一种短小芽孢杆菌分离鉴定及培养条件研究

为实施城市垃圾渗透液的生物无害化处理,分离、筛选、鉴定,获得特定菌株,并对其最适培养条件和最佳培养基组分进行优化。从城市垃圾填埋场垃圾渗透液中分离芽孢杆菌,通过设计特异性引物进行PCR反应鉴定目的菌株。此菌细胞呈现杆状,革兰氏阳性,经鉴定为短小芽孢杆菌。采用单因素实验和正交实验法对菌株生长适宜的培养基进行了优化。优化后的培养基主要成分为：玉米淀粉0.1%,酵母提取物1.0%,小牛浸膏0.3%,NaCl0.5%,MgSO4·7H2O 0.49%。在这种条件下,菌株培养10h,其OD320由1.44上升到6.93,为该菌株的深入研究和应用奠定了基础。     

Kaiser 效应点识别方法及储层地应力预测

在储层岩心Kaiser 实验中,声发射累积曲线通常出现多个突变点,导致常规Kaiser 效应点识别方法不精确,甚至存在无法读取Kaiser 点的问题。为此,提出将声发射能量图谱与声发射累积曲线结合的Kaiser 效应点优化识别方法,并用于某油田X区块储层地应力预测。岩心单轴加载实验结果表明：加载初期,岩心处于压缩阶段,声发射数量较多,声发射能量值波动范围较大;加载中期,岩心处于弹性形变阶段,声发射数量较少,声发射能量值较低,变化幅度均一;加载后期,应力达到储层岩心破裂压力,岩心发生破裂,声发射数量急剧增加,声发射能量值达到峰值。加载中期阶段,当轴向应力达到储层岩心承受的历史最大应力时,岩心突然释放大量能量,声发射数量和能量值均突增,随后迅速降低,该现象与Kaiser 现象相吻合,因此通过声发射能量图谱与声发射累积曲线结合的方法能够识别Kaiser 效应点。利用优化后的Kaiser 效应点识别方法,分析某油田X区块地应力分布,计算结果与现场测试结果吻合。     

生球干燥过程及其数学模型

本文探讨了生球干燥过程,发现干燥速度与时间的关系曲线呈“双峰”状和“过渡”状等现象,分析了这种现象的原因,在此基础上,综合考虑了生球干燥过程的物质平衡和能量平衡,建立了生球干燥的全过程模型,实验证明该模型能很好地描述生球干燥的全过程。     

Electrochemical and microstructural characterization of cyclic redox behaviour of SOFC anodes

The oxidation of Ni to NiO in solid oxide fuel cell (SOFC) anode will result in large bulk volume change, which may change the interfaces of the two phases in the anode cermet and thus may cause significant performance degradation. The reduction and oxidation (redox) of the Ni/YSZ cermet were studied at 800 ℃. Anodic polarization measurements were performed before and after redox cycles. The anode current density at an overpotential of 100 mV kept decreasing during the whole redox treatment. It decreased from 19.11 to 7.95 mA·cm-2 after two redox cycles. Anode supported unit cell was assembled for cell's discharge measurements. Cell performance declined after each redox cycle. The maximum power density decreased from 126.28 to 40.32 mW·cm-2 . The microstructural changes after redox cycling were recorded using scanning electron microscopy (SEM). The results reveal that after re-oxidation, the Ni gets coarse and has a higher porosity; the nickel network structure turns to be desultory.     

脉冲等离子体微弧氧化法制备TiO2薄膜及膜层的性能研究

采用硅酸盐溶液体系，利用正交分析法得到其组分的最佳配比，用直流脉冲微弧氧化法在TA2工业纯钛基体上生成多孔的钛氧化物陶瓷膜。用X射线衍射法检测了氧化陶瓷膜的晶体结构，主要由金红石晶型构成，考查了膜的抗热冲击性、在还原性酸中的耐腐蚀能力，用紫外-可见光-分光光度计进行了氧化膜层的光催化活性研究，验证了TiO2薄膜优良的光催化特性。     

Dissolution mechanism of solid nickel in liquid zinc saturated with Fe

The dissolution behavior of solid nickel in static liquid zinc saturated with Fe at 723 K was studied. The results show that when immersing solid Ni in liquid Zn saturated with Fe, the intermetallic compound layers consisted of γ and δ phases are formed on nickel substrate, which is the same as that in liquid pure zinc. However, some F2 particles are formed in the liquid near the solid/liquid interface. These Г2 particles can easily heterogeneously nucleate on （particles and grow fast. The dissolution process is governed by diffusion of nickel atom across a concentration boundary layer in liquid Zn saturated with Fe, and is different from a mixed control mechanism of nickel in liquid pure zinc. The participation of Г2 particles makes the dissolution of solid Ni in the liquid accelerated.     

热镀锌钢白锈产生原因分析及预防

通过扫描电镜观察及X射线衍射测试,对热镀锌钢在海洋环境下产生的白锈进行了分析,结果表明,在海洋环境下白锈由ZnCl2.4Zn(OH)2、2ZnCO3.3Zn(OH)2和ZnO组成,腐蚀产物疏松,不能阻碍腐蚀进一步进行。探讨了白锈形成机理,总结了国内外热镀锌标准有关对热镀锌钢白锈的论述,并提出了有关的防护及处理措施。     

连续冲压中跳废料的防止措施

随着制造技术的不断发展,为了提高生产效率,多工位连续冲压越来越多地应用到冷冲压生产实践中来。随之也带来了一些不同于传统冲压的技术问题,跳废料就是其中之一,若能很好解决这一问题,可以很大程度提高冲压生产效率。     

基于ISO13584-31零件库标准的实体构造原理

研究探讨了PLIB实体的构造原理，并结合螺母零件族进行了说明。     

基于XRD的薄膜界面结合强度试验研究

利用X射线衍射技术（XRD）分析了薄膜结合界面应力及其变化规律，通过对薄膜界面结合状态的检测，建立了X衍射法测量薄膜界面结合强度的原理、方法与过程。其检测界面结合强度方法可对薄膜试样进行非接触检测，适用于晶体或多晶体薄膜的界面结合强度测量，是一种研究无损检测薄膜结合强度的试验新方法。