring the insulation condition of ac machine stator windings is proposed in this paper. The concept is to measure the differential leakage currents of each phase winding from the terminal box in a noninvasive manner to assess the insulation condition during motor operation. The conventional differential CTs used for phase fault protection can be replaced with high performance current sensors to measure the leakage current with higher accuracy. Indicators for insulation condition such as the capacitance and dissipation factor are calculated based on the measurements to provide a low cost solution for online insulation condition assessment. A simplified online insulation system model is derived for analysis and interpretation of the measured data. Experimental results on a 15-hp induction motor under simulated insulation degradation conditions show that the proposed technique is a very sensitive method capable of detecting incipient signs of insulation degradation. 相似文献
888.
In a mobile ad hoc network, difficulties exist in supporting address autoconfiguration and naming resolution due to the lack of centralized servers. This letter presents a novel approach, called name‐based autoconfiguration (NBA), which uses host names to determine IP addresses and provides address autoconfiguration and name resolution as a single protocol. 相似文献
889.
Lau H. C. W. Tsui W. T. Lee C. K. M. Ho G. T. S. Ning A. 《Industrial Informatics, IEEE Transactions on》2006,2(4):303-312
In today's competitive logistics business environment, airfreight forwarders need to optimize every aspect of their logistics operations. However, forwarders still heavily rely on human brain and working experiences for calculating complex cargo packing and scheduling problems. Although recent research studies related to cargo packing and scheduling problems have resulted in the development of a number of advanced techniques of cargo planning, it can be seen that most of the research work is focused on the optimization of space in order to achieve the maximum possible amount of cargo to be packed in the minimum of space. After numerous site evaluation and end-user feedbacks, it is found that space optimization does not necessarily cause profit optimization, which is the ultimate aim of logistics providers. A study of contemporary research publications indicates that there are inadequate research studies related to profit-based optimization in cargo packing areas. This paper presents a profit-based air cargo loading information system (ACLIS) that embeds an innovative technology known as heuristics iterative reasoning technology (HIRT) that supports loading plan generation, focusing on maximization of the profit margin. In general, the proposed system is meant to maximize the profit in the airfreight forwarding business. It adopts an objective function governed by a list of constraints together with rule-based reasoning to provide expert advice to support the generation of appropriate loading plans 相似文献
890.
The current paper addresses the problem of 2-D modelling of the onset of failure process in a layered composite with periodic
array of interfacial cracks under static compression along layers. The statement of the problem is based on the most accurate
approach, the model of piecewise-homogenous medium. The condition of plane strain state is considered. The shear and the extensional
buckling modes are examined. The laminae are modelled by transversally isotropic material (a matrix reinforced by continuous
parallel fibres). The complex non-classical failure mechanics problem is solved utilizing finite element analysis. It is found
that the 0°-plies volume fraction, the crack length and the mutual position of cracks influence the critical strain in the composite. 相似文献