Preparation of M-Ba-ferrite fine powders by sugar-nitrates process

In this paper, fine M-type barium hexaferrite (M-Ba-ferrite) particles were synthesized from sugar and nitrates by simple route, which revealed the feasibility of using sugar as chelating agent in forming solid precursors of BaFe₁₂O₁₉. The effects of factors, such as the molar ratio of Fe/Ba, calcination temperature and time, on the morphology, the phase component and the magnetic properties of M-type barium hexaferrite particles were studied by means of X-ray diffraction, infrared spectroscopy, transmission electron microscopy and physical property measurement system. The results showed that the molar ratio of Ba²⁺ to Fe³⁺ influenced significantly on the formation of the single phase barium ferrite. The hexagonal platelet barium ferrite particles with a specific saturation magnetization of 64.48 emu/g, remanence magnetization (Mr) of 33.84 emu/g, and coercive force (Hc) of 1848.85 Oe were obtained when the molar ratio of Fe/Ba was 11.5 and the calcination temperature was 1100 °C for 2 h.     

The formation of ilmenite FeTiO3 powders by a novel liquid mix and H2/H2O reduction process

FeTiO₃ powder was prepared via a liquid mix and H₂/H₂O reduction process. First, an intermediate compound was synthesized by a liquid mix process. This precursor compound to FeTiO₃ was characterized by thermal analysis (TG/DTA) and Fourier Transform Infrared spectroscopy (FT-IR). Second, the precursor was annealed in the air, H₂/H₂O(g) mixing gas stream, respectively. The obtained powder was characterized by X-ray diffraction (XRD), energy dispersive X-ray analysis spectroscopy (EDAX) and scanning electron microscope (SEM). It was showed that pure and homogenous FeTiO₃ was successfully obtained below 600 °C.     

The ferroelectric and optical properties of (Pb0.92La0.08)(Zr0.65Ti0.35)O3 thin films deposited by radio-frequency magnetron sputtering

Ferroelectric (Pb_0.92La_0.08)(Zr_0.65Ti_0.35)O₃ (PLZT) films have been prepared on Pt/Ti/SiO₂/Si and fused quartz substrates using radio-frequency (rf) magnetron sputtering at a deposition temperature of 650°C. X-ray diffraction analysis shows that the PLZT thin films on platinized silicon are polycrystalline with (100)-preferential orientation. A Al/PLZT/Pt capacitor has been fabricated and it shows that the films have excellent ferroelectric character, with saturation polarization (P _s), remanent polarization (P _r) and coercive field (E _c) of 32.8μC/cm², 24.3μC/cm² and 142 kV/cm, respectively. The PLZT thin films exhibit good insulating property and the leakage current density of the films on platinized silicon is only about 0.86 × 10⁻⁷ A/cm² at 200 kV/cm. By the optical transmission spectra measurements, the energy gap (E _g) of the PLZT films on fused quartz is found to be about 3.54 eV. The optical constants (n and k) of the films in the wavelength range of 250–900 nm are obtained by a Filmetrics F20 reflectance spectrometer.     

深处的激情

在澳大利亚一片森林的深处，当弯曲钢架结构的假日别墅内泛起火光的时候，它确实将世界照亮了，《Wallpaper》总第83期讲述一段深处的激情。[编者按]     

几种常用制冷剂的过冷制冷循环特性分析

详细分析了过冷制冷循环特性和空调常用的四种制冷剂(R22、R134a、R407C、R410A)的过冷度对制冷循环制冷量、耗功和性能系数COP的影响,并拟合了过冷度对循环性能参数影响的关系式。针对冰蓄冷系统给出了过冷度控制数值和冷量提高的程度。     

Performance and optimization of multistage partial parallel interference cancellation for wideband CDMA systems in multipath fading channels

In this paper, a closed-form bit error rate (BER) of hard-decision multistage partial parallel interference cancellation (PPIC) having perfect and imperfect channel estimation for complex spreading code-division multiple access (CDMA) over multipath Rayleigh channels was derived. The effects of receiving BER, power ratio of pilot to data channels, multiple-access interference (MAI) and multipath interference, additive white Gaussian noise, and other factors affecting channel estimation error are analyzed. The expression determining the optimal interference cancellation weight at path level for PPIC is first derived. Then, the oscillatory behavior of user-level-optimized PIC and the convergence of perfect channel estimation PIC and path-level-optimized PIC are validated. Results indicate that all factors determining the optimal weight certainly affect the BER performance of PPIC and that the lower BER limit of multistage PPIC depends on the adjustable factors, which include power ratio, observation length, and signal-to-noise ratio, and an unchangeable factor, i.e., number of users. In addition, the variance of MAI for complex spreading sequence is obtained, and the analytical expression can also be employed to predict the performance of multicode CDMA.     

Combined and iterative form of spatial and temporal error concealment for video signals

Video transmission over unreliable channels may suffer from the data loss or corruption. To facilitate the transmission, video content is compressed to save the bandwidth. The compression algorithms remove the redundancies in the video signal, meanwhile increasing the dependencies among symbols in the compressed bit-stream. Thus, when errors occur, they may propagate in both space and time. Among various error control techniques, error concealment (EC) is an effective method that is performed at the decoder to mitigate the influence of errors on the quality of reconstructed images. In this paper, a joint spatial and temporal EC algorithm (JSTEC) is presented. First, several existing temporal EC algorithms are combined in an appropriate order. Then, the spatial correlation in the video is exploited in an iterative form to improve the performance of the temporal EC. Experimental results show that JSTEC performs better both in peak signal-to-noise ratio and subjective quality of images than the existing algorithms.     

H2对UHV/CVD低温选择性外延生长Si1-xGex的影响

利用超高真空化学气相沉积(UHV/CVD)成功实现了Si1-xGex的低温选择性外延生长,并研究了H2对选择性外延生长的影响及其作用机理.以SiH4和GeH4为反应气源,在开有6mm×6mm窗口氧化硅片上进行Si1-xGex外延层的生长.首先分别以不含H2(纯GeH4)和含H2(90%H2稀释的GeH4)的两种Ge源进行选择性外延生长.通过SEM观察两种情况下氧化硅片表面,发现H2的存在对选择性外延生长有至关重要的作用.接着以90%H2稀释的GeH4为Ge源,变化Si源和Ge源的流量比改变H2分压,以获得SiH4和GeH4(90%H2)的最佳流量比,使外延生长的选择性达到最好.利用SEM观察在不同流量比时,经40min外延生长后各样品的表面形貌,并对其进行比较,分析了H2分压在Si1-xGex选择性外延生长中的作用机理.     

A novel frequency offset estimation method for OFDM systems with large estimation range

In this paper, we proposed a novel frequency synchronization method which has larger estimation range than conventional method proposed by Tufvesson. A two steps frequency offset estimation method is performed in the new method. In the first step the received signal is correlated with local training sequence to eliminate the influence of training sequence which makes the estimation range of frequency offset is independent of period of the repeated data in the training sequence. The received signal is correlated with its delay in the second step to obtain the fine estimation of frequency offset. Precise estimation can be achieved in the proposed method than Tufvesson's method. The period of the repeated data in the training sequence determines the estimation range of the frequency offset in the conventional method, while in the new method they are irrelevant. Tens of subcarriers spacing can be estimated by the new method. The new method can be used in other cases as long as a known sequence is transmitted, which will introduce valuable flexibility in training sequence design. The validity of the algorithm is verified in AWGN channel and multipath fading channel.