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Ion V. Nicolaescu Gabriel Tardos Richard E. Riman 《Journal of the American Ceramic Society》1994,77(9):2265-2272
A thermogravimetric method for the measurement of carbon, nitrogen, and oxygen in aluminum nitride is described. Since carbon oxidation occurs at lower temperatures than the oxidation of the aluminum compounds, thermogravimetric analyses in the respective temperature regimes can yield measurement of the oxygen, nitrogen, and carbon content. Thermogravimetric analyses were performed on mixtures of aluminum nitride and carbon with various concentrations in order to evaluate the accuracy of this method. The results were compared with those obtained by the hot gas extraction method. Errors produced by overlapping of the temperature ranges of the reactions were evaluated and experimental conditions were optimized to minimize error. This method can produce reliable results at elemental concentrations higher than a few percent. The absolute errors of the C/AI, N/Al, and O/Al atomic ratios were less then 0.02. The detection limit was evaluated to 0.2 wt% of each element. The applicability of the method to the study of the kinetics of the nitridation reaction was demonstrated. 相似文献
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Alexander Pavlov Gonzalo D Garcia De Fernando Juan A Ordoez Lorenzo Hoz 《Journal of the science of food and agriculture》1994,64(2):141-143
The β-hydroxyacyl-CoA-dehydrogenase (HADH) activity of unfrozen and thawed frog legs was investigated. The enzyme was extracted by either immersing frog legs in phosphate buffer 0.1 M, pH 6.0 at 25°C for 15 min or pressing them between trichinoscopy glasses. The enzyme activity was assayed using acetoacetyl-CoA as substrate and measured spectrophotometrically at 340 nm. It was possible by both extraction methods to distinguish between thawed and unfrozen samples although when the juice was obtained by pressing the HADH activity of the dilution was ~ 1.5 times higher than that obtained by immersion. The HADH activity was significantly higher (P≤0·001) in frozen-thawed frogs than in unfrozen legs because during freezing there is a release of HADH. No significative differences were found in the HADH activity in samples frozen in the temperature range -10 to -196°C. HADH activity was not affected by the storage time in crushed ice up to 6 days. 相似文献
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Vicente Rodríguez Montequín Francisco Ortega Fernández Nicolás Abajo de Martínez Juan Antonio González Rodríguez 《JOM Journal of the Minerals, Metals and Materials Society》2002,54(7):46-50
This research summary discusses the application of neural networks, evolutionary strategies, and other artificial intelligence
techniques in the modeling and optimization of the models used for temperature, rolling force, and torque calculation in heavy
plate milling. 相似文献
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TIC is a timed algebraic calculus which combines ideas from asynchronous and synchronous calculi. Time is introduced by assigning explicit time restrictions to the events of an asynchronous calculus. The semantics is defined in an operational way. Interleaving of behaviours is defined in such a way that a proper merge of events in time is achieved. Weak timed bisimulation is also defined. Examples are presented to show the applicability of the calculus to the study of timed behaviours.This work was partially supported by CICYT under the TIC program (MEDAS project) 相似文献
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