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131.
Branched polystyrenes were prepared by quasi‐living radical copolymerization of N,N‐diethylaminodithiocarbamoylmethylstyrene (inimer: DTCS) with styrene under UV irradiation. DTCS monomers play an important role in this copolymerization system as an inimer capable of initiating living radical polymerization of the vinyl group. Two monomers (DTCS and styrene) showed equal reactivity toward both propagating species, and the copolymer composition was the same as the comonomer feed. This result means that both the branching and chain length of the hyperbranched molecules can be controlled statistically by the feed monomer ratios. The compact nature of the branched macromolecules is demonstrated by viscosity measurements compared to the linear analogues. © 2001 Society of Chemical Industry 相似文献
132.
Koji Nishimoto Yoshihiro Okumoto Tomoki Harano Ken Atagi Hiroo Fujii Seiji Katayama 《Welding International》2013,27(10):734-743
Dissimilar metal joints of galvannealed steel and commercially available pure aluminium (A1050) sheets were produced by changing the laser power and the roller pressure by the laser pressure welding method. In this method, the YAG laser beam was irradiated into a flare groove made by these dissimilar metal sheets. In addition, the laser beam was scanned at various frequencies and patterns through the fθ lens using two-dimensional scanning mirrors. Then the sheets were pressed by the pressure rolls to be joined. The compound layers in the weld interface were observed by optical microscope, and the layer thicknesses were measured. The thicknesses were in the range of 7–20 μm. The mechanical properties of welded joints were evaluated by the tensile shear test and the peel test. In the tensile shear test, the strengths of the joints produced under the most welding conditions were so high that the fracture occurred through the base aluminium sheet. In the peel test of the specimens subjected to the laser beam of 1200–1400 W power under the roller pressure of 2.94 kN, the specimen fracture took place in the base aluminium sheet. Even if the compound layer was thick, high joint strength was obtained. In order to know the reason for such high strength of joints with thick compound layers and the joining mechanism, the compound layer was observed by the HR-TEM. The TEM observation results revealed that the main phase in the compound layer was the solid solution of Al + Zn. Moreover, the intermetallic compound was identified as FeAl, Fe2Al5, Fe4Al13, and Fe2Al5Zn0.4 phase by electron diffraction. The Fe3Zn10 (Γ phase) of Fe–Zn intermetallic compound was confirmed on a Fe base material. It is assumed that the joining areas were heated in a range of 782°C more than 665°C, a melting point of Al, by laser irradiation because the δlk phase aspect was not confirmed. Because the surfaces of A1050 and Zn plated layer were melted thinly, the layer was over 10 μm thicker. The reason for the production of high strength joints with the relatively thick intermetallic compound layer was attributed to the formation of (Al + Zn) phase with finely dispersed intermetallic compounds. 相似文献
133.
Yasuhito Takahashi Shinji Wakao Koji Fujiwara Hiroyuki Kaimori Akihisa Kameari 《Electrical Engineering in Japan》2010,170(1):26-35
This paper describes a benchmark model proposed for the clarification of the characteristic of various methods for modeling the laminated iron core. In order to obtain a reference solution of the benchmark model, a large‐scale nonlinear magnetostatic field analysis with a mesh fine enough to represent the microscopic structure of the laminated iron core is carried out by using the hybrid finite element–boundary element (FE‐BE) method combined with the fast multipole method (FMM) based on diagonal forms for translation operators. The computational costs and accuracy of two kinds of homogenization methods are discussed, comparing them with the reference solution. As a consequence, it is verified that the homogenization methods can analyze magnetic fields in laminated iron core within acceptable computational costs. © 2009 Wiley Periodicals, Inc. Electr Eng Jpn, 170(1): 26–35, 2010; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20809 相似文献
134.
Shinichi Komaba Naoaki Yabuuchi Tomoaki Ozeki Koji Okushi Hiroharu Yui Kozo Konno Yasushi Katayama Takashi Miura 《Journal of power sources》2010,195(18):6069-6074
Poly(acrylic acid) (PAA), poly(methacrylic acid) (PMA), and poly(vinyl alcohol) (PVA), which have oxygen species as functional groups, were utilized as a binder for graphite electrodes, and the electrochemical reversibility of lithium intercalation was examined in PC medium and ionic liquid electrolyte, lithium bis(trifluoromethanesulfonyl)amide dissolved in 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesulfonyl)amide (BMP-TFSA). Columbic efficiency of 75–80% with more than 300 mAh g?1 was achieved upon first reduction/oxidation cycle in both electrolytes using these binding polymers, which were significantly improved in comparison to a conventional PVdF binder (less than 45% of columbic efficiency for the first cycle). For the graphite-PVdF electrode, co-intercalation and/or decomposition of PC molecules solvating to Li ions were observed by the electrochemical reduction, resulting in the cracking of graphite particles. In contrast, the co-intercalation and decomposition of PC molecules and BMP cations for the first reduction process were completely suppressed for the graphite electrodes prepared with the polymers containing oxygen atoms. It was proposed that the selective permeability of lithium ions was attained by the uniform coating of the graphite particles with PAA, PMA, and PVA polymers, because the electrostatic interaction between the positively charged lithium ions and negatively charged oxygen atom in the polymer should modulate the desolvation process of lithium ions during the lithium intercalation into graphite, showing the similar functions like artificial solid-electrolyte interphase. 相似文献
135.
A method to detect slip frequency from rotor slot harmonics of a three-phase squirrel-cage induction motor is proposed. The rotor slot harmonic voltage Is obtained by summing the three phase voltages, and after being sampled with a multiple of the stator frequency, it is changed into slip frequency waves, from which a voltage proportional to the slip frequency is obtained. Sophisticated sampling techniques allow elimination of the third harmonic voltage induced in the sum of the three-phase voltages and also allow reduction of time constant of the slip frequency detector. Expenmental results show that the slip frequency detector has a good linearity in the range of slip frequency of about -50 to +30 percent of the stator frequency. 相似文献
136.
Suzuki K Sami M Kadokura H Nakajima H Kitamoto K 《International journal of food microbiology》2002,76(3):223-230
We isolated a strain from hop-resistant Lactobacillus hrevis ABBC45, which had lost a plasmid (pRH45) harboring a putative hop resistance gene, horA. The hop resistance level of this horA-deficient strain, named ABBC45(C), was initially low but gradually induced by repeated growth in media containing progressively increasing levels of hop compounds. Although the hop resistance level was substantially lower than that of the hop-adapted wild type strain, hop-adapted ABBC45(C) (ABBC45(CR)) was still capable of growing in beer, suggesting ABBC45 possesses at least two hop resistance mechanisms. Hop resistance acquired by ABBC45(CR) gradually diminished to the pre-adapted level, when the strain was grown repeatedly in the absence of hop compounds. ABBC45(CR) was found to be cross-resistant to several structurally unrelated drugs, including ethidium bromide, daunomycin and nisin. In addition, ABBC45(CR) was shown to extrude ethidium in an energy-dependent manner, while ABBC45(C) did not show such activity. This indicates that the efflux pump was induced by adaptation to hop compounds. The efflux activity of ethidium was reduced by the addition of hop compounds, suggesting hop compounds are also the substrate of the efflux pump. It was also shown that the efflux activity was completely dissipated with the abolition of proton motive force (PMF). These results, taken together, suggest the hop resistance mechanism of ABBC45(C) is mediated by PMF-dependent multidrug efflux pump. 相似文献
137.
We demonstrate a novel method of equalizing a laser diode (LD) beam into a circular beam. This method uses the twist effect of graded index (GI) fiber optics. An asymmetric LD beam with beam qualities of M2 = 500 in the slow axis and M2 = 4 in the fast axis is converted successfully into a symmetric circular beam with a beam quality of M2 = 175. The circular-output beam with 92% coupling efficiency from the fiber input to the fiber output is obtained with a 5-m-long GI1200 (1200 means a core diameter of 1200 microm) fiber for a 2-W LD array. We extend the experiments to a higher-power source with higher asymmetric beam qualities of M2 = 3000 and M2 = 4. By slightly bending the GI10000 (10000 means a core diameter of 10,000 microm) fiber, we have succeeded in generating a symmetric beam with a improved beam quality of M2 = 2000. The average beam quality is preserved when the asymmetric ratio is not high, and the beam quality degradation ratio is investigated up to asymmetric ratios of 750. 相似文献
138.
In this paper, we investigate iterative learning control (ILC) for non‐minimum phase systems from a novel viewpoint. For non‐minimum phase systems, the magnitude of a desiredinput obtained by ILC using forward‐time updating and Silverman's inversion are too large because of the influence of the unstable zeros. On the other hand, stable inversion constructs a bounded desired input by using non‐causal inverse for non‐minimum phase systems. In this paper, we first clarify that ILC using an adjoint system achieves the desired input defined by stable inversion. Hence, ILC using an adjoint system is an effective method for the control of non‐minimum phase systems with uncertainty. However, a useful convergence condition of ILC using an adjoint system was not achieved. Next, we develop a simple convergence condition in the frequency domain. 相似文献
139.
In this paper we propose a new software development process simulation model. The model can predict variations of productivity based on dynamic changes in the developer's knowledge structure. An important concept of the model is that a developer's productivity is influenced by the developer's knowledge. Moreover, a developer can acquire new knowledge by executing activities of a project. In other words, the developer's knowledge structure changes during the project. The knowledge structure is defined using a cognitive map that consists of knowledge elements and prerequisite relationships among the knowledge elements. By adding the specific developer's knowledge and the specific project workload to the knowledge structure, an increment of the developer's knowledge and the project progress are calculated into the model. The simulation results are useful for making project plans including technical reviews, which are an efficient technique for acquiring new knowledge. The simulation model can predict what knowledge should be discussed in the technical review, when the review should be held, and who the members of the review should be. The simulation results help managers make the most appropriate and executable project plan. 相似文献
140.
OBJECTIVE: To determine the utility of CT-determined main pulmonary artery diameter (MPAD) for predicting pulmonary hypertension (PH) in patients with parenchymal lung disease. DESIGN: Retrospective review of right-heart hemodynamic data and chest CT scans in 45 patients. SETTING: Tertiary-referral teaching hospital and VA hospital. PATIENTS: Between October 1990 and December 1995, 36 patients referred for evaluation of parenchymal lung disease or possible pulmonary vascular disease were found to have PH, as defined by mean pulmonary artery pressure (mPAP) > or =20 mm Hg. Nine control patients (mPAP <20 mm Hg) were also identified (4 from hospital records search, 5 after evaluation for possible PH). RESULTS: CT-determined MPAD was 35+/-6 mm in patients with PH and 27+/-2 mm in control subjects. In our group of patients, MPAD > or =29 mm had a sensitivity of 87%, specificity of 89%, positive predictive value (PPV) of 0.97, and positive likelihood ratio (LR) of 7.91 for predicting PH; in the subgroup of patients with parenchymal lung disease (n=28, PH and control subjects), MPAD > or =29 mm had a sensitivity of 84%, specificity of 75%, PPV of 0.95, and positive LR of 3.36 for predicting PH. The most specific findings for the presence of PH were both MPAD > or =29 mm and segmental artery-to-bronchus ratio > 1:1 in three or four lobes (specificity, 100%). There was no linear correlation between the degree of PH and MPAD (r=0.124). CONCLUSIONS: CT-determined MPAD has excellent diagnostic value for detection of PH in patients with advanced lung disease. Therefore, standard chest CT scans can be used to screen for PH as a cause of exertional limitation in patients with parenchymal lung disease. Because CT is commonly used to evaluate parenchymal lung disease, this information is readily available. 相似文献